工作气压对电子束沉积ZrO2薄膜折射率和聚集密度的影响

采用电子束蒸发的方法，用石英晶体振荡法监控薄膜的蒸发速率，在不同工作气压下制备了ZrO2薄膜样品.在相调制型椭圆偏振光谱仪和分光光度计上对样品的光谱特性进行了测试.根据波长漂移的理论，计算出薄膜的聚集密度.结果表明，随着工作气压的降低，薄膜的聚集密度和折射率都随之增大.     

N指标d维广义Wiener过程象集的m项代数和的几个性质

设珮犠（狋）：犚犖＋ →犚犱是犖指标犱维广义Ｗｉｅｎｅｒ过程，对任意紧集犈１，…，犈犿犚犖＞ ，该文研究了犿项代数和珮犠（犈１）…珮犠（犈犿）的Ｈａｕｓｄｏｒｆｆ维数，Ｐａｃｋｉｎｇ维数和正的Ｌｅｂｅｓｇｕｅ测度及内点的存在性． 其结果包含并推广了布朗单的结果．     

PACKING PAIRS BY QUINTUPLES:THE CASE OF ZERO CONGRUENCE MOD 4

ＰＡＣＫＩＮＧＰＡＩＲＳＢＹＱＵＩＮＴＵＰＬＥＳ：ＴＨＥＣＡＳＥＯＦＺＥＲＯＣＯＮＧＲＵＥＮＣＥＭＯＤ４ＹＩＮＪＩＡＮＸＩＮＧＡｂｓｔｒａｃｔ：ＬｅｔＤ（ｖ）ｄｅｎｏｔｅｔｈｅｍａｘｉｍｕｍｎｕｍｂｅｒｏｆｑｕｉｎｔｕｐｌｅｓｏｆａｖ－ｓｅｔｏｆｐｏ...     

Packing into the smallest square: Worst-case analysis of lower bounds

We address the problem of packing a given set of rectangles into the minimum size square. We consider three versions of the problem, arising when the rectangles (i) are squares; (ii) have a fixed orientation; (iii) can be rotated by 90. For each case we study lower bounds, and analyze their worst-case performance ratio. In addition, we evaluate through computational experiments their average performance on instances from the literature.     

A hybrid genetic algorithm-heuristic for a two-dimensional orthogonal packing problem

In this paper we address a two-dimensional (2D) orthogonal packing problem, where a fixed set of small rectangles has to be placed on a larger stock rectangle in such a way that the amount of trim loss is minimized. The algorithm we propose hybridizes a placement procedure with a genetic algorithm based on random keys. The approach is tested on a set of instances taken from the literature and compared with other approaches. The computation results validate the quality of the solutions and the effectiveness of the proposed algorithm.     

The nanogranular nature of C-S-H

Despite its ubiquitous presence as binding phase in all cementitious materials, the mechanical behavior of calcium-silicate-hydrates (C-S-H) is still an enigma that has deceived many decoding attempts from experimental and theoretical sides. In this paper, we propose and validate a new technique and experimental protocol to rationally assess the nanomechanical behavior of C-S-H based on a statistical analysis of hundreds of nanoindentation tests. By means of this grid indentation technique we identify in situ two structurally distinct but compositionally similar C-S-H phases heretofore hypothesized to exist as low density (LD) C-S-H and high density (HD) C-S-H, or outer and inner products. The main finding of this paper is that both phases exhibit a unique nanogranular behavior which is driven by particle-to-particle contact forces rather than by mineral properties. We argue that this nanomechanical blueprint of material invariant behavior of C-S-H is a consequence of the hydration reactions during which precipitating C-S-H nanoparticles percolate generating contact surfaces. As hydration proceeds, these nanoparticles pack closer to center on-average around two characteristic limit packing densities, the random packing limit (η=64%) and the ordered face-centered cubic (fcc) or hexagonal close-packed (hcp) packing limit (η=74%), forming a characteristic LD C-S-H and HD C-S-H phase.     

钛-锆氧化物复合填料的正相色谱性能评价

采用油乳法制备了钛锆复合氧化物并系统评价了该填料的正相色谱性能。研究结果表明，该填料对碱性化合物有良好的分离选择性，峰形对称；但对酚类化合物强烈保留，峰形较差；中性化合物和碱性化合物的色谱行为均符合Snyder吸附顶替模型。     

Optimizing constrained subtrees of trees

Given a treeG = (V, E) and a weight function defined on subsets of its nodes, we consider two associated problems. The first, called the rooted subtree problem, is to find a maximum weight subtree, with a specified root, from a given set of subtrees.The second problem, called the subtree packing problem, is to find a maximum weight packing of node disjoint subtrees chosen from a given set of subtrees, where the value of each subtree may depend on its root.We show that the complexity status of both problems is related, and that the subtree packing problem is polynomial if and only if each rooted subtree problem is polynomial. In addition we show that the convex hulls of the feasible solutions to both problems are related: the convex hull of solutions to the packing problem is given by pasting together the convex hulls of the rooted subtree problems.We examine in detail the case where the set of feasible subtrees rooted at nodei consists of all subtrees with at mostk nodes. For this case we derive valid inequalities, and specify the convex hull whenk 4.Research supported in part by Nato Collaborative Research Grant CRG 900281, Science Program SC1-CT91-620 of the EEC, and contract No 26 of the programme Pôle d'attraction interuniversitaire of the Belgian government.     

A note on packing paths in planar graphs

Seymour (1981) proved that the cut criterion is necessary and sufficient for the solvability of the edge-disjoint paths problem when the union of the supply graph and the demand graph is planar and Eulerian. When only planarity is required, Middendorf and Pfeiffer (1993) proved the problem to be NP-complete. For this case, Korach and Penn (1992) proved that the cut criterion is sufficient for the existence of a near-complete packing of paths. Here we generalize this result by showing how a natural strengthening of the cut criterion yields better packings of paths.Analogously to Seymour's approach, we actually prove a theorem on packing cuts in an arbitrary graph and then the planar edge-disjoint paths case is obtained by planar dualization. The main result is derived from a theorem of Seb (1990) on the structure of ±1 weightings of a bipartite graph with no negative circuits.Research partially supported by the Hungarian National Foundation for Scientific Research Grants OTKA 2118 and 4271.     

Packing capilllary electrochromatography columns using vacuum--a preliminary study

This paper introducesa novel method for packing Capillary Electrochromatography Columns (CEC). Using vacuum packing methodology, silica particles as small as 1 microm were successfully packed into the capillary columns with 75 microm inner diameter. The columns are verystable and show no noticeable loss in efficiency after 200 sample injections. The performance of these vacuum packed capillary columns was evaluated with a mixture of aromatic and non-aromatic compounds. A 24 cm long capillary column can produce peak efficiencies of around 45,000 plates for benzene.