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Cellulose - Polyacrylonitrile (PAN)-based carbon precursor is a well-established and researched material for electrodes in energy storage applications due to its good physical properties and... 相似文献
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Esra Imamoglu Meltem Conk Dalay Fazilet Vardar Sukan 《Applied biochemistry and biotechnology》2013,171(8):2065-2074
Agricultural by-products are becoming an attractive substrate for bioethanol production. The aim of this study was to evaluate the effects of regional differences in the rice hulls using Escherichia coli KO11 for bioethanol production. The rice hulls coded Edirne were obtained from Thrace Region, and the rice hulls coded Izmir were obtained from Aegean Region in Turkey. Rice hulls were treated by dilute acid before using them as substrates. The cells were incubated on an orbital shaker at 160 rpm under 30 °C during 96 h of the fermentation period. It was found that the maximum yield of ethanol from sugar (0.44 g ethanol/g reducing sugar) was obtained with the substrate C/N ratio of 29.16 in Izmir medium. The main difference was the dominant carbon source available as a substrate. It was detected that glucose concentration was about 2.5 times higher in Izmir medium, whereas xylose concentration was about two times higher in Edirne medium. The different results obtained with rice hulls from different origins could depend on the type of paddy as well as different cultivation conditions. These findings provide a valuable indicator for identifying suitable agricultural waste materials to be used as substrates for bioethanol production. 相似文献
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Ömer Kesmez Nadir Kiraz Esin Burunkaya H. Erdem Çamurlu Meltem Asiltürk Ertuğrul Arpaç 《Journal of Sol-Gel Science and Technology》2010,56(2):167-176
SiO2 sols were prepared by hydrolysis and condensation reactions of tetraethyl orthosilicate through a one step acid or a two
step acid + base catalysis process, in the presence of nitric acid and four different base catalyzers, namely trimethylamine,
triethylamine, tripropylamine and tributylamine. Hydrolysis of TEOS was followed by FT-IR analyses. Particle size distributions
of the sols were evaluated after predetermined durations in 1–22 days. Particle growth was seen to be faster in amine catalyzed
systems than in one step acid catalyzed system. The highest rate of growth was in triethylamine catalyzed system. Glass substrates
were dip coated with the prepared SiO2 sols. Effect of sol aging duration on film thickness and on light transmittance properties of the films was investigated
with respect to type of base catalyst. Thicknesses of the films which were measured to be in the range of 100–400 nm, were
seen to increase with aging duration of the sols. Triethylamine catalyzed system presented the highest film thickness. Films
obtained from one step acid catalyzed system presented an increase of 4.8%; whereas acid + base catalyzed films provided an
increase in the light transmittance of 5.7% in the first 4 days of aging. Surfaces of films were examined by FESEM and AFM.
The antireflective character of the films was verified by diffuse reflectance analyses. 相似文献
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Meltem Öztürk 《Annals of Operations Research》2008,163(1):177-196
Semiorders may form the simplest class of ordered sets with a not necessarily transitive indifference relation. Their generalization
has given birth to many other classes of ordered sets, each of them characterized by an interval representation, by the properties
of its relations or by forbidden configurations. In this paper, we are interested in preference structures having an interval
representation. For this purpose, we propose a general framework which makes use of n-point intervals and allows a systematic analysis of such structures. The case of 3-point intervals shows us that our framework
generalizes the classification of Fishburn by defining new structures. Especially we define three classes of ordered sets
having a non-transitive indifference relation. A simple generalization of these structures provides three ordered sets that
we call “d-weak orders”, “d-interval orders” and “triangle orders”. We prove that these structures have an interval representation. We also establish
some links between the relational and the forbidden mode by generalizing the definition of a Ferrers relation. 相似文献
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We consider a lot sizing problem with setup times where the objective is to minimize the total inventory carrying cost only. The demand is dynamic over time and there is a single resource of limited capacity. We show that the approaches implemented in the literature for more general versions of the problem do not perform well in this case. We examine the Lagrangean relaxation (LR) of demand constraints in a strong reformulation of the problem. We then design a primal heuristic to generate upper bounds and combine it with the LR problem within a subgradient optimization procedure. We also develop a simple branch and bound heuristic to solve the problem. Computational results on test problems taken from the literature show that our relaxation procedure produces consistently better solutions than the previously developed heuristics in the literature. 相似文献
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Highly Luminescent Cesium Lead Halide Perovskite Nanocrystals with Tunable Composition and Thickness by Ultrasonication 下载免费PDF全文
Yu Tong Eva Bladt Meltem F. Aygüler Aurora Manzi Dr. Karolina Z. Milowska Verena A. Hintermayr Prof. Dr. Pablo Docampo Prof. Dr. Sara Bals Dr. Alexander S. Urban Dr. Lakshminarayana Polavarapu Prof. Dr. Jochen Feldmann 《Angewandte Chemie (International ed. in English)》2016,55(44):13887-13892
We describe the simple, scalable, single‐step, and polar‐solvent‐free synthesis of high‐quality colloidal CsPbX3 (X=Cl, Br, and I) perovskite nanocrystals (NCs) with tunable halide ion composition and thickness by direct ultrasonication of the corresponding precursor solutions in the presence of organic capping molecules. High angle annular dark field scanning transmission electron microscopy (HAADF‐STEM) revealed the cubic crystal structure and surface termination of the NCs with atomic resolution. The NCs exhibit high photoluminescence quantum yields, narrow emission line widths, and considerable air stability. Furthermore, we investigated the quantum size effects in CsPbBr3 and CsPbI3 nanoplatelets by tuning their thickness down to only three to six monolayers. The high quality of the prepared NCs (CsPbBr3) was confirmed by amplified spontaneous emission with low thresholds. The versatility of this synthesis approach was demonstrated by synthesizing different perovskite NCs. 相似文献
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Paweł Berczyński Aleksandra Kładna Irena Kruk Teresa Piechowska Hassan Y. Aboul-Enein Oya Bozdağ-Dündar Meltem Ceylan-Unlusoy 《Journal of fluorescence》2013,23(6):1319-1327
The antioxidant properties of 11 new synthesized chromonyl-2,4-thiazolidinediones and chromonyl-2,4-imidazolidinediones (CBs) were investigated. The antioxidant activities and mechanisms of the CBs interaction with reactive oxygen species (ROS) were clarified using various in vitro antioxidant assay methods including superoxide anion radical ( $ \mathrm{O}\overline{{}_2^{\bullet }} $ ), hydroxyl radical (HO?), 1,1-diphenyl-2-picryl-hydrazyl free radical (DPPH?) scavenging activity and the iron (II)-ferrozine complex formation. The potassium superoxide/18-crown-6 ether dissolved in dimethylsulfoxide (DMSO) was applied as a source of superoxide anion radical. Hydroxyl radicals were produced in the Fenton-like reaction Fe(II)+H2O2. Chemiluminescence, spectrophotometry, and electron paramagnetic resonance (EPR) spectroscopy using 5,5-dimethyl-1-pyrroline-1-oxide (DMPO) as spin trap were applied as the measurement techniques. The CBs examined that exhibited good free radical scavenging activity also showed strong total antioxidant power capacity. Possible mechanisms of antioxidation are proposed to explain the differences in the experimental results between the chromone derivatives with imidazolidine-2,4-dione ring and those with thiazolidine-2,4-dione ring. In conclusion, some of the new CBs are promising to be applied as inhibitors of free radicals. 相似文献
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In this article, we study the C4- and D4-modules in terms of perspective direct summands, providing new characterizations and results. Endomorphism rings of C4-modules and extensions of right C4-rings are also investigated. Decompositions of C4-modules with restricted ACC on direct summands and D4-modules with restricted DCC on direct summands are obtained. 相似文献