Microwave-Assisted Synthesis of Disulfides |
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Authors: | Halil Kutuk Nalan Turkoz |
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Institution: | Ondokuz May?s üniversitesi, Fen-Edebiyat Fakültesi, Kimya B?lümü , Samsun , Atakum , Turkey |
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Abstract: | Abstract A new microwave-assisted synthesis methodology for the preparation of substituted disulfide derivatives is presented. 4-Substituted sulfenimides were reacted with 4-substituted thiols under neat (to right doughy consistency) conditions in chloroform, with both microwave heating and conventional methods. The resulting 4-substituted disulfide derivatives were obtained at higher yields and in shorter reaction times with microwave heating. Their chemistry was confirmed by 1H-NMR, 13C-NMR, infrared (IR), and elemental analysis. GRAPHICAL ABSTRACT |
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Keywords: | Disulfides microwave microwave effect synthesis |
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