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排序方式: 共有358条查询结果,搜索用时 15 毫秒
1.
Rostami Sara Toghraie Davood Esfahani Masihollah Ahmadi Hekmatifar Maboud Sina Nima 《Journal of Thermal Analysis and Calorimetry》2021,143(2):1119-1128
Journal of Thermal Analysis and Calorimetry - In the current work, after generating experimental data points for different volume fraction of nanoparticles ( $$\phi$$ ) and different temperatures,... 相似文献
2.
In this research, the main emphasis has been focused on the preparation of a novel Fe3O4-supported propane-1-sulfonic acid-grafted graphene oxide quantum dots (Fe3O4@GOQD-O-(propane-1-sulfonic acid)) that it was readily synthesized via a five-step procedure as a hitherto unreported magnetic nanocatalyst. This newly prepared Fe3O4@GOQD-O-(propane-1-sulfonic acid) nanocomposite was structurally well-established by different analytical techniques including Fourier transform infrared (FT-IR), X-ray diffraction (XRD), energy-dispersive X-ray (EDX), thermal gravimetric analysis (TGA), field emission gun-scanning electron microscope (FESEM), high-resolution transmission electron microscopy (HRTEM) and vibrating sample magnetometer (VSM) analyses. The high catalytic performance of this nanocomposite was exhibited in one-pot synthesis of dihydropyrano[2,3-c]pyrazole and 4H-chromene derivatives under mild conditions. Low reaction times, excellent yields of the products, benignity of the catalyst, easy reaction work-up and magnetic recyclability of the catalyst are the main advantages of the present protocol. Also, our research indicated that the Fe3O4@GOQD-O-(propane-1-sulfonic acid) could be reused up to five times without considerable loss of catalytic activity. 相似文献
3.
Samaneh Mahmoudi‐GomYek Davood Azarifar Masoumeh Ghaemi Hassan Keypour Masoumeh Mahmoudabadi 《应用有机金属化学》2019,33(6)
A novel Cu (II) Schiff‐base complex immobilized on core‐shell magnetic Fe3O4 nanoparticles (Fe3O4@SPNC) was successfully designed and synthesized. The structural features of these nanoparticles were studied and confirmed by using various techniques including FT‐IR spectroscopy, scanning electron microscopy (SEM), transmission electron microscopy (TEM), energy‐dispersive X‐ray spectroscopy (EDS), vibrating sample magnetometer (VSM), X‐Ray diffraction (XRD), wavelength dispersive X‐ray spectroscopy (WDX), and inductively coupled plasma (ICP). These newly synthesized nanoparticles have been used as efficient heterogeneous catalytic system for one‐pot multicomponent synthesis of new pyrano[2,3‐b]pyridine‐3‐carboxamide derivatives. Notably, the catalyst could be easily separated from the reaction mixture by using an external magnet and reused for several successive reaction runs with no significant loss of activity or copper leaching. The present protocol benefits from a hitherto unreported MNPs‐immobilized Cu (II) Schiff‐base complex as an efficient nanocatalyst for the synthesis of newly reported derivatives of pyrano[2,3‐b]pyridine‐3‐carboxamide from one‐pot multicomponent reactions. 相似文献
4.
Karimi Kerdabadi Javad Haghanimanesh Maedeh Karimipour Arash Toghraie Davood Tlili Iskander 《Journal of Thermal Analysis and Calorimetry》2021,143(1):293-308
Journal of Thermal Analysis and Calorimetry - Hot-rolled strips are cooled on the run-out table to achieve the customer-required mechanical properties. Cooling reduces the oxidation, which can... 相似文献
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6.
We show that for an inverse semigroup S with the set idempotents E acting on S trivially from left and by multiplication from right, any bounded module derivation from \(\ell ^1(S)\) to \(({\ell ^1(S)}/{J})^*=J^{\perp }\) is inner, where J is the closed ideal generated by elements of the form \(\delta _{set}-\delta _{st}\) with \(s,t\in S\) and \(e\in E\). 相似文献
7.
Ghasemi Mahdi Niknejadi Mohammadreza Toghraie Davood 《Journal of Thermal Analysis and Calorimetry》2021,144(6):2483-2495
Journal of Thermal Analysis and Calorimetry - The thermal behavior of CuO-water nanofluid is examined on an aluminum surface. The dimensions of simulation boxes are... 相似文献
8.
Ebrahimiasl Hakimeh Azarifar Davood Mohammadi Mahsa Keypour Hassan Mahmood abadi Masoumeh 《Research on Chemical Intermediates》2021,47(2):683-707
Research on Chemical Intermediates - In this research, synthesis and characterization of a novel Schiff base Cu (II) complex immobilized on Fe3O4@SiO2 nanoparticles are reported. Then, the... 相似文献
9.
An efficient ionic liquid with both Brønsted acidic and Lewis basic sites, namely 1,4-dimethyl-1-(4-sulphobutyl)piperazinium hydrogen sulphate (IL1), was synthesised and characterised. IL1 is a “green”, homogeneous and reusable catalyst for: i) the synthesis of pyranopyrazoles (Va-Vj)and benzopyrans (VIa-VIj and VIIa-VIIf) at ambient temperature under solvent-free conditions and ii) the synthesis of amino-2-chromenes (VIIIa-VIIIi and IXa-IXi) and dihyropyrano[c]chromenes (Xa-Xi) at 80 °C under solvent-free conditions. The reactions were rapid with excellent product yields. In addition, the double Brønsted acid, 1,4-dimethyl-1,4-bis(4-sulphobutyl)piperazinium hydrogen sulphate (IL2), was prepared to evaluate the cooperation efficiency of their Brønsted acidic and Lewis basic sites as compared with the double Brønsted acidic sites in IL1. 相似文献
10.