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71.
Many previous researches have concentrated on the noise of backward-curved (BC) blades and forward-curved (FC) multi-blade centrifugal fans. In this paper, an experimental study has been carried out to study the noise reduction of an industrial FC blades centrifugal fan. First of all, the performance and noise characteristics of the FC centrifugal fan were tested to compare the similarities and differences from those of BC blades and FC multi-blade centrifugal fans. And then, some different volute geometric configurations were carried out in order to study the effects of inclined volute tongue, impeller blade-tongue clearance, hub-volute clearance and their coupling effect to the performance and noise of the FC blades centrifugal fan. The aim of many different experimental tests is to validate whether the effects of different modifications to fan performance and noise are additive and to find a good impeller-volute matching to reduce the centrifugal fan noise without reducing performance. The experimental results show that a good coupled modification not only could reduce the fan noise but also could advance the fan performance and extend the operating range.  相似文献   
72.
Watson’s theory of pure rotational spectra in nonpolar molecules is adapted to show that, if appropriate symmetry conditions are met, centrifugal distortion can lead to the appearance of the forbidden 0-0 origin band in an electronically forbidden spectrum. The intensity of such bands will be low; in the case of the benzene Ã1B2u-1A1g system the maximum intensity of the forbidden origin is estimated to be about 10−7 of that of the 610 band in the main vibronic spectrum. The prospects for the experimental detection of such weak bands are discussed.  相似文献   
73.
Vandaterosides are polar glucosyloxybenzyl eucomate derivatives found in Vanda teres (Orchidaceae), which display biological activities that slow the skin ageing process. In order to obtain larger quantities to allow us to go further in the bioassays, the hydroalcoholic extract of aerial parts (leaves and stems) of V. teres were fractionated by centrifugal partition chromatography, combining isocratic, gradient, and dual elution modes. The first fractionation was performed on the extract maintained in the stationary phase as water saturated in butanol, while increasing the polarity of the mobile phase by changing the proportions of ethyl acetate/1‐butanol/water, in order to obtain two enriched fractions. Vandateroside I was then purified by isocratic mode with ethyl acetate/ethanol/water (46:14:40), while vandateroside II was obtained by combining isocratic elution with ethyl acetate/isopropanol/water (30:20:50) followed by a multiple dual mode with ethyl acetate/ethanol/water (46:14:40). In this manner, hundreds of milligrams of vandateroside I and II were recovered from 10 g of V. teres extract.  相似文献   
74.
Microfluidic DNA microarray analysis: a review   总被引:1,自引:0,他引:1  
Microarray DNA hybridization techniques have been used widely from basic to applied molecular biology research. Generally, in a DNA microarray, different probe DNA molecules are immobilized on a solid support in groups and form an array of microspots. Then, hybridization to the microarray can be performed by applying sample DNA solutions in either the bulk or the microfluidic manner. Because the immobilized probe DNA binds and retains its complementary target DNA, detection is achieved through the read-out of the tagged markers on the sample target molecules. The recent microfluidic hybridization method shows the advantages of less sample usage and reduced incubation time. Here, sample solutions are confined in microfabricated channels and flow through the probe microarray area. The high surface-to-volume ratio in microchannels of nanolitre volume greatly enhanced the sensitivity as obtained with the bulk solution method. To generate nanolitre flows, different techniques have been developed, and this including electrokinetic control, vacuum suction and syringe pumping. The latter two are pressure-driven methods which are more flexible without the need of considering the physicochemical properties of solutions. Recently, centrifugal force is employed to drive liquid movement in microchannels. This method utilizes the body force from the liquid itself and there are no additional solution interface contacts such as from electrodes or syringes and tubing. Centrifugal force driven flow also features the ease of parallel hybridizations. In this review, we will summarize the recent advances in microfluidic microarray hybridization and compare the applications of various flow methods.  相似文献   
75.
Conventional centrifugal pumps with volute casing generate fluid-dynamic noise particularly at the so-called blade-passing frequency, which is attributed to the interaction of the flow exiting the pump impeller with the volute tongue. Following previous work by the authors to characterize the effect of that blade–tongue interaction on the tonal sound produced, this paper presents a simple acoustic model for centrifugal pumps that considers ideal sound sources of arbitrary position and properties. The model is to be implemented in a software code that applies it systematically to a pump previously tested at laboratory, until identifying the set of ideal sources that best reproduce the pressure fluctuation measurements. In this model, the ideal sources are assumed to radiate plane sound waves along the impeller channels, volute, and outlet diffuser. The volute was considered to be composed by a succession of slices, each of them equivalent to a linear 3-port acoustic system with individual sound transmission and reflection coefficients. A series of tests was conducted to check the validity of the acoustic model, by applying an external acoustic load onto the pump outlet duct and measuring the noise reflected. The resulting reflection coefficient was in good agreement with the predictions of the acoustic model. Finally, the model was used to investigate the pump internal sound field at the blade-passing frequency when operating at 70% of nominal flow rate. It was concluded that the sound field can be characterized reasonably by a dipole-like source located at the tongue region.  相似文献   
76.
Centrifugal experiments were carried out to investigate the responses of suction bucket foundations under horizontal and vertical dynamic loading. It is shown that when the loading amplitude is over a critical value, the sand at the upper part around the bucket is softened or even liquefied. The excess pore pressure decreases from the upper part to the lower part of the sand layer in the vertical direction and decreases radially from the bucket’s side wall in the horizontal direction. Large settlements of the bucket and the sand layer around the bucket are induced by dynamic loading. The dynamic responses of the bucket with smaller height (the same diameter) are heavier. The project supported by the fund of Chinese Ocean Oil Co. and Chinese Academy of Sciences(KZCX2-YW-302-02).  相似文献   
77.
Soybean oil deodorized distillate (SODD) is a byproduct from refining edible soybean oil; however, the deodorization process removes unsaponifiable materials, such as sterols and tocopherols. Tocopherols are highly added value materials. Molecular distillation has large potential to be used in order to concentrate tocopherols, because it uses very low levels of temperatures because of the high vacuum and short operating time for separation and, also, it does not use solvents. However, nowadays, the conventional way to recover tocopherols is carrying out chemical reactions prior to molecular distillation, making the process not so suitable to deal with natural products. The purpose of this work is to use only molecular distillation in order to recover tocopherols from SODD. Experiments were performed in the range of 140–220°C. The feed flow rate varied from 5 to 15 g/min. The objective of this study was to remove the maximum amount of free fatty acids (FFA) and, so, to increase the tocopherol concentration without add any extra component to the system. The percentage of FFA in the distillate stream of the molecular still is large at low feed flow rates and low evaporator temperatures, avoiding thermal decomposition effects.  相似文献   
78.
Preparative centrifugal partition chromatography (CPC) was successfully carried out for the separation of sinomenine from the methanolic extract of Sinomenium acutum stems and rhizomes. The optimum two-phase solvent system of CPC was composed of n-hexane/ethyl acetate/methanol/water at a volume ratio of 1:6:2:8 (v/v/v/v) with 0.1% triethylamine (TEA). Preparative CPC yielded 44.3 mg of sinomenine from 400 mg of MeOH extract with a purity of 96.9%.  相似文献   
79.
离心模型中的固结时间是原型的固结时间缩短至1/N2,能够在较短的时间内模拟软土地基的长期沉降.采用离心模型试验方法,模拟软土地基在粉喷桩处理后的渗透固结性状。通过对地基施工期阶段及工后的沉降进行分析,证实了用粉喷桩进行处理地基是可行的。  相似文献   
80.
In this study, citrate‐stabilised iron oxide nano‐particles (~16 nm) have been immobilised on commercial silica monolithic centrifugal spin columns (MonoSpin) for the extraction of phosphorylated compounds. Two alternative strategies were adopted involving either direct electrostatic attachment to an aminated MonoSpin (single‐layer method) in the first instance, or the use of a layer‐by‐layer method with poly(diallyldimethylammonium) chloride. Field‐emission scanning electron spectroscopy and energy‐dispersive X‐ray spectroscopy was used for confirming notably higher coverage of nano‐particles using the layer‐by‐layer method (2.49 ± 0.53 wt%) compared with the single‐layer method (0.43 ± 0.30 wt%). The modified monolith was used for the selective separation/extraction of adenosine monophosphate, adenosine diphosphate and adenosine triphosphate with elution using a phosphate buffer. A reversed‐phase liquid chromatographic assay was used for confirming that adenosine, as a non‐phosphorylated control was not retained on the modified MonoSpin devices, whereas recovery of 80% for adenosine monophosphate, 86% for adenosine diphosphate and 82% for adenosine triphosphate was achieved.  相似文献   
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