Morphology of Platinum Nanowire Array Electrodepostied Within Anodic Aluminium Oxide Template Characterized by Atomic Force Microscopy |
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作者姓名: | KONGLing-Bin LUMei LIMeng-Ke GUOXin-Yong LIHu-Lin |
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作者单位: | [1]CollegeofChemistryandChemicalEngineering,LanzhouUniversity,Lanzhou730000 [2]LaboratoryofSpecialFunctionalMaterials,HenanUniversity,Kaifeng475001 |
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摘 要: | Unifrom platinum nanowires were synthesized by electrodepositing the platinum under a very low altering current frequency(20Hz) and increasing voltage(5-15V)in the proes of anodic aluminium oxide(AAO) template. Atomic force microscopy observation indicates that the template membranes we obtained have hexagonally clse-packed nanochannels.The platinum nanowires have highly ordered arrays after partially dissolving the aluminium oxide membrane.With the increasing dissolvoing time,the platinum nanowire array collapsed.A concave topography of the aluminium substrate was observed after the aluminium oxide membrane was dissolved completely and the platinum nanowires were released from the template.Platinum nanowires were also characterized by transmission electron microscopy and the phase structure of the Al/AAO/Pt composite was proven by x-ray diffraction.
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关 键 词: | 原子力显微镜 氧化铝薄膜 铂 X射线衍射 显微结构 |
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