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N. G. Zabirov F. D. Sokolov V. V. Brus'ko R. A. Cherkasov 《Phosphorus, sulfur, and silicon and the related elements》2013,188(1)
Abstract The analysis of all known synthesis methods of N-(thio)phosphorylthiómides of the common formula RC(S)NHP(X)R'2 (1), where R=Alk, Ar; R'=óIk, ór, SAIk, SAr. Alk, Ar; X=O,S has been gave in this report. We worked out the simple and convenient syntheses methods of this class compounds. 相似文献
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Mikhailov Oleg V. Tatarintseva Tatyana B. Brus'ko Vasiliy V. Zabirov Nahil G. 《Transition Metal Chemistry》2002,27(4):423-428
Complexing processes in MII-N-diisopropoxythiophosphorylthiobenzamide binary systems (M = Co, Ni, Cu) in metal(II) hexacyanoferrate(II) gelatin-immobilized matrices upon contact with aqueous–alkaline (pH = 12.0 ± 0.1) solutions of organic compounds have been studied. It has been shown that, in CoII and CuII, the initial act of complexing involves destruction of the CoII and CuII hexacyanoferrates(II) by OH– ions, leading to formation of the corresponding hydroxides which react with the ligand indicated. In the both systems, successive addition of two ligand molecules per M(OH)2 fragment occurs and [MB(OH)(OH2)] and [MB2] coordination compounds are formed (B–-a singly deprotonated ligand form). In the NiII-N-diisopropoxythiophosphorylthiobenzamide system, the formation of three complexes, (Ni2BOH)2[Fe(CN)6], [NiB(OH)(OH2)] and [NiB2] occurs. 相似文献
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Shaidarova L. G. Gedmina A. V. Brus'ko V. V. Zabirov N. G. Ulakhovich N. A. Budnikov G. K. 《Russian Journal of Applied Chemistry》2002,75(6):919-925
A method is proposed for determining Ni2
+, Co2
+, Cu2
+, Cd2
+, and Pb2
+ ions by inversion voltammetry on carbon-paste electrodes modified with N-diisopropoxythiophosphoryl-N'-phenyl thiourea and its derivatives: N,N'-bis-(diisopropoxythiophosphorylamidothiocarbonyl)-1,5-diamino-3-oxapentane, N,N'-bis- (diisopropoxythiophosphorylamidothiocarbonyl)-1,8-diamino-3,6-dioxaoctane and N,N'-bis-(diisopropoxythio- phosphorylaminothiocarbonyl)-1,10-diaza-18-crown-6. 相似文献
4.
V. V. Ovchinnikov V. V. Brus'ko L. I. Lapteva M. G. Kireev 《Phosphorus, sulfur, and silicon and the related elements》2013,188(9):2035-2038
The heat capacities of 2,4-dimethyl-2-oxo-(I)-, 2,5,5-trimethyl-2-oxo(II)-1,3,2-dioxaphosphorinanes, methylphosphonic acid (III), O,O-dimethyl(IV)-, O,O-diethyl(V)-, O,O-di-isopropyl(VI)esters of dithiophosphorus acid, 4,5-dimethyl-2-thiono-2-mercapto-1,3,2-dioxaphospholane(VII), and 4-methyl-2-thiono-2-mercapto-1,3,2-dioxaphosphorinane(VIII) were determined using the scanning calorimetry. 相似文献
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