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A novel method for the preparation of thioesters starting from Iso-Fujisawa disulfides is reported. The presence of an acylamino group cis to the disulfide function on the β-lactam nucleus seems to be an essential requirement for this reaction. In the absence of such a cis-acylamino group, desulfurization, is the preferred course. 相似文献
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The game of molecular engineering of liquid crystalline systems via a combination of molecular architecture and functionalization of mesogens has opened interesting perspectives in the field of liquid crystals. Here we report on the synthesis and characterization of star-like heptameric triphenylenes. The discotic subunits in these molecules have been arranged in a hexagonal fashion around a central discotic core, thus leading to a new type of molecular arrangement for discotic liquid crystals. These oligomers do not crystallize and combine a well-defined structure with a discotic polymer-like processing. 相似文献
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Zur Verbindungsbildung von MeO:M2O3. VI. Darstellung und Strukturaufklärung von Sr1,33 Pb0,67 Al6O11
Compound Formation MeO: M2O3. VI. Synthesis and Structure Determination of Sr1,33 Pb0,67 Al6O11 Single crystal of Sr1,33Pb0.67Al6O11 could be prepared with a PbO flux. (Space group D–Pnnm, a = 22.13, b = 4.88, c = 8.42 Å, Z = 4) Sr2+ and Pb2+ are statistically intercalated into a framework of AlO6 octahedra and AlO4 tetrahedra. The typical coordination of Sr2+ and Pb2+ is realized by occupying different positions in the same cavern. 相似文献
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