磁控溅射(Ti,N)/Al纳米复合薄膜的微结构和力学性能

采用Al和TiN靶通过磁控共溅射方法, 制备了一系列Ti:N≈1的不同(Ti, N) 含量的铝基纳米复合薄膜, 利用X射线能量分散谱仪、X射线衍射仪、透射电子显微镜和纳米力学探针表征了薄膜的成分、 微结构和力学性能, 研究了(Ti, N)含量对复合薄膜微结构和力学性能的影响. 结果表明: Ti, N原子的共同加入使复合薄膜形成了同时具有置换固溶和间隙固溶特征的"双超过饱和固溶体", 薄膜的晶粒随着溶质含量的增加逐步纳米化, 并进一步形成非晶结构, 晶界区域形成溶质原子的富集区. 相应地, 复合薄膜的硬度在含1.8 at.%(Ti, N) 时就可迅速提高到3.9 GPa; 随着TiN含量的增加, 薄膜的硬度进一步提高到含17.1 at.%(Ti, N)时的8.8 GPa. 以上结果显示出Ti和N"双超过饱和固溶"对Al薄膜极其显著的强化效果.     

基于主元分析与动态时间弯曲的故障诊断方法及应用研究

轴承是工程实际中常用而又极易损坏的部件,特别是对其早期微弱响应的辨识,具有重要的社会价值和意义。为提高运转轴承的安全可靠性和可维护性,提出了基于主元分析与动态时间弯曲距离的故障诊断方法,它可以准确对早期微弱动态响应辨识、诊断。该方法首先将典型故障样本信号与待测信号小波去噪并EMD分解,并对若干固有模态分量主元分析求取主元,然后对主元分量进行分析,获得相关特征值组成特征向量,计算待测信号与已知故障样本信号特征向量的弯曲距离,弯曲距离越小表明两信号越相似,从而辨识故障。此外,还可将其应用于转子、碰磨、齿轮故障诊断中,工程应用实例表明该方法可以准确故障分类,高效故障诊断。     

氢化物发生-催化共振瑞利散射光谱法测定痕量砷

在硫酸介质中,以硼氢化钠(NaBH₄)为还原剂,可将As(Ⅲ)还原为砷化氢(AsH₃)气体使其逸出,用Ce(SO₄)₂-H₂SO₄-KI混合液做吸收液,在催化剂KI存在下四价铈与AsH₃气体反应生成具有共振瑞利散射(RRS)的砷微粒和具有荧光的三价铈,导致体系在370 nm处的RRS信号和在351 nm处的荧光强度增大。在选定条件下,As(Ⅲ)浓度分别在0.006～0.76 mg·L-1和0.006～0.28 mg·L-1范围内与RRS增加值ΔI和荧光强度增大值ΔF₃₅₁呈线性关系,检出限均为3.0 μg·L-1。据此可建立新的检测As(Ⅲ)的催化RRS和荧光光谱法。     

微沟槽结构注塑成形的充型过程计算方法

微注塑成形制造方法适合于热塑性材料微小型器件大批量加工,对微注塑关键步骤——充型进行分析计算,有助于微注塑工艺参数和模具结构优化。目前研究表明,微尺度聚合物熔体流动与常规流动存在显著差异,采用常规尺度流动计算分析工具会带来较大偏差。本文以开源计算代码OpenFOAM为基础,综合由实验获得的熔体表面特性规律和粘度变化规律等,采用面向对象编程方法构建了熔体填充微结构型腔流动过程的计算模块,以微流体器件中的典型微结构——微沟槽注塑充型过程为例进行数值模拟,分析了表面力和粘度作用对其注塑充型填充率的影响。     

Interactions Between Solitons and Cnoidal Periodic Waves of the(2+1)-Dimensional Konopelchenko–Dubrovsky Equation

The(2+1)-dimensional Konopelchenko–Dubrovsky equation is an important prototypic model in nonlinear physics, which can be applied to many fields. Various nonlinear excitations of the(2+1)-dimensional Konopelchenko–Dubrovsky equation have been found by many methods. However, it is very difficult to find interaction solutions among different types of nonlinear excitations. In this paper, with the help of the Riccati equation, the(2+1)-dimensional Konopelchenko–Dubrovsky equation is solved by the consistent Riccati expansion(CRE). Furthermore, we obtain the soliton-cnoidal wave interaction solution of the(2+1)-dimensional Konopelchenko–Dubrovsky equation.     

Finite symmetry transformation group and localized structures of the (2+1)-dimensional coupled Burgers equation

In this paper, the finite symmetry transformation group of the (2+1)-dimensional coupled Burgers equation is studied by the modified direct method, and with the help of the truncated Painleve′ expansion approach, some special localized structures for the (2+1)-dimensional coupled Burgers equation are obtained, in particular, the dromion-like and solitoff-like structures.     

Interactions Between Solitons and Cnoidal Periodic Waves of the Boussinesq Equation

The Boussinesq equation is one of important prototypic models in nonlinear physics.Various nonlinear excitations of the Boussinesq equation have been found by many methods.However,it is very difcult to find interaction solutions among diferent types of nonlinear excitations.In this peper,two equivalent very simple methods,the truncated Painlev′e analysis and the generalized tanh function expansion approaches,are developed to find interaction solutions between solitons and any other types of Boussinesq waves.