The system of L-band 2 × 10 Gb/s WDM transmission over conventional single mode fibre with 600 km by chirped fibre Bragg gratings dispersion compensation

A chirped fibre Bragg grating according to ITU-T suggested L-band （2nd channel λ1 = 1570.83 nm; 80th channel λ2 = 1603.57 nm） with more than 1800 ps/nm single channel dispersion compensation is presented in this paper, of which the cladding mode loss, the delay curve ripple and the power fluctuation of the reflected spectrum are less than 0.5 dB, 50 ps and 0.25 dB, respectively. With this new FBG as dispersion compensation device, a 2 × 10 Gb/s wavelength division multiplexing （WDM） L-band transmission of 600 km based on conventional single mode fibre （G.652 fibre） is performed without forward error correction. The bit error rate （BER） is less than 10-12 and the power penalties of the 2nd and 80th channel of L-band are 1.8 dB and 2.0 dB, respectively.     

沙摆实验误差分析

从实验误差理论角度，分析了沙摆重心变化引起的实验误差，结果表明由重心变化引起的误差相对于其它误差而言在实验中占主要地位．     

Lattice dynamics study of low energy guest-host coupling in clathrate hydrate

Our lattice dynamics simulation of Xe-hydrate with four-site TIP4P oxygen-shell model can accurately reproduce each peak position in the inelastic incoherent neutron scattering spectrum at the acoustic band （below 15 meV） and yield correct relative intensity. Based on the results, the uncertain profile at ～6 meV is assigned to anharmonic guest modes coupled strongly to small cages. Blue shift is proposed in phonon dispersion sheet in the case of anticrossing and found to be an evident signal for guest-host coupling that explains the anomalous thermal conductivity of clathrate hydrate.     

陶瓷真空室镀膜工艺改进及脉冲磁场时间特性测量

 介绍了合肥光源二期工程注入段陶瓷真空室的改进情况,采用新的镀膜技术,大大改善了脉冲磁场的延时特性,减少了储存环注入时的轨道扰动,提高了注入束流累积效速率。改进了原来的点线圈磁场测量方法,采用带有积分电路及抗干扰措施的双线圈测量装置测量了真空室内的脉冲磁场延时特性,使脉冲磁场延时误差测量的分辨率达到ns量级,给出了测量结果。     

含非线性能量汇的简支输液管非线性振动控制研究

论文建立了一个含有非线性能量汇(NES)装置并输运脉动内流的简支输液管道理论模型, 研究了NES装置对管道的非线性动力学特性与振动控制的影响. 利用Galerkin和龙格库塔法, 得到了在含NES和不含NES装置时管道动力学响应的数值结果. 研究表明, NES装置能有效地抑制管道振动. 通过对比可知, NES对管道系统的稳定性和非线性振动控制有着明显的影响. 此外, 本文还详细讨论了NES装置相关参数对系统的动力学影响. 结果表明, 增大NES的弹簧刚度、阻尼和质量比有利于管道减振, 且最佳安装位置在管道中点. 此外, 增大阻尼?能缩小失稳激励频率区域, 而其他参数的变化对失稳激励频率区域影响较小.     

塑料拉伸强度测量结果的不确定度评定

依据GB/T 1040.2-2006<塑料拉伸性能的测定>,测定了聚丙烯塑料的拉伸强度,对拉伸强度测量不确定度进行了分析和量化.当聚丙烯的拉伸强度为26.2 MPa时,测量结果的扩展不确定度为0.40 MPa.     

Scanning the energy dissipation process of energetic materials based on excited state relaxation and vibration–vibration coupling

The energy dissipation mechanism of energetic materials(EMs) is very important for keeping safety. We choose nitrobenzene as a model of EM and employ transient absorption(TA) spectroscopy and time-resolved coherent anti-stokes Raman scattering(CARS) to clarify its energy dissipation mechanism. The TA data confirms that the excited nitrobenzene spends about 16 ps finishing the twist intramolecular charge transfer from benzene to nitro group, and dissipates its energy through the rapid vibration relaxation in the initial excited state. And then the dynamics of vibrational modes(VMs) in the ground state of nitrobenzene, which are located at 682 cm~(-1)(v_1), 854 cm~(-1)(v_2), 1006 cm~(-1)(v_3), and 1023 cm~(-1)(v_4),is scanned by CARS. It exhibits that the excess energy of nitrobenzene on the ground state would further dissipate through intramolecular vibrational redistribution based on the vibrational cooling of vi and v_2 modes, v_1 and v_4 modes, and v_3 and v_4 modes. Moreover, the vibration-vibration coupling depends not only on the energy levels of VMs, but also on the spatial position of chemical bonds relative to the VM.     

微波消解-ICP-MS测定土壤样品中的重金属离子

采用微波消解-ICP-MS测定土壤样品中铬、铜、镍、锌、镉、铅,利用国家环境标准样品ESS-1验证了方法的准确度,准确度在100%左右,测定值与标准值吻合,相对偏差小于4%,并比较了两种消化方法对测定结果的影响;优化了ICP/MS工作参数;用多内标法有效的校正了基体干扰.进行东北老工业基地某厂区土壤测试.方法的检出限0.0144-1.0218μg·g-1精密度为0.15%-3.51%,回收率为83.2%-108.9%,为环境土壤样品的分析测试提供了一种可靠、高灵敏分析方法.     

基于变形镜的气动光学效应仿真实验研究

基于高速飞行器流场光传输数据和变形镜系统,提出了一种气动光学效应半实物仿真方法。根据流体力学、统计、几何和物理光学等理论,建立远场目标的光学传输模型,获得气动光学效应引起的目标光波的波前畸变数据,控制变形镜系统调制光波来仿真生成畸变。完成了初步验证,建立了一个超音速飞行模型(马赫数Ma=5)并进行了仿真实验,计算了实验的波前仿真误差,并分析了成像偏移和模糊特性。对高速飞行中的气动光学效应进行仿真,在实验室条件下实现对相关成像系统性能和校正技术的测试。     

碱熔试样-原子吸收光谱法测定铜阳极泥预处理渣料中的Sb

铜阳极泥是一种重要的冶金工业副产品,因其中含有多种贵金属和有价金属元素,铜阳极泥的综合回收利用日益受到关注。铜阳极泥预处理富集渣中富含的Sb难以用常规方法溶解,有必要建立一种准确、简便的测试方法实现Sb的定量分析。采用X射线荧光光谱、X射线衍射光谱和场发射扫描电镜能谱分析等多种光谱学分析手段对富集渣的化学成分、物相和微观结构做了全面分析,结果表明,富集渣的化学组成和物理结构复杂,组分化学性质稳定且共生紧密。Sb以高锑酸金属化合物的形式存在,结构稳定化学惰性强。采用Na₂O₂熔融法消解试样,合成标准样品做标准系列,用火焰原子吸收光谱法测定了富集渣中Sb的含量值为8.23%,相对标准偏差为0.97%。该方法的检出限为0.072%,加标回收率为94.9%~99.2%。本方法溶样彻底,不需贵重试剂和仪器,方法简单易行。采用与样品基体相近的合成标准样品,消除了样品化学成分复杂所造成的共存物质干扰。通过标准样品测试验证和其他仪器方法比对,证明本方法灵敏度高,准确性好,可用于铜阳极泥预处理渣料中Sb的定量测定。