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排序方式: 共有173条查询结果,搜索用时 15 毫秒
1.
Jung‐woo Chae Hyun‐moon Baek Sang Kyum Kim Ho‐il Kang Kwang‐il Kwon 《Biomedical chromatography : BMC》2013,27(8):953-955
The major metabolite of duloxetine is a glucuronide conjugate of 4‐hydroxy duloxetine (4‐HD). However, interestingly, there have been no reports determining concentrations of 4‐HD and no fully validated method has been established for measuring duloxetine and 4‐HD in rat plasma. We developed a method for the simultaneous quantification of duloxetine and its metabolite in rat plasma using high‐performance liquid chromatography tandem mass spectrometry. Duloxetine and 4‐HD were analyzed on a reverse‐phase C18 analytical column after protein precipitation of the plasma sample with methanol, using carbamazepine as an internal standard. The isocratic mobile phase of 5 mm ammonium acetate–methanol (4:6, v/v) was eluted at 0.4 mL/min. Quantification was performed on a triple‐quadrupole mass spectrometer using electrospray ionization, and the ion transition monitored in selective reaction monitoring mode. The coefficient of variation for assay precision was <18.0%, and the accuracy was 84.0–118.0%. This method was successfully used to measure the concentrations of duloxetine and its metabolite in plasma following the oral administration of a single 40 mg/kg dose in rats. Copyright © 2013 John Wiley & Sons, Ltd. 相似文献
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New explicit exact solutions to a nonlinear dispersive-dissipative equation 总被引:1,自引:0,他引:1 下载免费PDF全文
Using the first-integral method, we obtain a series of new explicit exact solutions such as exponential function solutions, triangular function solutions, singular solitary wave solution and kink solitary wave solution of a nonlinear dispersive-dissipative equation, which describes weak nonlinear ion-acoustic waves in plasma consisting of cold ions and warm electrons. 相似文献
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Adiabatic population transfer in effective three-level systems driven by laser beams 总被引:1,自引:0,他引:1 下载免费PDF全文
The population transfer in effective three-state systems driven by laser beams has been studied based on the theory of Lewis-Riesenfeld Hermitian invariants in the full- and partial-adiabatic approximations. A strict formulation of adiabatic conditions is given, and a new adiabatic condition for inducing a complete population transfer is found. 相似文献
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An alternating periodic-chaotic ISI sequence of HH neuron under external sinusoidal stimulus 下载免费PDF全文
A study of Hodgkin-Huxley (HH) neuron under external sinusoidal excited stimulus is presented in this paper. As is well known, the stimulus frequency is to be considered as a bifurcate parameter, and numerous phenomena, such as synchronization, period, and chaos appear alternatively with the changing of the stimulus frequency. For the stimulus frequency less than 2fB (fB being the base frequency in this paper), the simulation results demonstrate that the single HH neuron could completely convey the sinusoidal signal in anti-phase into interspike interval (ISI) sequences. We also report, perhaps for the first time, another kind of phenomenon, the beat phenomenon, which exists in the phase dynamics of the ISI sequences of the HH neuron stimulated by a sinusoidal current. It is shown furthermore that intermittent transition results in the general route to chaos. 相似文献
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Fractal localized structures related to Jacobian elliptic functions in the higher-order Broer-Kaup system 下载免费PDF全文
This work reveals a novel phenomenon—that the localized coherent structures of a (2﹢1)﹣dimensional physical model possesses fractal behaviours. To clarify the interesting phenomenon, we take the (2﹢1)﹣dimensional higher-order Broer-Kaup system as a concrete example. Starting from a B?cklund transformation, we obtain a linear equation, and then a general solution of the system is derived. From this some special localized excitations with fractal behaviours are obtained by introducing some types of lower-dimensional fractal patterns that related to Jacobian elliptic functions. 相似文献
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Photoemission spectra are measured for Yb covered surface of wet-chemically-etched H-Si (111). The results reveal that the lattice structure of the H-Si (111) surface is stable against the deposition of Yb atoms. X-ray photoemission spectra indicate the formation of a polarized (dipole) surface layer, with the silicon negatively charged. Ultraviolet photoemission spectra exhibit the semiconducting property of the interface below one monolayer coverage. Work function variation during the formation of the Yb/H-Si (111) interface is measured by the secondary-electron cutoff in the ultraviolet photoemission spectral line. The largest decrease of work function is ~1.65eV. The contributions of the dipole surface layer and the band bending to the work function change are determined to be ~1.15eV and ~0.5eV, respectively. The work function of metal Yb is determined to be ~2.80±0.05eV. 相似文献
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Ground state properties of a Bose-Einstein condensate confined in an anharmonic external potential 下载免费PDF全文
In light of the interference experiment of Bose-Einstein condensates, we present an anharmonic external potential model to study ground state properties of Bose-Einstein condensates. The ground state energy and the chemical potential have been analytically obtained, which are lower than those in harmonic trap. Additionally, it is found that the anharmonic strength of the external potential has an important effect on density and velocity distributions of the ground state for the Thomas-Fermi model. 相似文献
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Comprehensive research about the cooperative up-conversion luminescence of the ytterbium-doped oxyfluoride vitroceramics 下载免费PDF全文
The cooperative up-conversion blue luminescence of Yb^{3+} ion-doped oxyfluoride vitroceramic material (Yb:FOV) and the influence of co-doped Ho^{3+} ion, when excited by a 960 nm diode-laser, are studied in this paper. A strong blue 479.1 nm up-conversion luminescence of the Yb:FOV material is discovered. It is found that the 479.1 nm luminescence results from the cooperative up-conversion of the coupled states of the Yb^{3+}-Yb^{3+} clusters formed by two adjacent Yb^{3+} ions. The measured cooperative up-conversion luminescence main peak 479.1 nm of this paper is different from the characteristic fluorescence main peak of the Tb^{3+} ion positioned at about 495-504 nm wave-range. Our result coincides with all the published correct papers, whose cooperative up-conversion luminescence main peaks of the direct Yb^{3+}-Yb^{3+} clusters are all positioned at about 476-480 nm wave-range. All of these indicate that the large cooperative up-conversion blue luminescence of the direct Yb^{3+}-Yb^{3+} clusters discovered in this paper is stable. It further proves that the cooperative up-conversion green luminescence may result from the Yb^{3+}-Tb^{3+} cooperative effect. In particular, the original work of this paper improves considerably on the traditional concept by the experimental facts that the blue 479.1 nm cooperative up-conversion luminescence strength of Yb(5):FOV is 230 times greater than that of fluoride glass Yb(3):ZBLAN. This is a great development to meet the practical requirements for blue up-conversion luminescence strength. This result indicates that the large cooperative up-conversion blue luminescence could be achieved excellently by using a suitable material, such as oxyfluoride vitroceramic, which provides a better chance to form better Yb^{3+}-Yb^{3+} clusters and has less relaxation to keep the more efficient up-conversion luminescence. It is also found that impurities seriously reduce the cooperative up-conversion luminescence intensity due to the cross-relaxation from the Yb^{3+}-Yb^{3+} clusters, which means that the cooperative up-conversion blue luminescence could be further improved by pure Yb^{3+} ion-doped materials that have as few impurities as possible to reduce the cross-relaxation. The large cooperative up-conversion blue luminescence of Yb(5):FOV also comes from its higher concentration (5 mol%) of activator Yb^{3+} ion which acts well because the cooperative up-conversion blue luminescence intensity varies linearly against the square of the concentration of Yb^{3+} ions in the range of 0.5-5 mol%. In summary, the great improvement of our work on cooperative up-conversion blue luminescence results from the comprehensive enhancement of the factors of better-coupled chance of the Yb^{3+}-Yb^{3+} clusters, less cross-relaxation, better concentration contribution of Yb^{3+} activator, non-saturation, and better up-conversion luminescence efficiency. 相似文献