电感耦合等离子体原子发射光谱标准加入法测定铜精矿中锌、铅、砷、铜、铋、氧化镁

建立电感耦合等离子体原子发射光谱标准加入法测定铜精矿中Zn、Pb、As、Cu、Bi、MgO.分别对酸的加入种类和数量进行条件试验,采用盐酸–硝酸–盐酸–氢氟酸–高氯酸溶样,以标准加入法配制系列标准工作溶液,建立校正曲线,有效消除了样品基体对目标物检测结果的影响.目标物的分析谱线分别为Zn 206.2 nm,Pb 182.2 nm,As 197.2 nm,Cu 324.7 nm,Bi 190.2 nm,MgO 279.5 nm.各目标物校正曲线线性相关系数均不小于0.999,检出限为0.0002％～0.0006％,测定结果的相对标准偏差为0.62％～8.92％(n=6).按照该方法测定ZBK337、ZBK340铜精矿标准物质中Zn、Pb、As、Cu、Bi、MgO,测定值均在规定的标准值再现性限范围内.     

能量连续可调LCS光源SINAP-III

X/γ探测器在航天等国家战略需求领域具有非常广泛和重要的应用。 然而, X/γ探测器要在其有效能区进行精确的标定后才能发挥作用。 目前我国缺乏sub MeV～MeV能量连续可调、 单色性好的γ源, 而用于航天的X/γ探测器无法完成精确定标, 从而使航天探测的发展出现瓶颈问题。 提出了升级原有的激光康普顿散射(LCS)原理性实验装置的方案, 建立了一个通过改变激光入射角来连续调节散射光子能量、 准单色、 极化、 sub MeV～MeV LCS光源(SINAP-III), 从而开拓LCS光源在我国航天领域（如用于航天的X/γ探测器能量定标和抗辐射加固评估研究）的崭新应用前景, 并为将来建设一个基础和应用研究相结合的多功能的γ源实验平台打下基础。 The X/γ detectors in the field of national stratagem, such as astronautical technology, have very broad and important application. These detectors, however, will play their role properly only after accurate calibrations in effective energy region. For the shortage of continuously adjustable and quasi monochromatic γ source in China, it is impossible for the detector employed in aerospace to achieve an accurate calibration so that development of such detector has encountered a big obstacle (or a bottleneck). Therefore, we propose to upgrade the original LCS device to an adjustable photon energy by changing incident angle of laser beam, monochromatic, and polarized sub MeV~MeV LCS γ source(SIMAP III) , in order to explore the new applications of LCS γ source in aerospace as well as to establish a platform for a multifunctional of γ source.     

镍离子(Ⅱ)印迹聚合物的制备及性能研究

以镍(Ⅱ)离子为模板,丙烯酰胺为功能单体,二乙烯基苯为交联剂,偶氮二异丁腈为引发剂,甲醇为溶剂,采用本体聚合法制备了镍离子(Ⅱ)印迹聚合物.用红外光谱对镍离子印迹聚合物的结构进行表征,红外光谱研究表明聚合物中存在与模板分子相互作用的特征基团.通过研究Ni2+与单体的物质的量之比、单体与交联剂的物质的量之比、溶剂量对镍离...     

Measurement of PV asymmetry in n＋p→d＋γ and γ＋d→n＋p

The measurement of parity-violating （PV） observables in few-nucleon system can shed light on our current understanding of the weak interaction between nucleons.Theoretical models describe the nucleonnucleon weak interaction at low energies use a series of undetermined parameters.Two parity violating measurements have been considered： the capture of polarized slow neutrons on hydrogen （n ＋ p → d ＋ γ） at Los Alamos National Laboratory for first phase and Oka Ridge National Laboratory for second phase and the helicity dependence of the deuteron photodisintegration cross section using circularly polarized photons （γ ＋ d → n ＋ p） at Shanghai Institute of Applied Physics.The goal of both experiments is to constraint the weak meson-nucleon couplings to a precision of 1 ×10^-8 .The introduction of both experiments is presented.     

用光学极限的Glauber模型结合相对论平均场对8Li和8B的半径的研究

We study the reaction cross sections （σR） and root-mean-square （RMS） radii of ^8Li and ^8B, the halo-like nuclei, with stable target ^12C, ^27Al and ^9Be within the standard optical-limit Glauber model, using densities obtained from relativistic mean-field （RMF） formalisms and other types of distributions. It is found that the experimental σR can be reproduced well at high energy. The RMS radius and Ar extracted by RMF- theory and harmonic oscillator distribution are compared. larger than those of SLi. In addition, we analyze in detail the We find that the RMS radius and Ar of SB are relationship between σR and density distribution.     

Measurement of electric polarizabilities of light nucleus(nucleons)

The measurement of the electromagnetic polarizabilities have been given extensive attention, which is also a fresh field of the experimental nuclear physics. Now we will use the method - the light nucleus scattered by the heavy nucleus at energies below the Coulomb barrier to precisely and systematically measure the polarizabilities of the light nucleus. We hope we can solve the inconsistency among the results of the ³He polarizabilities and extract the ⁴He polarizabilities by our experiment. It is useful to mention that our experiment now is a supplement to the future experiment on SLEGS.     

Determination of the stellar reaction rate for 12C（α,γ）16O： using a new expression with the reaction mechanism

The astrophysical reaction rate of 12C(α, γ)16O plays a key role in massive star evolution. However, this reaction rate and its uncertainties have not been well determined yet, especially at T9=0.2. The existing results even disagree with each other to a certain extent. In this paper, the E1, E2 and total (E1+E2) 12C(α, γ)16O reaction rates are calculated in the temperature range from T9=0.3 to 2 according to all the available cross section data. A new analytic expression of the 12 C(α, γ)16 O reaction rate is brought forward based on the reaction mechanism. In this expression, each part embodies the underlying physics of the reaction. Unlike previous works, some physical parameters are chosen from experimental results directly, instead of all the parameters obtained from fitting. These parameters in the new expression, with their 3σ fit errors, are obtained from fit to our calculated reaction rate from T9=0.3 to 2. Using the fit results, the analytic expression of 12C(α, γ)16O reaction rate is extrapolated down to T9=0.05 based on the underlying physics. The 12C(α, γ)16 O reaction rate at T9=0.2 is (8.78 ± 1.52) × 1015 cm3s-1mol-1. Some comparisons and discussions about our new 12 C(α, γ)16 O reaction rate are presented, and the contributions of the reaction rate correspond to the different part of reaction mechanism are given. The agreements of the reaction rate below T9=2 between our results and previous works indicate that our results are reliable, and they could be included in the astrophysical reaction rate network. Furthermore, we believe our method to investigate the 12C(α, γ)16O reaction rate is reasonable, and this method can also be employed to study the reaction rate of other astrophysical reactions. Finally, a new constraint of the supernovae production factor of some isotopes are illustrated according to our 12C(α, γ)16O reaction rates.     

电感耦合等离子体原子发射光谱法同时测定石灰石中铁、铝、钙、镁、硅

采用碱熔法,以移液枪分取试样,用电感耦合等离子体原子发射光谱法同时分析石灰石中铁、铝、钙、镁、硅5种化学成分。在分析过程中对氩气加湿,避免盐析效应的影响,铁、铝、钙、镁、硅的分析谱线分别为259.940,396.152,315.887,279.553,251.611 nm。5种成分在各自的线性范围内均具有良好的线性,线性相关系数在0.990 74~0.999 99之间,方法检出限为0.000 6%~0.005 1%,回收率为95.6%~105.4%,测定结果的相对标准偏差小于1%(n=6)。该方法检出限低、重现性好,适合于石灰石样品中铁、铝、钙、镁、硅的快速检测。