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1.
Matthias Mawick Carolin Jaworski Jens Bittermann Dr. Ljuba Iovkova Yinglan Pu Prof. Dr. Carmen Wängler Prof. Dr. Björn Wängler Prof. Dr. Klaus Jurkschat Prof. Dr. Norbert Krause Prof. Dr. Ralf Schirrmacher 《Angewandte Chemie (International ed. in English)》2023,62(50):e202309002
The ring-opening Si-fluorination of a variety of azasilole derivatives cyclo-1-(iPr2Si)−4-X−C6H3−2-CH2NR ( 4 : R=2,6-iPr2C6H3, X=H; 4 a : R=2,4,6-Me3C6H2, X=H; 9 : R=2,6-iPr2C6H3, X=tBuMe2SiO; 10 : R=2,6-iPr2C6H3, X=OH; 13 : R=2,6-iPr2C6H3, X=HCCCH2O; 22 : R=2,6-iPr2C6H3, X=tBuMe2SiCH2O) with different 19F-fluoride sources was studied, optimized and the experience gained was used in a translational approach to create a straightforward 18F-labelling protocol for the azasilole derivatives [18F] 6 and [18F] 14 . The latter constitutes a potential clickable CycloSiFA prosthetic group which might be used in PET tracer development using Cu-catalysed triazole formation. Based on our findings, CycloSiFA has the potential to become a new entry into non-canonical labelling methodologies for radioactive PET tracer development. 相似文献
2.
The tomographic reconstruction of supersonic flows faces two challenges. Firstly, techniques used in the past, such as the
direct Fourier method (DFM) (Gottlieb and Gustafsson in On the direct Fourier method for computer tomography, 1998; Morton
in Tomographic imaging of supersonic flows, 1995) or various backprojection (Kak and Slaney in Principles of computerized
tomographic imaging, vol. 33 in Classics in Applied Mathematics, 2001) techniques, have only been able to reconstruct areas
of the flow which are upstream of any opaque objects, such as a model. Secondly, shock waves create sharp discontinuities
in flow properties, which can be difficult to reconstruct both in position and in magnitude with limited data. This paper
will present a reconstruction method, matrix inversion using ray-tracing and least squares conjugate gradient (MI-RLS), which uses geometric ray-tracing and a sparse matrix iterative solver (Paige and Saunders in ACM Trans. Math. Softw.
8(1):43–71, 1982) to overcome both of these challenges. It will be shown, through testing with a phantom object described
in tomographic literature, that the results compare favourably to those produced by the DFM technique. Finally, the method
will be used to reconstruct three-dimensional density fields from interferometric shock layer images, with good resolution
(Faletič in Tomographic reconstruction of shock layer flows, 2005).
This paper was based on work that was presented at the 3rd International Symposium on Interdisciplinary Shock Wave Research,
Canberra, Australia, March 1–3, 2006. 相似文献
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4.
为实现正电子发射断层成像(Positron Emission Tomography,PET)探测器的作用深度(Depth Of Interaction,DOI)信息获取,本文提出一种基于分光技术的探测器设计方案.探测器采用晶体单元与硅光电倍增管(Silicon Photomultiplier,SiPM)一对一耦合、蛇形光路的设计和单端Anger加权读出方法进行DOI解码.基于GATE软件进行蒙特卡罗模拟,建立8×1的LSO晶体阵列(单根晶体尺寸3.1×3.1×20mm3);模拟泛场照射获取位置查找表;并进行不同深度的模拟,获得各晶体在各深度的空间分辨率.结果显示所模拟的探测器模块DOI分辨率在1.0~6.7mm之间,平均值为3.2mm.本文提出的基于蛇形光路的PET探测器方案能在维持系统成本和复杂度的前提下实现DOI解码,提升PET系统的成像性能. 相似文献
5.
6.
S.M.Mefire 《计算数学(英文版)》2009,(4):495-524
From a limit model in electric field obtained by letting the frequency vanish in the time-harmonic Maxwell equations, we consider a limit perturbation model in the tangential boundary trace of the curl of the electric field for localizing numerically certain small electromagnetic inhomogeneities, in a three-dimensional bounded domain. We introduce here two localization procedures resulting from the combination of this limit perturbation model with each of the following inversion processes: the Current Projection method and an Inverse Fourier method. Each localization procedure uses, as data, a finite number of boundary measurements, and is employed in the single inhomogeneity case; only the one based on an Inverse Fourier method is required in the multiple inhomogeneities case. Our localization approach is numerically suitable for the context of inhomogeneities that are not purely electric. We compare the numerical results obtained from the two localization procedures in the single inhomogeneity configuration, and describe, in various settings of multiple inhomogeneities, the results provided by the procedure based on an Inverse Fourier method. 相似文献
7.
为了同时获取样品的表面和深度信息,研究光学相干层析的成像原理,建立了基于光学相干层析技术的内窥系统,实现了旋转扫描成像,系统的工作波长为1 310 nm,工作带宽为80 nm.理论推导及计算机仿真得到了系统信噪比与干涉仪的分光比、反射率之间的关系并分析了理论分辨率和探测深度.提出外径为5 mm的内窥镜扫描探头,聚焦距离为12 mm,数值孔径NA为0.47,折射率分布常量A=0.218 7.利用微型电机驱动直角棱镜实现扫描,旋转速度为25 rpm,旋转一周得到640个采样点.采用多层盖玻片和洋葱表皮作为样品进行实验分析,得到了盖玻片和洋葱的图像,横向分辨率和纵向分辨率分别为10 μm和15 μm.结果表明,设计的光学相干层析内窥系统能够用于旋转扫描成像,获取更多的组织信息. 相似文献
8.
A tomographic reconstruction method based on Monte Carlo random searching guided by the information contained in the projections
of radiographed objects is presented. In order to solve the optimization problem, a multiscale algorithm is proposed to reduce
computation. The reconstruction is performed in a coarse-to-fine multigrid scale that initializes each resolution level with
the reconstruction of the previous coarser level, which substantially improves the performance. The method was applied to
a real case reconstructing the internal structure of a small metallic object with internal components, showing excellent results. 相似文献
9.
10.
Exterior tomographic data are taken over lines outside a central region, and such data occur in the industrial nondestructive evaluation of large objects such as rockets. We explain, using microlocal analysis, which singularities are well reconstructed from exterior data, and we explain how this phenomenon is reflected in the singular value decomposition for the exterior transform [E.T. Quinto, Singular value decompositions and inversion methods for the exterior Radon transform and a spherical transform, J. Math. Anal. Appl. 95 (1983) 437–448]. We extend Lambda Tomography to exterior data and to limited angle exterior data. The algorithm is tested on industrial data from Perceptics, Inc. 相似文献