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M. Yamamoto Syarbaini K. Kofuji A. Tsumura K. Komura K. Ueno D. J. Assinder 《Journal of Radioanalytical and Nuclear Chemistry》1995,197(1):185-194
An analytical method has been developed for the determination of low-level99Tc in environmental samples by High Resolution ICP-MS. The method consists of leaching of99Tc by HNO3 and separation by three different solvent extractions with 30% TOA-xylene, MEK, and cyclohexanone. Finally, purification of99Tc was made by using an anion exchange resin column to reduce dissolved solids content. The final solution was adjusted to 1M HNO3 for introducing into the HR-ICP-MS. The accuracy and precision of the method was confirmed to be satisfactory by applying this technique to the determination of99Tc in IAEA marine algae sample (AG-B-1). Measurements of99Tc using 0.5–2.5 g of sediment samples from the Irish Sea, UK, were successfully performed by the present method. 相似文献
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Zhenyu Luo Chunxiao Zou Saad Syed Luthfia A. Syarbaini Guofang Chen 《Colloid and polymer science》2012,290(2):141-150
Chemically reactive particles with controllable sizes from 383 to 756 nm in very narrow size distributions (well below 5%)
have been synthesized by the modified surfactant-free emulsion homopolymerization of inhibitor-free glycidyl methacrylate
with the dropwise addition of ionic initiators during the initial reaction of 10 min. The effects of monomer concentration
and the amount of initiator were systematically studied on the particle diameter. In addition, changes of the particle diameter
and its size distribution during the whole synthesis process were also investigated. The mechanism for the formation of coalesced
and highly monodisperse chemically reactive colloidal particles was discussed based on the colloidal stability governed by
chemical reaction and physical interactions between the precursor or primary particles. Colloidal photonic crystals with different
brilliant visible colors in a large scale were prepared by shearing assembly of such chemically reactive monodisperse particles
with spin coating technique. The reflection wavelengths in the visible spectrum range are from the high-order including the
second-order light diffraction of the as-prepared PGMA photonic crystals. Such monodisperse chemically reactive particles
will be very useful in optical and sensing technologies, and in biochemical analysis. 相似文献
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