Study on the laser treatment of electroless Ni-P-SiC composite coatings

Effect of the laser treatment on electroless Ni-P-SiC composite coatings was investigated. The microscopic structure, surface morphology, ingredient, and performance of the Ni-P-SiC composite coatings were synthetically analyzed by the use of X-ray diffraction apparatus, scanning electron microscope, energy distribution spectrometer, micro-hardness tester, wear tester and so on. It was found that the composite coatings did make crystalloblastic transformation after laser heating. Structural analysis confirmed that some new types of phase Ni2Si or Ni3Si compound would emerge in the Ni-P-SiC coatings after laser treatment. The micro-hardness measurement results showed that when the laser power was 450 W with scanning speed of 0.5 m/min, the hardness of the coating was superior to the coating obtained by the conventional furnace heating, and wear resistance of the composite coating after laser treating could also improve.     

激光淬火和冲击复合强化处理40Cr钢的耐磨性能研究

对激光淬火40Cr钢强化区域进行激光冲击复合强化处理，并分别同激光淬火和氮化处理40Cr钢对比考察了激光淬火和冲击复合强化处理40Cr钢的表面硬度和耐磨性．结果表明：经激光淬火和冲击复合强化处理的40Cr钢的硬度比激光淬火处理40Cr钢的硬度高11％；同氮化和激光淬火处理40Cr钢相比，复合强化处理40Cr钢的耐磨性分别提高了约4．3倍和1．6倍．     

Microstructure and properties of plastic deformed martensite induced by laser shock processing

Firstly, 45# steel was quenched by the NEL-2500A rapidly axial flow CO2 laser. The experimental parameters were the laser power of 750 W, the laser beam diameter of 4 mm, the scanning velocity of 7 mm/s.The thickness of coating layer was 0.1 mm and the width was 8 mm. Secondly, the martensite induced by laser quench was shocked by Nd:YAG laser. The parameters of laser shock processing were the wavelength of 1.06 μm, the pulse duration of 23 ns, and the output energy of 16-20 J. The laser was focused on a spot of φ7 mm. K9 optical glass was used as confinement. The sample was coated with black paint 86-1 (the thickness is about 0.025 mm). By testing and analysis of samples which were treated by laser quench and laser quench+shock with transmission electron microscope (TEM), it was discovered that the surface layer of martensite was deformed plastically by laser shock processing. In the secondary hardened zones,there were a lot of slender secondary twin crystal martensites, dislocation tangles, and cellular dislocations.Compared with that of the hardened zones through laser quench only, the residual stress and mechanical properties of the secondary hardened zones were improved and increased through laser compound method.     

Study of the substructure in nanometer copper thin films treated by laser shock processing

We study nanometer copper thin films prepared by magnetron sputtering and treated with laser shock processing (LSP). We observe the formation of firstborn twin crystals and some complete twin crystals in the copper thin films. After LSP, scanning electron microscope (SEM) images show obvious plastic deformation of the copper grain on the film surface, dramatically increased grain size, and the appearance of a large number of twin crystals. Moreover, the width of the crystals is a few dozen nanometers, and the cross angle is more than or close to 90°.Many vacancy defects appear during the sliding of atomic plane, which leads to a faulty structure; however, no obvious dislocation is observed. These substructures play a significant role in improving the mechanical performance of nanometer copper thin films.     

均匀与混合蛾眼结构减反射性能的模拟

采用时域有限差分法,对均匀蛾眼结构(UMS)和双混合蛾眼结构(BHMS)进行仿真,分析底面直径和高度对反射率的影响规律,比较了UMS与BHMS的减反射性能。基于反射率曲线和电场强度分布,分析了BHMS优异的减反射性能。结果表明:在300～1200 nm波段,UMS的反射率随着高度的增大而减小,随着底面直径的增大而先减小后增大;当底部直径为250 nm时,由不同高度的UMS组成的BHMS的平均反射率大于相应UMS的最小平均反射率;由不同底面直径UMS组成的BHMS的减反射性能可以进一步提升。     

Microstructure and properties of plastic deformed martensite induced by laser shock processing

Firstly, 45# steel was quenched by the NEL-2500A rapidly axial flow CO2 laser. The experimental parameters were the laser power of 750 W, the laser beam diameter of 4 mm, the scanning velocity of 7 mm/s. The thickness of coating layer was 0.1 mm and the width was 8 mm. Secondly, the martensite induced by laser quench was shocked by Nd:YAG laser. The parameters of laser shock processing were the wavelength of 1.06 μm, the pulse duration of 23 ns, and the output energy of 16-20 J. The laser was focused on a spot of φ7 mm. K9 optical glass was used as confinement. The sample was coated with black paint 86-1 (the thickness is about 0.025 mm). By testing and analysis of samples which were treated by laser quench and laser quench+shock with transmission electron microscope (TEM), it was discovered that the surface layer of martensite was deformed plastically by laser shock processing. In the secondary hardened zones, there were a lot of slender secondary twin crystal martensites, dislocation tangles, and cel