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以轻质柔性的三聚氰胺泡沫(MF)作为基体,将其置于由乙二醇(EG)、硝酸银(AgNO3)、聚乙烯吡咯烷酮(PVP)和氯化铜(Cu Cl2)组成的反应溶液中,利用高温环境中发生的氧化还原反应在泡沫骨架上生成纳米银(Ag),随后通过真空浸渍法在泡沫基体中封装月桂酸(LA)制备相变复合材料.采用扫描电子显微镜(SEM)、X射线衍射仪(XRD)、差示扫描量热仪(DSC)和红外热成像仪等对制得的相变复合材料的形貌、结构和热性能进行研究.结果表明,当Ag NO3浓度为4 mg/m L时,纳米Ag均匀致密地沉积在MF骨架表面,且同时存在Ag纳米粒子(Ag NPs)和Ag纳米线(Ag NWs)两种形态.相变复合材料的相变焓高达144.0 J/g,相变焓效率超过了80%,呈现出优异的温度调节和储热能力.本文提供了一种制备综合性能优异的相变复合材料的新策略,有利于拓宽相变复合材料的应用领域. 相似文献
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Zi-Chao Gao 《中国物理 B》2022,31(12):128401-128401
Based on the principle of electron cyclotron maser (ECM), gyrotrons are among the most promising devices to generate powerful coherent terahertz (THz) radiation and play a vital role in numerous advanced THz applications. Unfortunately, THz ECM systems using a conventional high-Q cavity were theoretically and experimentally demonstrated to suffer from strong ohmic losses, and, accordingly, the wave output efficiency was significantly reduced. A scheme to alleviate such a challenging problem is systematically investigated in this paper. The traveling-wave operation concept is employed in a 1-THz third harmonic gyrotron oscillator, which strengthens electron-wave interaction efficiency and reduces the ohmic dissipation, simultaneously. A lossy belt is added in the interaction circuit to stably constitute the traveling-wave interaction, and a down-tapered magnetic field is employed to further amplify the forward-wave (FW) component. The results demonstrate that the proportion of ohmic losses is nearly halved, and output efficiency is nearly doubled, which is promising for further advancement of high-power continuous-wave operation of the ECM-based devices. 相似文献
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