用双表面活性剂为共模板合成中孔分子筛MCM-48

利用水热法以非离子表面活性剂聚乙二醇辛基苯基醚和阳离子表面活性剂十六烷基三甲基溴化铵为共模板合成了中孔分子筛MCM-48.实验中发现利用较强的范德华力和氢键,聚乙二醇辛基苯基醚可在很大程度上降低合成MCM-48所需阳离子表面活性剂的用量,且利于制备有序性好、骨架聚合度高、稳定性好的MCM-48.通过调节聚乙二醇辛基苯基醚与十六烷基三甲基溴化铵的比例,可得到不同物相结构的分子筛.     

激光主动探测中回波信号的小波去噪方法

在分析激光主动探测中回波信号的噪声特性和小波变换去噪原理的基础上，提出了一种基于最大信噪比准则的小渡阈值去噪方法。首先用最大信噪比准则对小波变换系数进行阈值选取，然后采用软阂值方法对小波系数进行量化处理后再重构。仿真结果表明最大信噪比准则小波去噪方法改善信噪比效果十分显著，检测下限达到-16．2dB。证明了该方法在激光主动探测系统回波信号检测中的有效性。     

汽车稳定杆拟动态实验分析

本文主要通过汽车稳定杆在疲劳试验中应力、刚度拟动态试验，采用电测法^[1]，在分析杆件中实际应变和位移的基础上进行逆解分析，从而确定稳定杆的实际刚度，支座摩阻反力矩和应力集中系数，为建立稳定杆的简化力学分析及其疲劳寿命预测提供试验依据．     

Photoluminescence Characterization of Nanocrystalline ZnO Array

High-density and uniform well-aligned ZnO sub-micron rods are synthesized on the silicon substrate over a large area. The morphology and structure of the ZnO sub-micron rods are investigated by x-ray diffraction, transmission electron microscopy and Raman spectra. It is found that the ZnO sub-micron rods are of high crystal quality with the diameter in the range of 400-600 nm and the length of several micrometres long. The optical properties were studied by photoluminescence spectra. The results show that the intensity of the ultraviolet emission at 3.3eV is rather high, meanwhile the deep level transition centred at about 2.38eV is weak. The free exciton emission could a/so be observed at low temperature, which implies the high optical quality of the ZnO sub-micron rods.This growth technique provides one effective way to fabricate the high crystal quality ZnO nanowires array, which is very important for potential applications in the new-type optoelectronic nanodevices.     

Mid-IR Laser Generating Ultrasound in a Polyetheretherketone Polymer

We demonstrate laser ultrasonic generation in polyetheretherketone(PEEK). A middle infrared ZnGeP2 optical parametric oscillator(ZGP-OPO) pumped by a Q-switched Ho:YAG laser is employed as the ultrasonic excitation source. The ZGP-OPO has a spectral range of 3.2–3.4 μm. At an output wavelength of 3.4 μm, the maximum average output power of ZGP-OPO is 3.05 W with a pulse width of 24.3 ns, corresponding to a peak power of approximately 127.5 kW. The ultrasound is generated by the laser converted from 3.2 to 3.4 μm in the PEEK composite. The maximum ultrasonic signal amplitude in PEEK is 33 mV under the condition of thermoelastic excitation at 3.4 μm. Ablation occurs in the CPRF sample when the energy fluence is over 122.45 m J/cm~2. PEEK has a stronger absorption at 3.4 μm and laser-ultrasound generation is influenced by the wavelength of the laser.     

化学课件中的板书设计

板书设计是教学设计中必不可少的部分。教学过程中充分发挥多媒体授课的优势,运用先进的教学理念,制作符合教学设计的课件;通过使用软件中的动画设计功能、丰富的播放形式,体现教学中主板书和辅助板书的功效。     

回转体零件特征和GT编码自动转换系统的研制

文章主要介绍了作者研制的回转体零件特征和ＧＴ编码的自动转换系统的原理和实现方法。该系统具有良好的实用价值。     

混合表面活性剂与调节pH值法高效合成MCM-48

以正硅酸乙酯（TEOS）为硅源、十六烷基三甲基溴化铵（CTAB）与曲拉通X- 100(TX-100)热合成中孔MCM-48．在合成过程中通过调节溶液pH值可有效提高MCM- 48的收率和水热稳定性，同时采用剂使模板剂的利用效率达到了6.0TEPOS／1.0 Surf．并通过XRD、N_2-吸附／脱附和FT-IR等测试手段对产物进行了表征.     

支持向量学习并行区域增长结合活动轮廓模型的图像分割算法

为克服经典区域增长算法门限设置困难和图像分割精度不高的问题,提出了基于支持向量机学习的区域增长与活动轮廓模型结合的高精度图像分割算法。首先交互式选择属于目标区域的子块和背景区域的子块形成支持向量机的训练样本;并利用这些已知的训练样本训练支持向量分类器。在目标与背景的并行竞争增长过程中,利用训练好的支持向量分类器(SVC)进行分类判决,得到目标对象的初始轮廓。为提高分割对象的精度,采用活动轮廓模型获得准确的边缘。仿真实验获得了较好的分割效果,表明该提出的算法是合理可行的。