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Extraction and Crystal Structure of β-Sitosterol 总被引:1,自引:0,他引:1
The title compound β-sitosterol(C29H50O), an active phytosterol in many medicinal and edible plants, was characterized by X-ray diffraction analysis and extensive nuclear magnetic resonance(NMR) data. It crystallizes in monoclinic system, space group P21 with C29H50O·1/2H2O, a = 9.4226(7), b = 7.4824(9), c = 36.889(3) , V = 2597.0(4) 3, Z = 4, Dx = 1.084 g/cm3, Mr = 423.70, F(000) = 948, and μ = 0.064 mm-1. The final R = 0.0886 and wR = 0.2234 for 10157 observed reflections(I 2σ(I)). The molecular crystal structure of β-sitosterol shows relative stereochemistry of 24R-ethylcholest-5-en-3β-ol. The molecule is composed of one steroid nucleus(3 six-membered rings and 1 five-membered ring) and one sidechain of 10 carbons. There are two C29H50O molecules and one H2O molecule in a symmetrical unit, and the title compound is stacked into a special laminated structure through hydrogen bonds and van der Waal forces. The special laminated structure was first reported. 相似文献
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摘要:随着无人机民用化的持续加速, 其应用场景越来越复杂, 自主避障技术成为拓宽应用领域的技术瓶颈. 自主避障技术的突破, 无疑成为无人机更大规模应用必要条件. 自抗扰控制器技术, 是发扬PID控制技术的精髓并吸取现代控制理论思想归纳探索而来. 自抗扰控制器具有的不依赖被控对象精确模型、算法简单、参数易于调节的特点, 使其适合作为无人机自主避障的控制算法来应用. 针对无人机避障中位置给定阶跃信号幅值较大且幅值不定的情况, 传统PID控制器快速性不能很好满足要求且需要重复调节参数, 而自抗扰控制器则具有更好的鲁棒性. 为了更好的实现无人机自主避障, 设计了基于自抗扰控制器的外环位置控制器, 对基于自抗扰的无人机自主避障系统进行仿真和实验研究, 并与传统双环PID控制器进行对比分析, 结果证明外环控制器采用自抗扰控制器的无人机自主避障系统的可行性. 相似文献
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