双相高强钢FeNiAlC的动态剪切行为及微结构机理

绝热剪切带是金属材料在高应变率载荷下常见的一种失效模式。利用霍普金森压杆装置,对双相钢Fe-24.86Ni-5.8Al-0.38C不同微结构的帽形样品施加冲击载荷,研究它的动态剪切变形行为及微结构机理。先通过对固熔处理得到的粗晶态样品进行大应变冷轧获得冷轧态样品,再使用透射电子显微镜和扫描电子显微镜表征两种样品冲击前后微结构的变化差异。结果表明,双相钢FeNiAlC拥有较优异的动态剪切性能,剪切强度达1.3 GPa,均匀剪切应变达1.5。变形前,材料由奥氏体相和马氏体相构成,马氏体体积分数约为20%。变形过程由位错滑移和孪生变形主导,但因应变速率较高致使马氏体相变被抑制。不同微结构样品内均形成绝热剪切带,带内发生动态再结晶,形成超细晶粒,平均晶粒尺寸约300 nm,且剪切带内不发生相变;冷轧态剪切带宽度的实验值（14.6 μm）与理论计算值(12.3 μm)较好吻合,而粗晶态剪切带宽度的实验值（14.6 μm）与理论计算值（30 μm）相差甚远,初步分析可能是因为粗晶态样品应变较大基本不满足完全绝热的理论条件。在变形过程中,粗晶态因塑性变形做功产生的绝热温升高达720 K,而冷轧态的只有190 K。通过实验结果与热塑模型分析,得出绝热温升不是形成绝热剪切带的唯一因素,而应考虑材料的微观结构和局部化变形等的共同影响。     

微压痕尺度效应的理论和实验

对压入深度为亚微米量级的微压痕实验来说,硬度与压入深度的关系将表现出强烈的尺度效应,然而,由传统的弹塑性理论无法预测.采用塑性应变梯度理论对微压痕实验中的尺度效应进行预测;同时对单晶铜和单晶铝进行微压痕实验研究.通过将理论预测结果应用于实验,获得塑性应变梯度理论中的微尺度参量值,该值对于常规金属材料（如铜、铝、银等）来说,取值范围为0.8～1.5　μm.另外,对微压痕边界附近所出现的挤出现象（pile-up）和沉陷现象（sink-in）进行了预测和详细分析.     

金属管线高温环境下的断裂失效分析

超燃冲压发动机燃烧室试验台配置了大量金属管线,煤油作为燃料和冷却介质在其中输运,在实验过程中发生管线早期断裂失效,对此开展了分析。首先利用三维体视显微镜与扫描电镜进行了断口观察与分析,表明管线的开裂起源于焊缝根部,具有典型的多源起源特征;裂纹源区具有蓝色半圆形特征,表明存在焊接裂纹。同时,断口呈现明显的疲劳辉纹,间距为亚微米量级。根据辉纹间距与管材壁厚以及使用寿命分析,确定了疲劳载荷的频率范围;根据理论公式与有限元模态分析对管线的自振频率进行了估算,其结果与断口分析的结果吻合良好。以上研究结果表明管线断裂是典型的振动疲劳失效导致的。为此,建议在管线中部增加固定点约束,改变管线的自振频率以降低振幅,并改进焊接工艺,提高管线焊接质量。基于以上措施,有效解决了管线的早期断裂失效问题。     

Theoretical and experimental researches of size effect in micro-indentation test

Micro-indentation tests at scales on the order of sub-micron have shown that the measured hardness increases strongly with the indent depth or indent size decreasing, which is frequently referred to as the size effect. However, the trend is at odds with the size-independence implied by conventional elastic-plastic theory. In this paper, strain gradient plasticity theory is used to model the size effect for materials undergoing the micro-indenting. Meanwhile, the micro-indentation experiments for single crystal copper and single crystal aluminum are carried out. By the comparison of the theoretical predictions with experimental measurements, the micro-scale parameter of strain gradient plasticity theory is predicted, which is fallen into the region of 0.8–1.5 micron for the conventional metals such as copper (Cu), aluminum (Al) and silver (Ag). Moreover, the phenomena of the pile-up and sink-in near micro-indent boundary are investigated and analyzed in detail.     

微纳米晶金属的应变率敏感性及应变硬化行为分析

基于亚微米、纳米晶粒组织塑性变形过程中多种变形机制(位错机制、扩散机制及晶界滑动机制)共存,建立了理论模型,用于定量研究亚微米、纳米晶粒组织的塑性变形行为.以铜为模型材料,计算分析了晶粒尺度、应变率以及温度对亚微米、纳米晶粒组织塑性变形行为的影响.结果表明:相比粗晶铜,亚微米晶铜表现出明显的应变率敏感性,并且应变率敏感系数随晶粒尺度及变形速率的减小而增大;同时,增大变形速率或降低变形温度都能提高材料的应变硬化能力,延缓颈缩发生,进而提高材料的延性.计算分析结果与实验报道吻合.     

Step Structure in Cold-Rolled Deformed Nanocrystalline Nickel

The microstructure characteristic of the cold-rolled deformed nanocrystalline nickel metal is studied by transmission electron microscopy. The results show that there are step structures nearby the grain boundary （CB）, and the contrast of stress field in front of the step corresponds to the step in the shape. It is indicated that the interaction between twins and dislocations is not a necessary condition to realizing the deformation. In the later stage of the deformation when the grain size becomes about lOOnm, the deformation can depend upon the moving of the boundary of the stack faults （SFs） which result from the partial dislocations emitted from CBs. However, when the size of SFs grows up, the local internal stress which is in front of the step gradually becomes higher. When this stress reaches a critical value which stops the gliding of the partial dislocations, the SFs will stop to grow up and leave a step structure behind.     

Curie Transition of NC Nickel by Mechanical Spectroscopy and Magnetization Study

Mechanical spectroscopy measurement is performed to study the internal friction of nanocrystalline （NC） nickel with an average grain size of 23 nm from room temperature to 610 K. An internal friction peak is observed at about 550 K, which corresponds to the Curie transition process of the NC nickel according to the result of magnetization test. Moreover, the fact that the explained by an analytical model Curie temperature of NC nickel is based on the weakening of cohesive lower than that of coarse-grained nickel is energy.