排序方式: 共有5条查询结果,搜索用时 15 毫秒
1
1.
建立了固相萃取结合气相色谱串联质谱联用仪检测土壤中15种邻苯二甲酸酯残留的方法。样品采用丙酮和石油醚超声提取,取上清液浓缩,上弗罗里硅土固相萃取柱净化,收集洗脱液,定容,以气相色谱串联质谱法分析。该方法在20~2 000 ng/g范围内线性关系良好(r~20.999 0),检出限(S/N=3)为0.12~0.61 ng/g。20,50,200 ng/g 3个添加浓度的15种邻苯二甲酸酯的加标回收率在78.9%~101.8%之间,测定结果的相对标准偏差为0.19%~8.34%(n=5)。该方法准确、灵敏,符合痕量分析的要求,适用于土壤中邻苯二甲酸酯类残留的分析。 相似文献
2.
基于线性调频变换算法的SAW富氏谱分析技术是现代雷达、通讯、电子对抗及射电天文等领域的新一代支持技术之一。其中测频是其最基本功能。由于所用SAW色散延迟线基底材料延时温度系数的影响,所测频率通常随工作温度变化。故实用中正确认识测频随温度变化规律,是系统正确设计与补偿的前提。迄今据作者所知尚无令人满意的定量分析理论。本文由时间比例关系出发,定量分析了此类技术中基础结构的M-C型功率谱仪测频温度特性。给出相对不同频率分量的延时随温度变化的解析表达式。指出这种变化不仅与器件参数及基片延时温度系数有关,且与工作频率有关。应用本文结果还可合理地解释法国Thomson CSF公司的Claude Lardat有关实验中理论与实验的偏差。 相似文献
3.
4.
5.
A new ultrasonic cylindrical linear phased array (CLPA) transducer is designed and fabricated for the borehole wall imaging in petroleum logging based on the previous theoretical researches. First, the CLPA transducer, which is made up of numbers of the piezoelectric elements distributed on the surface of a cylinder uniformly, is designed and fabricated. By transmitting and receiving acoustic waves with 16 active elements and using different groups of the elements under the control of the electric system, the CLPA can scan all areas of the borehole wall dynamically and rapidly without a traditional mechanism around the borehole axis. Then, the theoretical and experimental investigations are conducted in detail for the borehole wall scanning and imaging by the steel pipe and casing borehole with defects distributed in different shapes and directions. It is shown by experiments that the CLPA transducer has good focusing characteristic and good resolution for the borehole wall imaging in acoustic logging. 相似文献
1