塞曼石墨炉原子吸收光谱法直接测定垃圾焚烧废气中锡

采用钯加抗坏血酸溶液作为基体改进荆，用塞曼效应扣除背景，对消化后的垃圾焚烧废气滤筒直接进行测定。方法的检出限为100pg，线性范围为0．2～4ng，回收率为96．8％～102．0％。     

试题质量评价研究

教学过程的规范化管理是保证教学质量的重要手段。考试是对教和学的效果的检验，是教学过程管理规范化必须要解决的问题，一直受到教学管理部门的重视，采取了多项措施解决有关问题，其中一个重要的手段是采用试题库。在采用试题库时，必须要有高质量的试题作保证。本探讨基于KDD技术的试题质量评价方法和指标，并通过实例来说明其有效性。     

BOUNDEDNESS OF FRACTIONAL INTEGRALS IN HARDY SPACES WITH NON-DOUBLING MEASURE - In Memory of Professor Sun Yongsheng

Let μ be a Borel measure on Rd which may be non doubling. The only condition that μ must satisfy is μ(Q) ≤ col(Q)n for any cube Q () Rd with sides parallel to the coordinate axes and for some fixed n with 0 ＜ n ≤ d. The purpose of this paper is to obtain a boundedness property of fractional integrals in Hardy spaces H1 (μ).     

全面成绩管理的初探

利用数量化方法,数字特征法,W ilcoxon顺序和检验法以及试卷分析的各种方法(试题难度,区分度,信度,效度等),定量地解决了影响学生成绩的主要因素,并引入全面管理方法,明显地改善了学生成绩,学生综合能力明显加强.     

超声波在废橡胶再生中应用的最新进展

全世界每年产生大量废旧橡胶，它们需要很长时间才能降解，这既污染环境，又浪费资源，解决此问题的唯一方法是再生利用。在众多再生方法中，新近出现的超声波脱硫再生法，被认为是最有希望的方法，本文详细地介绍了这方面的最新进展情况。     

UNIFORM CONVERGENCE OF CESARO MEANS OF NEGATIVE ORDER OF DOUBLE TRIGONOMETRIC FOURIER SERIES

In this paper we prove that iff ∈ C([-π,π]2) and the function f is bounded partial p-variation for some p ∈ [1, ∞), then the double trigonometric Fourier series of a function f is uniformly (C;-α,-β) summable (α β＜ 1/p,α,β＞ 0) in the sense of Pringsheim. If α β≥ 1/p, then there exists a continuous function f0 of bounded partial double trigonometric Fourier series of fo diverge over cubes.     

XPS investigations of ink‐jet printed paper

Different ink‐jet printed paper materials were investigated using X‐ray photoelectron spectroscopy (XPS) yielding the elemental composition of the near‐surface region of the papers. We found significant differences with respect to the detected elements and their atomic concentrations in the different inks studied here. Two different groups of inks could be identified by means of a lower ratio of the O and C atomic concentrations and lower concentrations in specific trace elements like Mg, Na and Si. High‐resolution spectra of C 1s and O 1s core levels allowed a detailed determination of the chemical state of the respective elements. On the basis of a detailed deconvolution of these XPS signals, significant differences between all the investigated ink‐jet printed papers were found, thereby allowing their discrimination. The applicability of the measurements and, more generally, the XPS technique for forensic investigations of paper are discussed. Copyright © 2007 John Wiley & Sons, Ltd.     

X射线荧光光谱滤纸片法测定矿石中的铜

我们用Ｘ射线荧光光谱滤纸片法分析了古今１３铜矿石样品中的铜含量，测量结果与化学法一致。此法不需要铜矿石的标样，而且手续简单，方便，检出限低，灵敏度高，测量结果正确可靠，是分析矿石中单一或几个元素的含量较好的方法之一。     

Development and critical comparison of greener flow procedures for nitrite determination in natural waters

Two greener procedures for flow-injection spectrophotometric determination of nitrite in natural waters were developed and critically compared. Replacement of toxic reagents, waste minimization and treatment were exploited to attend the standards of clean chemistry. The flow system was designed with solenoid micro-pumps in order to minimize reagent consumption and waste generation. The first procedure is based on the Griess diazo-coupling reaction with sulfanilamide and N-(1-naphthyl)ethylenediamine (NED) yielding an azo dye, followed by photodegradation of the low amount of waste generated based on the photo-Fenton reaction. The second procedure is based on the formation of iodine from nitrite and iodide in acid medium in order to avoid the use of toxic reagents. For Griess method, linear response was achieved up to 1.0 mg L^− 1, described by the equation A = − 0.007 + 0.460C (mg L^− 1), r = 0.999. The detection limit was estimated as 8 μg L^− 1 at the 99.7% confidence level and the coefficient of variation was 0.8% (n = 20). The sampling rate was estimated as 108 determinations per hour. The consumption of the most toxic reagent (NED) is reduced 55-fold and 20-fold in comparison to batch method and flow injection with continuous reagent addition, respectively. A colorless residue was obtained by in-line photodegradation with reduction of 87% of the total organic carbon content. The results obtained for natural water samples were in agreement with those achieved by the reference method at the 95% confidence level. For the nitrite–iodide method, linear response was observed up to 2.0 mg L^− 1, described by the equation A = − 0.024 + 0.148C (mg L^− 1), r = 0.999. The detection limit was estimated as 25 μg L^− 1 at the 99.7% confidence level and the coefficient of variation was 0.6% (n = 20). The sampling rate was estimated as 44 determinations per hour. Despite avoiding the use of toxic reagents, the nitrite–iodide method presented worst performance in terms of selectivity and sensitivity.     

固相微萃取/GC直接测定废水中的三种氯酚

研究了运用固相微萃取／GC直接测定水中的三种氯酚的方法，得到了分析三种氯酚的SPMF最佳萃取条件。选取聚丙烯酸酯（PA）萃取头，水溶液调pH=2,并用NaCl饱和，室温下在持续磁力搅拌下直接萃取40min，纤维萃取头在260℃脱附5min。所建立的方法适于快速、方便地测定水中三相氯酚，无须浓缩和预处理。