Regression and ANN models for estimating minimum value of machining performance

Surface roughness is one of the most common performance measurements in machining process and an effective parameter in representing the quality of machined surface. The minimization of the machining performance measurement such as surface roughness (R_a) must be formulated in the standard mathematical model. To predict the minimum R_a value, the process of modeling is taken in this study. The developed model deals with real experimental data of the R_a in the end milling machining process. Two modeling approaches, regression and Artificial Neural Network (ANN), are applied to predict the minimum R_a value. The results show that regression and ANN models have reduced the minimum R_a value of real experimental data by about 1.57% and 1.05%, respectively.     

Investigating semiconductor layered systems of photonics

The structure of a heterostructures-based semiconductor laser is experimentally investigated by complex means involving systems of scanning electron microscopy, scanning probe microscopy, and Raman spectroscopy. The possibilities of high-resolution microscopy for diagnostics of layered microelectronic systems are demonstrated.     

$QTAG$-Modules whose $h$-Pure-$S$-High Submodules Have Closure

A right module $M$ over an associative ring $R$ with unity is a $QTAG$-module if every finitely generated submodule of any homomorphic image of $M$ is a direct sum of uniserial modules. This article considers the closure of $h$-pure-$S$-high submodules of $QTAG$-modules. Here, we determine all submodules $S$ of a $QTAG$-module $M$ such that each closure of $h$-pure-$S$-high submodule of $M$ is $h$-pure-$\overline{S}$-high in $\overline{M}$. A few results of this theme give a comparison of some elementary properties of $h$-pure-$S$-high and $S$-high submodules.     

On some imbedding relations between certain sequence spaces

We introduce a space of sequences l_p^l \ell_p^\lambda of nonabsolute type, which is a p-normed space and a BK-space in the cases of 0 < p < 1 and 1 ≤ p < ∞; respectively. Further, we deduce some imbedding relations and construct a basis for the space l_p^l \ell_p^\lambda , where 1 ≤ p < ∞.     

Determination of Phenolic Compounds in Various Propolis Samples Collected from an African and an Asian Region and Their Impact on Antioxidant and Antibacterial Activities

The biological activities of propolis samples are the result of many bioactive compounds present in the propolis. The aim of the present study was to determine the various chemical compounds of some selected propolis samples collected from Palestine and Morocco by the High-Performance Liquid Chromatography–Photodiode Array Detection (HPLC-PDA) method, as well as the antioxidant and antibacterial activities of this bee product. The chemical analysis of propolis samples by HPLC-PDA shows the cinnamic acid content in the Palestinian sample is higher compared to that in Moroccan propolis. The results of antioxidant activity demonstrated an important free radical scavenging activity (2,2-Diphenyl-1-picrylhydrazyl (DPPH); 2,2′-azino-bis 3-ethylbenzothiazoline-6-sulphonic acid (ABTS) and reducing power assays) with EC₅₀ values ranging between 0.02 ± 0.001 and 0.14 ± 0.01 mg/mL. Additionally, all tested propolis samples possessed a moderate antibacterial activity against bacterial strains. Notably, Minimum Inhibitory Concentrations (MICs) values ranged from 0.31 to 2.50 mg/mL for Gram-negative bacterial strains and from 0.09 to 0.125 mg/mL for Gram-positive bacterial strains. The S2 sample from Morocco and the S4 sample from Palestine had the highest content of polyphenol level. Thus, the strong antioxidant and antibacterial properties were apparently due to the high total phenolic and flavone/flavonol contents in the samples. As a conclusion, the activities of propolis samples collected from both countries are similar, while the cinnamic acid in the Palestinian samples was more than that of the Moroccan samples.     

Chemical Exchange Saturation Transfer (CEST) Agents: Quantum Chemistry and MRI

Diamagnetic chemical exchange saturation transfer (CEST) contrast agents offer an alternative to Gd³⁺‐based contrast agents for MRI. They are characterized by containing protons that can rapidly exchange with water and it is advantageous to have these protons resonate in a spectral window that is far removed from water. Herein, we report the first results of DFT calculations of the ¹H nuclear magnetic shieldings in 41 CEST agents, finding that the experimental shifts can be well predicted (R²=0.882). We tested a subset of compounds with the best MRI properties for toxicity and for activity as uncouplers, then obtained mice kidney CEST MRI images for three of the most promising leads finding 16 (2,4‐dihydroxybenzoic acid) to be one of the most promising CEST MRI contrast agents to date. Overall, the results are of interest since they show that ¹H NMR shifts for CEST agents—charged species—can be well predicted, and that several leads have low toxicity and yield good in vivo MR images.     

Determination of Cadmium in Human Serum and Blood Samples after Dispersive Liquid–Liquid Microextraction Using a Task-Specific Ionic Liquid

Task-specific ionic liquid dispersive liquid–liquid microextraction (TSIL-DLLME) is a simple and rapid preconcentration approach for the measurement of cadmium in serum and blood samples of human subjects. In this method a novel task-specific ionic liquid, trioctylmethyl ammonium thiosalicylate (TOMATS), which has dual characteristics as a chelating agent and extractive solvent, was investigated. TOMATS complexes with Cd due to the chelating effect of the ortho-positioned carboxylate relative to the thiol functionality. The assessment of the optimum values of variables including the pH, amount of reagents (TOMATS, diluents, Triton X114, and back extracting acid solution), temperature, and incubation time, which affect the recoveries of analyte by TSIL-DLLME method were studied. After enrichment experiments, acidic solution was used to back extract the metal ions from the ionic liquid rich phase and with determination by electrothermal atomic absorption spectrometry. Using the optimal experimental conditions, the limit of detection (3?s), precision (relative standard deviation), preconcentration, and enhancement factors of developed method for Cd were found to be 0.05?µg/L, greater than 5%, 62.5, and 52.8, respectively. To check the accuracy of the developed method, certified reference material of serum and blood were analyzed by the developed method, and the measured values of Cd were in good agreement with the certified values. The developed method was applied successfully to determine Cd in blood and serum samples of lymphatic cancer patients relative to healthy controls.     

Integrated inventory and inspection policies for stochastic demand

In this paper, we develop integrated inventory inspection models with and without replacement of nonconforming items. Inspection policies include no inspection, sampling inspection, and 100% inspection. We consider a buyer who places an order from a supplier when his inventory level drops to a certain point, due to demand which is stochastic in nature. When a lot is received, the buyer uses some type of inspection policy. The fraction nonconforming is assumed to be a random variable following a beta distribution. The order quantity, reorder point and the inspection policy are decision variables. In the inspection policy involving determining sampling plan parameters, constraints on the buyer and manufacturer risks is set in order to obtain a fair plan for both parties. A solution procedure for determining the operating policies for inventory and inspection consisting of order quantity, sample size, and acceptance number is proposed. Numerical examples are presented to conduct a sensitivity analysis for important model parameters and to illustrate important issues about the developed models.     

Isospin violations in largeP T pion inclusive processes in perturbative quantum chromodynamics

We investigate the asymmetries arising due to electromagnetic interactions in largeP _T pion inclusive processes. The hardqcd processes that contribute to such asymmetries areq+g→q+γ,q+q→g+γ etc. which are suspected to be substantial, as indicated by theqcd predictions for a significant and increasingγ/π ^o ratio at largeP _T. We calculate the expected isospin related asymmetries and propose tests that might detect them. Our estimates indicate that the effects are much smaller than may be naively expected. We also observe a remarkable scaling of asymmetries in the variableP _T/(s)^1/2.