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1.
Miller TJ Farquar HD Sheybani A Tallini CE Saurage AS Fronczek FR Hammer RP 《Organic letters》2002,4(6):877-880
[reaction: see text] The thiazole C-nucleoside analogue was synthesized by the Hantzsch cyclization method to form the thiazole ring and was then converted to the thiazole N-oxide C-nucleoside analogue by peracid oxidation of the heterocycle nitrogen. Incorporation of the thiazole and thiazole N-oxide phosphoramidites into DNA was successful though significant deoxygenation of the N-oxide occurred during DNA assembly. The mechanism proposed for the reduction of the thiazole N-oxide to thiazole involves the formation of an N-oxide phosphite ester. 相似文献
2.
We consider a remarkable class of rings, which we call corpids, that is the rings (K, +, ·), such that (K, ·) is an inverse semigroup (or groupid, which is the name used by Tallini (Ann Math 71:295–322, 1966). We prove several theorems concerning this structure, an order relation which allows us to formulate characterization theorems. We define the notion of simple idempotent and prove theorems about zero-divisors, idempotents, subcorpids, ideals and characteristic in a corpid. 相似文献
3.
The process of polarised deep inelastic scattering and the information it has given on the spin structure of the nucleon are introduced. The experimental programmes in this field are described and the latest inclusive and semi-inclusive data and analyses are reviewed. Proposed future measurements are summarised. 相似文献
4.
制备了甘氨酸-壳聚糖复合膜修饰玻碳电极(Gly-CTS/GCE),研究了抗坏血酸(AA)和尿酸(UA)在该修饰电极上的电化学行为。结果表明在pH=5.59的磷酸盐缓冲溶液中,AA、UA在Gly-CTS/GCE上均产生灵敏的不可逆氧化峰,其峰电流与浓度在一定范围内呈良好的线性关系。对AA和UA混合溶液平行测定7次,相对标准偏差分别为4.6%、2.9%,表明该电极重现性和稳定性良好。AA、UA在Gly-CTS/GCE电极上的氧化峰峰电位相差340mV,据此可实现对二者的同时检测,并可应用于实际样品测定。 相似文献
5.
6.
A. Berthon L. K. Rangan J. Vrana
I. Butterworth
P. J. Litchfield A. M. Segar J. R. SmithJ. Meyer
E. Pauli B. Tallini 《Nuclear Physics B》1970,20(3):476-492A formationstudy of the reaction K−p→Λπo at 13 c.m. energies between 1915 and 2168 MeV is presented. Experimental differential cross sections and polarizations are given as expansions of Legendre polynomials and associated Legendre polynomials respectively. Partial wave analysis confirms the
assignment of the Σ(2030) and the
assignment of the Σ(1915). The parameters of these resonances are determined. The possible existence of other resonances coupled to this channel is investigated. 相似文献
7.
We transfer the whole geometry of PG(3, q) over a non-singular quadric Q4,q of PG(4, q) mapping suitably PG(3, q) over Q4,q. More precisely the points of PG(3, q) are the lines of Q4,q; the lines of PG(3, q) are the tangent cones of Q4,q and the reguli of the hyperbolic quadrics hyperplane section of Q4,q. A plane of PG(3, q) is the set of lines of Q4,q meeting a fixed line of Q4,q. We remark that this representation is valid also for a projective space
over any field K and we apply the above representation to construct maximal partial spreads
in PG(3, q). For q even we get new cardinalities for
For q odd the cardinalities are partially known. 相似文献
8.
9.
C70X2(X=H,F, Cl)的稳定性和电子光谱 总被引:1,自引:0,他引:1
用INDO方法研究C70H2四种异构体的稳定性, 表明其最稳定异构体为1, 9-C70H2和7, 8-C70H2, 两者能量差为16.3KJ.mol^-^1, 与实验值及ab initio计算值接近; 光谱计算表明, 其特征吸收峰与实验值一致。在此基础上预测C70F2和C70Cl2的稳定性和电子光谱, 表明C70F2四种异构体的稳定性顺序与C70H2一致, 而C70Cl2则以21, 42-异构体最为稳定。二者的电子光谱与C70H2极其相似只是在500nm以上有细微差别。 相似文献
10.