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981.
Precipitate-forming chemical reactions have been studied in chemically cross-linked poly(vinyl alcohol) gel medium. One of the reactive components was incorporated into the gel, the other was allowed to diffuse into it. Depending on the experimental conditions the reaction-diffusion process often results in patterns of different type. Experiments performed in tubes and in thin layers were carried out in order to investigate the effects of various factors (cross-linking density, swelling degree as well as the concentrations of the outer and inner electrolytes) on the morphologies of the precipitate patterns. It was found that precipitation occurs not only in the Liesegang bands, but also between bands. Beside Liesegang-type structures, tree-like patterns have been observed, showing a characteristic periodicity in the density profile obtained by digitalized image analyses. 相似文献
982.
双(十二烷基亚磺酰)乙烷溶剂萃取钯及其机理的研究 总被引:2,自引:0,他引:2
本文研究用双(十二烷基亚磺酰)乙烷萃取钯的性能,在KI存在下从7mol/L盐酸介质中用含有BDSE的氯仿能定量萃取钯,有机的钯可被硫脲或氨溶液反萃继之用TMK-TritonX-100光度法测定,研究了萃取的最佳条件及干扰情况,斜率法测得萃合物组成为Pd:I:BDSE=1:2:1,红外光谱证实萃合物中BDSE的二个亚砜以硫原子与钯配位,萃合物为异位体络合物,提出了选择性萃取分离钯的新方法。 相似文献
983.
Vipul Dav Wolfgang G. Glasser Garth L. Wilkes 《Journal of Polymer Science.Polymer Physics》1993,31(9):1145-1161
Fibers were spun from isotropic and anisotropic dimethylacetamide solutions of cellulose esters. Take-up speeds of the dry jet/wet spinning process varied. Water served as the coagulant. The mechanical properties of the fibers increased as spinning progressed from the isotropic to the anisotropic state of the solution. A trade-off in solubility and fiber properties was noted as the butyryl acetyl ratio decreased. Whereas high butyryl content enhances both overall solubility and the formation of liquid–crystalline solutions at lower concentration, it results in lower fiber modulus and strength. Morphology of the fibers depended on the coagulation rate which was influenced by the concentration of the sppinning solution. The level of orientation and crystallinity of the fibers increased somewhat when they were spun from liquid-crystalline solutions. © 1993 John Wiley & Sons, Inc. 相似文献
984.
Summary.
We consider a discontinuous Galerkin finite element method
applied in time to a model Volterra equation of the second kind.
A residual-based computable
Galerkin-error estimate is derived
for .
This estimate does not explicitly
contain the time step and therefore the time step
control must be based
on a heuristic criterion, the estimate can then be used to
demonstrate the integrity, or otherwise, of the finite element
solution. After performing some numerical experiments
we conclude that this approach is at least competetive
with classical discretizations since it is
computationally simple to implement,
but has the added advantage of
reliable error feedback.
Received June 25, 1995 相似文献
985.
Glucose, maltose, sucrose, lactose, ethanol and urea concentrations were monitored simultaneously during the cultivation of Escherichia coli and Saccharomyces cerevisiae by means of enzyme field effect transistors (EnFETs) applying glucose dehydrogenase (GDH), maltase (MAL)/GDH, invertase (INV)/GDH, β-galactosidase (β-GAL)/galactosedehydrogenase (GALDH), alcoholdehydrogenase (ADH)/aldehydedehydrogenase (ALDH), and urease. These enzymes were (co)immobilized on the pH sensitive gates of an eight-FET array. The FET array was integrated in a commercial FIA system. 相似文献
986.
Michael Bildhauer 《manuscripta mathematica》1998,97(3):389-406
H?lder continuity up to the free boundary is proved for minimizing solutions if they meet the supporting surface in an angle
which is bounded away from zero. The problem is localized by proving the continuity of the distance function, a result which
is also true for stationary points.
Received: 14 April 1998 相似文献
987.
M. Sugawara H. Kusakari T. Murakami T. Kohno 《The European Physical Journal A - Hadrons and Nuclei》1998,1(3):237-239
A new rotational band has been observed in 167Lu by 152Sm (19F,4n)reaction at the HI-13 tandem accelerator of CIAE in Beijing. The high spin transition energies of the new band are almost
identical to the triaxial superdeformed bands recently discovered in 163Lu and 165Lu. This new band is predicted as a triaxial superdeformed band by total routhian surface calculations.
Received: 6 October 1997 相似文献
988.
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