锂离子筛前驱体正尖晶石结构LiMn_2O_4的合成及其特性研究

以 L i2 CO3 和 Mn O2 (EMD)为原料 ,用固相反应法合成了 λ- Mn O2 锂离子筛前驱体正尖晶石结构的L i Mn2 O4;通过 TG- DTA、XRD和 SEM分析 ,确定了最佳制备条件 :合成温度为 85 0°C,L i/ Mn的摩尔比为 0 .5 ,保温时间为 2 4h;设计和制作了流态化的离子交换装置 ,用 0 .2 0 mol· L- 1和 0 .5 0 mol· L- 1的盐酸分别对 L i Mn2 O4进行了动态酸浸析 ,并得到了高纯度的 λ- Mn O2 ,同时采用原子吸收光谱 (AAS)测定了交换液中锂的浸出和锰的溶损情况 .     

Experimental study on minimum resolvable velocity for heterodyne laser Doppler vibrometry

A high spatial resolution,high velocity resolution all-fiber laser Doppler vibrometry(LDV) based on heterodyne detection for vibration measurements is reported.A linewidth of 1-kHz single-mode continuous fiber laser,polarization-preserving fiber,and a telescope with 30-mm aperture are used in this LDV.With the inphase-quadrature circuit and the digital differentiating discriminator,a high velocity resolution of 96.9 nm/s and a high displacement resolution of 2.5 pm are obtained simultaneously with a glass a...     

基于双声光移频器的外差式激光多普勒测振计

分析了单声光移频器构成的外差式激光多普勒测振计中声光移频器驱动信号的频率稳定性和信号功率对待测振动信号的影响.为了降低声光移频器驱动信号频率漂移的影响,提出双声光移频器构成的外差式激光多普勒测振计,并基于直接数字频率合成技术,以相位噪音低、初始相位可控的芯片AD9912为核心器件,完成了声光移频器驱动信号生成及处理模块的设计.开展了双声光移频器组成的外差式激光多普勒测振计的振动测量实验,结果表明,驱动信号生成装置可以驱动声光移频器正常工作,且测振计的本底噪音在0～10kHz频带范围内呈现平坦分布,0～1kHz频段内噪音得到明显抑制,较单声光移频器构成的外差式激光多普勒测振计有显著改善.     

锂离子筛前驱体正尖晶石结构LiMn2O4的合成及其特性研究

以Li2CO3和MnO2(EMD)为原料,用固相反应法合成了λ-MnO2锂离子筛前驱体正尖晶石结构的LiMn2O4;通过TG-DTA、XRD和SEM分析,确定了最佳制备条件合成温度为850℃,Li/Mn的摩尔比为0.5,保温时间为24 h;设计和制作了流态化的离子交换装置,用0.20 mol·L-1和0.50 mol·L-1的盐酸分别对LiMn2O4进行了动态酸浸析,并得到了高纯度的λ-MnO2,同时采用原子吸收光谱(AAS)测定了交换液中锂的浸出和锰的溶损情况.     

基于双声光移频器的外差式激光多普勒测振计

分析了单声光移频器构成的外差式激光多普勒测振计中声光移频器驱动信号的频率稳定性和信号功率对待测振动信号的影响.为了降低声光移频器驱动信号频率漂移的影响,提出双声光移频器构成的外差式激光多普勒测振计,并基于直接数字频率合成技术,以相位噪音低、初始相位可控的芯片AD9912为核心器件,完成了声光移频器驱动信号生成及处理模块的设计.开展了双声光移频器组成的外差式激光多普勒测振计的振动测量实验,结果表明,驱动信号生成装置可以驱动声光移频器正常工作,且测振计的本底噪音在0~10kHz频带范围内呈现平坦分布,0~1kHz频段内噪音得到明显抑制,较单声光移频器构成的外差式激光多普勒测振计有显著改善.     

Development of an all-fiber heterodyne lidar for range and velocity measurements

A 1550-nm all-fiber monostatic lidar system based on linear chirp amplitude modulation and heterodyne detection for the measurements of range and velocity is presented. The signal processing method is given, after which the relationship between the peak frequency values in the final signal spectrum, the target＇s range, and the line-of-sight velocity is obtained in the presence of the fiber end-face-reflected signal plaguing many monostatic lidar systems. The range of an electric fan as well as the line-of-sight fan speed of different levels is tested. This proposed system has a potential application for the space-borne landing system.     

用于铝板缺陷无损检测的激光超声有限元模拟研究

激光超声技术能够在材料表面形成超声波，是实现材料缺陷无损检测的重要环节。借助Abaqus有限元分析工具，基于激光超声热弹机制建立了轴对称铝板的表面缺陷模型，模拟了激光激发产生的表面波在材料中的传播特性及其与铝板缺陷的相互作用过程。数值模拟实验表明，铝板表面缺陷的分布深度值越大，反射波越强，并且当缺陷深度达到一定程度时，反射波的幅值趋于稳定；但缺陷的分布宽度对于反射波的影响则十分有限。所得结论为基于激光超声的材料缺陷的定量检测及识别提供有效的理论依据。     

Laser Doppler vibrometer for real-time speech-signal acquirement

Laser Doppler vibrometer （LDV） has a potential application prospect in remote sensing. Based on the correlation theories of heterodyne detection, a LDV system with a configuration of all fiber and heterodyne techniques is developed to detect the sound signal through the vibration of glass. Experimental results show that the LDV system has an ability to acquire the real-time speech signal 25 m away through glass. While, the system signal-to-noise ratio （SNR） value decreases with the increase of the glass thickness and the detection distance.