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13CT1 relaxation times for the different carbons of the sodium dodecyl sulphate chain in micellar systems have been measured, using Gd3+ as a paramagnetic relaxation reagent. The fluorescence decay of ω-(-naphthyl) dodecanoic acid, solubflized in the sodium dodecyl sulphate micelles was obtained in the presence of various amounts of counterion quencher Both series of experiments point to the occurrence of chain folding and to the fact that the terminal group can approach the Stern region of the micelle. 相似文献
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Van Der Borght M Vanderzande D Adriaensens P Gelan J 《The Journal of organic chemistry》2000,65(2):284-289
In our laboratory a precursor route to poly(p-phenylenevinylene) derivatives is developed in which unsymmetrically substituted p-xylene derivatives, possessing a benzylic sulfinylalkyl group, are used as monomers. Because of this unsymmetry, we were forced to investigate thoroughly the synthesis of these sulfoxides, as we start from symmetric and readily accessible molecules, namely, bis(halomethyl)-p-xylene derivatives. In a former publication, a new extremely effective route for the production of these unsymmetrically substituted sulfinyl monomers was presented. This paper expands upon these previously reported results. To examine the scope and limitations of this elegant route, this new method was applied to the synthesis of various derivatives not included in the initial work. 相似文献
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Alves GA Amato S Anjos JC Appel JA Astorga J Bracker SB Cremaldi LM Darling CL Dixon RL Errede D Fenker HC Gay C Green DR Halling AM Jedicke R Karchin PE Kwan S Leuking LH Mantsch PM de Mello Neto JR Metheny J Milburn RH de Miranda JM da Motta Filho H Napier A Passmore D Rafatian A dos Reis AC Ross WR Santoro AF Sheaff M Souza MH Spalding WJ Stoughton C Streetman ME Summers DJ Takach SF Wallace A Wu Z 《Physical review D: Particles and fields》1994,49(9):R4317-R4320
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Alves GA Amato S Anjos JC Appel JA Astorga J Bracker SB Cremaldi LM Dagenhart WD Darling CL Dixon RL Errede D Fenker HC Gay C Green DR Jedicke R Karchin PE Kennedy C Kwan S Lueking LH de Mello Neto JR Metheny J Milburn RH de Miranda JM da Motta Filho H Napier A Passmore D Rafatian A dos Reis AC Ross WR Santoro AF Sheaff M Souza MH Spalding WJ Stoughton C Streetman ME Summers DJ Takach SF Wallace A Wu Z 《Physical review letters》1996,77(12):2388-2391
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Alves GA Amato S Anjos JC Appel JA Bracker SB Cremaldi LM Darling CL Dixon RL Errede D Fenker HC Gay C Green DR Jedicke R Kaplan D Karchin PE Kwan S Leedom I Lueking LH Luste GJ Mantsch PM de Mello Neto JR Metheny J Milburn RH de Miranda JM da Motta Filho H Napier A Rafatian A dos Reis AC Reucroft S Ross WR Santoro AF Sheaff M Souza MH Spalding WJ Stoughton C Streetman ME Summers DJ Takach SF Wu Z 《Physical review letters》1993,70(6):722-725
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M. L. Scheepers P. J. Adriaensens J. M. Gelan R. A. Carleer D. J. Vanderzande N. K. De Vries P. M. Brandts 《Journal of polymer science. Part A, Polymer chemistry》1995,33(6):915-920
1H and 13C NMR have been used for the quantitative determination of methylene-ether bridges in melamine-formaldehyde (MF) resins. The amount of methylene-ether bridges was determined by 13C NMR from the number of monomethylolated amino groups consumed in the condensation reactions and is in agreement with that calculated from the condensation water contents. This latter method, which involves a combination of 1H and 13C NMR, is based on the amount of condensation water released during the formation of both methylene and methylene-ether bridges. © 1995 John Wiley & Sons, Inc. 相似文献