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The ~(13)C-~1H long-range coupling constants of β-pyridine carboxylic ester are determined with the method of folding of two-dimensional NMR J spectroscopy and prove consistent with their simulated spectra. The modified computer program which can shorten the experimental time of heteronuclear two-dimensional J spectroscopy and improve the work is introduced. The experiment is performed on the Varian FT-80A NMR spectrometer. 相似文献
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本文介绍了对ROESY(CAMELSPIN)技术改进的脉冲序列的原理。这种改进的技术能有效的抑制偏共振效应的影响和提高谱的灵敏度。进行了1D和2D ROESY实验。实验结果表明,改进的ROESY实验能提高谱图灵敏度40%~80%,并能有效地压制其它2D响应信号。 相似文献
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