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1.
Lipunova G. N. Nosova E. V. Vasil"eva P. V. Charushin V. N. 《Russian Chemical Bulletin》2003,52(2):457-460
The reactions of 2-cyanomethylbenzimidazole with polyfluorobenzoyl chlorides afforded 2-(1,3-dihydrobenzimidazol-2-ylidene)-3-oxo-3-polyfluorophenylpropionitriles. Refluxing of the latter compounds in acetonitrile in the presence of DBU or in dimethylformamide in the presence of amines gave rise to fluorine-containing derivatives of benzimidazo[1,2-a]quinolone. 相似文献
2.
Anastacia A. Layeva Galina N. Lipunova Valerii N. Charushin 《Journal of fluorine chemistry》2007,128(7):748-754
A new approach for the synthesis of fluorinated 1H-quinazolin-4-ones and 4-substituted quinazolines has been developed. 6-Fluoro-1H-quinazolin-4-ones were obtained by intramolecular cyclization of fluorine-containing S-ethyl N-benzoylisothioureas. Nucleophilic substitution reactions at positions 2 and 7, as well as alkylation at 1-position of quinazolinones were investigated. In addition, the synthesis of fluorine-containing 4-aminoquinazolines was carried out. 相似文献
3.
E. V. Nosova L. P. Sidorova G. N. Lipunova N. N. Mochul'skaya O. M. Chasovskikh V. N. Charushin 《Chemistry of Heterocyclic Compounds》2002,38(8):922-928
Ethyl esters of 1-(7-Z-1-ethyl-6-fluoro-4-oxo-1,4-dihydroquinoline-3-carbamoyl)-5-X-6,7,8-trifluoro-4-oxo-1,4-dihydroquinoline-3-carboxylic acids (X = H, F; Z = pyrrolidino-, piperidino-, hexamethylenimino-, morpholino-, thiomorpholino-) have been synthesized by the interaction of quinolone-3-carboxylic acid hydrazides with ethyl esters of 3-ethoxy-2-(polyfluorobenzoyl)acrylic acid . It was shown possible to cyclize intramolecularly the esters obtained with the formation of 1,3,4-oxadiazino[6,5,4-i,j]quinoline derivatives. 相似文献
4.
Heterocyclic analogs of triphenylformazan have been synthesized: 1-(1'-benzylbenzimidazolyl)-3,5-diphenylformazan (I), 1-benzothiazolyl-3,5-diphenylformazan (II), and 1-benzoxazolyl-3,5-diphenylformazan (III). On a basis of the study of IR and UV spectra, the hypothesis has been put forward that I lacks a chelate ring while II and III have chelate rings with a weak intramolecular hydrogen bond. Ease of complex formation with many metals and a capacity for the formation of tetrazolium salts have been noted.For part XXII, see [1]. 相似文献
5.
G. N. Lipunova N. N. Gulemina A. P. Zeif N. P. Bednyagina 《Chemistry of Heterocyclic Compounds》1974,10(4):428-433
1-Benzothiazolyl-5-(p-nitrophenyl)formazans, which have thermochromic properties, were synthesized. The structure of the compounds was studied by means of IR and UV spectroscopy and quantum-mechanical calculations, the state of the tautomeric equilibrium was established, and the most probable planar conformations of the formazans as a function of the character of the substituent in the 3-position of the formazan chain were found. It is shown that the thermochromism of these compounds in solution is related to dissociation of the hydrogen of the NH bond of the formazan grouping and that the deeply-colored thermally induced form is the anionic aci form. 相似文献
6.
7.
T. V. Trashakhova E. V. Nosova M. S. Valova P. A. Slepukhin G. N. Lipunova V. N. Charushin 《Russian Journal of Organic Chemistry》2011,47(5):753-761
trans-2-Styryl-substituted 3H-, 3-phenyl-, and 3-naphthylquinazolin-4-ones and their 6,7-difluoro derivatives were synthesized by condensation of appropriate
2-methylquinazolin-4-ones with aromatic aldehydes or by the transformation of the heterocycle of 2-methyl-3,1-benzoxazin-4-one
under the action of benzylidenephenylamines. 相似文献
8.
G. N. Lipunova E. V. Nosova V. N. Charushin O. M. Chasovskikh 《Chemistry of Heterocyclic Compounds》2001,37(10):1278-1288
3-(2-Acylhydrazino)-2-tetra(penta)fluorobenzoylacrylates are readily converted to acylamino-substituted quinolones and, under more forcing conditions, annelation of oxadiazine ring occurs. We have identified the possible cyclization of the mentioned acrylates to 4,5-substituted pyrazoles. 相似文献
9.
Kh. Z. Brainina N. Yu. Stozhko L. V. Aleshina G. N. Lipunova 《Journal of Analytical Chemistry》2003,58(10):965-971
A mercury-free modified screen-printed electrode was proposed for the preconcentration and determination of Cu(II), Pb(II), Cd(II), and Zn(II). The simplicity of design, compactness, and low cost of the developed electrode; the possibility of using it as a disposable electrode; and no need in any operations on the mechanical treatment of the electrode surface make this electrode a candidate for portable transducers in flow and discrete analyses. 相似文献
10.
A. A. Layeva E. V. Nosova G. N. Lipunova T. V. Trashakhova V. N. Charushin 《Russian Chemical Bulletin》2007,56(9):1821-1827
5-Fluoroquinazoline-2,4-diones and their 2-thio analogs were obtained from 6-fluoroanthranilic acid. Two convenient routes
to 5-fluoroquinazolin-4-ones involved cyclocondensation of 6-fluoroanthranilamide with acid chlorides (anhydrides) or with
aromatic (heterocyclic) aldehydes. A method for the synthesis of 7-fluoroquinazolin-4-one from 2,4-difluorobenzoic acid was
proposed.
Dedicated to Academician G. A. Abakumov on the occasion of his 70th birthday.
Published in Russian in Izvestiya Akademii Nauk. Seriya Khimicheskaya, No. 9, pp. 1758–1764, September, 2007. 相似文献