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示波极谱滴定法测定盐酸氯喘等药物
引用本文:卢宗桂,朱俊杰,李伯南,高鸿.示波极谱滴定法测定盐酸氯喘等药物[J].化学研究与应用,1991(4).
作者姓名:卢宗桂  朱俊杰  李伯南  高鸿
作者单位:南京大学化学系,南京大学化学系,南京大学化学系,南京大学化学系 南京 210008,南京 210008,南京 210008,南京 210008
摘    要:盐酸氯喘,盐酸阿米替林和维生系B_6都是常用药物,中国药典和上海市药品标准用非水滴定法测定它们的含量,比较麻烦。梁云爱等用示波滴定法测定维生素B_6的含量,采用NaoH中和滴定测定盐酸吡多醇中的盐酸部分。我们在一定pH值的醋酸—

关 键 词:示波极谱滴定  盐酸氯喘  盐酸阿米替林  维生素B_6

DETERMINATION OF PHARMACEUTICALS BY OSCILLPOLAROGRAPHIC TITRATION
Lu Zonggui,Zhu Junjie,Li Bainan,H.Kao.DETERMINATION OF PHARMACEUTICALS BY OSCILLPOLAROGRAPHIC TITRATION[J].Chemical Research and Application,1991(4).
Authors:Lu Zonggui  Zhu Junjie  Li Bainan  HKao
Institution:Lu Zonggui,Zhu Junjie,Li Bainan,H.Kao Department fo Chemistry,Nanjing University,Nanjing 210008
Abstract:Oscillopolarographic titration can be applied to determine clorprenaline hydrochloride, amitriptyline hydrochloride and pyridoxin hydrochloride. The sample was precipitated with Na- PTB solution and the excess standard Na-TPB was back titrated with standard Tl_2SO_4 solution or hexadecyl pyridine chloride solution. The disappearance of the incision of Na-TPB on its oscillopolarogram indicated the endpoint the titration. The method is accurate, convenient and rapid.
Keywords:Oscillopolarographic Titration  Clorprena1ine Hydrochloride  Amitriptyline Hydrochloride  Pyridotin Hydrochloride
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