| 气相-质谱联用分析冠心苏合丸中的挥发性组分 |
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| 引用本文： | 孙秀燕,吴建兵,王素娟.气相-质谱联用分析冠心苏合丸中的挥发性组分[J].色谱,2002,20(4):378-380. |
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| 作者姓名： | 孙秀燕 吴建兵 王素娟 |
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| 作者单位： | 1. 沈阳药科大学分析测试中心,辽宁,沈阳,110016
2. 沈阳药科大学中药学院,辽宁,沈阳,110016 |
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| 摘 要： | 采用气相 质谱联用对冠心苏合丸及药材中的挥发性成分进行了分析。采用选择离子监测法 ,以水杨酸甲酯为内标 ,对冠心苏合丸中的两个指标成分冰片和苯甲酸苄酯进行了定量测定。冰片和苯甲酸苄酯的平均加标回收率分别为 91 7%和 89 7% ,RSD分别为 5 6 %和 2 3%。
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| 关 键 词： | 气相质谱 挥发性组分 冰片 苯甲酸苄酯 冠心苏合丸 |
| 文章编号： | 1000-8713(2002)04-0378-03 |
| 修稿时间： | 2001年11月15 |
Determination of Volatile Constituents in Guanxin Suhe Wan by Gas Chromatography-Mass Spectrometry |
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| SUN Xiu yan ,WU Jian bing ,WANG Su juan.Determination of Volatile Constituents in Guanxin Suhe Wan by Gas Chromatography-Mass Spectrometry[J].Chinese Journal of Chromatography,2002,20(4):378-380. |
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| Authors: | SUN Xiu yan WU Jian bing WANG Su juan |
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| Institution: | Center of Instrumental Analysis, Shenyang Pharmaceutical University, Shenyang 110016, China. |
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| Abstract: | The volatile constituents of Guanxin Suhe Wan and its ingredient drugs were analyzed by gas chromatography mass spectrometry. Two compounds, borneol and benzyl benzoate were determined by selected ion monitoring with methyl salicylate as the internal standard. The recoveries of borneol and benzyl benzoate were 91 7% and 89 7% with the RSDs of 5 6% and 2 3%, respectively |
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| Keywords: | gas chromatography mass spectrometry volatile constituent borneol benzyl benzoate Guanxin Suhe Wan |
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