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Binary alloys of lead and tin were dissolved in nitric acid (1 + 1) containing 10% sodium fluoride. The tin(IV) was effectively masked by the fluoride. The lead was quickly and accurately titrated with EDTA in a hexamine-buffered solution, with Xylenol Orange as indicator. 相似文献
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In [2] E. Dobrowolski and K.S. Williams considered a problem of obtaining estimates for the sum
n=a+1
a+N
f(n),for a certain class of functions f. One specific application of their result is a new method for estimating character sums. In particular, they obtain a form of the Pólya-Vinogradov inequality with the constant 1/(2 log 2). In this note we improve their estimates and obtain, in particular, a form of the Pólya-Vinogradov inequality with the constant 1/(3 log 3). A nice feature of our estimate is that it is obtained by a very simple argument. 相似文献
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Sigmund EE Calder ES Thomas GW Mitrović VF Bachman HN Halperin WP Kuhns PL Reyes AP 《Journal of magnetic resonance (San Diego, Calif. : 1997)》2001,148(2):309-313
We have studied the temporal instability of a high field resistive Bitter magnet through nuclear magnetic resonance (NMR). This instability leads to transverse spin decoherence in repeated and accumulated NMR experiments as is normally performed during signal averaging. We demonstrate this effect via Hahn echo and Carr--Purcell--Meiboom--Gill (CPMG) transverse relaxation experiments in a 23-T resistive magnet. Quantitative analysis was found to be consistent with separate measurements of the magnetic field frequency fluctuation spectrum, as well as with independent NMR experiments performed in a magnetic field with a controlled instability. Finally, the CPMG sequence with short pulse delays is shown to be successful in recovering the intrinsic spin--spin relaxation even in the presence of magnetic field temporal instability. 相似文献
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Ambrose D Arroyo C Bachman M Connor D Eckhause M Graessle S Hancock AD Hartman K Hebert M Hoff CH Hoffmann GW Irwin GM Kane JR Kanematsu N Kuang Y Lang K Lee R Martin RD McDonough J Milder A Molzon WR Pommot-Maia M Riley PJ Ritchie JL Rubin PD Vassilakopoulos VI 《Physical review letters》2000,84(7):1389-1392
We report results from Experiment 871, performed at the BNL AGS, of a measurement of the branching ratio K(0)(L)-->&mgr;(+)&mgr;(-) with respect to the CP-violating mode K(0)(L)-->pi(+)pi(-). This experiment detected over 6200 candidate &mgr;(+)&mgr;(-) events, a factor of 6 more than that seen in all previous measurements combined. The resulting branching ratio gamma(K(0)(L)-->&mgr;(+)&mgr;(-))/gamma(K(0)(L)-->pi(+)pi(-)) = (3. 474+/-0.057)x10(-6) leads to a branching fraction B(K(0)(L)-->&mgr;(+)&mgr;(-)) = (7.18+/-0.17)x10(-9), which is consistent with the current world average, and reduces the uncertainty in this decay mode by a factor of 3. 相似文献
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P. Walter J. H. Brunn H. Schanz W. F. Bruce W. Bach K. Suzuki F. E. Raurich-Sas E. Busse P. Görlich A. H. Furnstal J. M. Voith G. B. Bachman und J. Hudig 《Fresenius' Journal of Analytical Chemistry》1936,107(5-6):201-205
Ohne Zusammenfassung 相似文献
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