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原子吸收光谱法测定过氧化氢-柠檬酸溶液中铁铬镍钴
引用本文:李珊,杨桂荣,周贤玉.原子吸收光谱法测定过氧化氢-柠檬酸溶液中铁铬镍钴[J].理化检验(化学分册),1999(12).
作者姓名:李珊  杨桂荣  周贤玉
作者单位:中南工学院 衡阳421001 (李珊,杨桂荣),中南工学院 衡阳421001(周贤玉)
基金项目:核工业科学基金资助项目
摘    要:研究了原子吸收光谱法测定压水堆主回路去污液过氧化氢-柠檬酸溶液中铁、铬、镍、钴的影响因素,选择了合适的测量条件,用合成样品进行了试验.结果表明.铁、钴、镍、铬含量在0.5~5mg·L~(-1)范围的回收率为100%±10%,相对标准偏差为6.0%~10%.

关 键 词:原子吸收光谱法  压水堆主回路        

A AS DETERMINATION OF Fe Cr Ni AND Co IN A DETERGENT COMPOSING HYDROGEN PEROXIDE AND CITRIC ACID
Li Shan,Yang Quirong and Zhou Xianyu.A AS DETERMINATION OF Fe Cr Ni AND Co IN A DETERGENT COMPOSING HYDROGEN PEROXIDE AND CITRIC ACID[J].Physical Testing and Chemical Analysis Part B:Chemical Analgsis,1999(12).
Authors:Li Shan  Yang Quirong and Zhou Xianyu
Abstract:Optimum conditions for the AAS determination of Fe?Cr?Ni and Co in a detergent composing H_2O_2 and citric acid are studied and reported in this paper. For all these elements, a recovery of 100% ?10% is obtained for the concentration range of 0. 5~5mg ?L~(-1). RSD obtained for the determination lies between 6% ~ 10%.
Keywords:AAS  Pressurized water reactor  Fe  Cr  Ni  Co
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