单片机在测量声速实验中的应用

单片机在测量声速实验中的应用郭立群，李将录，万新（哈尔滨师范大学物理系１５００８０）（哈尔滨塑料十二厂）一、引言目前各级各类学校的普通物理实验课普遍开设声速测量实验．声速测量的一般方法有行波法、驻波法、共鸣法等间接测量方法．这些方法都很巧妙，但误差较...     

基于纳米Ag粒子的表面等离子体共振光谱测定CN-的研究

利用UV-辐照光化学还原法制备了平均直径为20 nm的黄色胶体银溶液,银粒子的表面等离子体共振(SPR)光谱的最大吸收波长位于399 nm处,摩尔吸光系数为1.3×104 L·mol-1·cm-1.利用Ag粒子与CN-反应的动力学特性,研究了SPR光谱的λMAX吸光与CN-浓度的关系及其影响因素,拟定了检测环境水样中隐色、有毒CN-离子的方法.标准工作曲线的线性相关系数0.9995,测定下限0.05 μg/mL, 相对标准偏差RSD(%)≤6.1 (n=5).对Ag粒子与CN-反应的机理进行了探讨.     

TOUGHENING OF POLYCARBONATE WITH PBA-PMMA CORE-SHELL PARTICLES

The miscibility, mechanical properties, morphology and toughening mechanism of PC/PBA-PMMA blends were investigated. The dynamic mechanical results show that PC/PBA-PMMA blend has good miscibility and strong interfacial adhesion. The Izod impact strength of blend PC/PBA-PMMA with 4% (volume fraction) PBA-PMMA core-shell modifier is 16 times higher than that of pure PC. The core-shell volume fraction and thickness of the PMMA shell have effect on the toughness of PC/PBA-PMMA blends. As PMMA volume fraction increases, the toughness of PC/PBA-PMMA blend increases, and reaches a maximum value at 30% volume fraction of PMMA or so. The tensile properties of PC/PBA-PMMA blend with a minimum amount of PBA-PMMA modifier show that brittle-tough transition has no significant variance in comparison with that of pure PC. The scanning electron microscopic (SEM) observation indicates that the toughening mechanism of the blend with the pseudo-ductile matrix modified by small core-shell latex polymer particles is the synergetic effect of cavitation and shear yielding of the matrix.     

本刊加入《中国学术期刊(光盘版)》和“中国期刊网”的声明本刊加入万方数据(ChinaInfo)系统科技期刊群的声明

为适应我国信息化建设需要，扩大作者学术交流渠道，本刊加入《中国学术期刊(光盘版)》和“中国期刊网”。作者著作权使用费与本刊稿酬一次性给付。如作者不同意将文章编入该数据库，请在来稿时声明，本刊将作适当处理。 为了实现科技期刊编辑、出版发行工作的电子化，推进科技信息交流的网络化进程，我刊现已入网“万方数据(ChinaInfo)系统科技期刊群”。所以，向本刊投稿并录用的稿件文章，将一律由编辑部统一纳入万方数据(ChinaInfo)系统，进行因特网提供信息服务。凡有不同意者，请在来稿时声明，本刊将作适当处理。本刊所付稿酬包含刊物内容上网服务报酬，不再另付。 《光谱实验室》编辑部     

Atomistic Simulation of He Clustering and Defects Produced in Ni

Using the molecular dynamics method, the stability of small He-vacancy clusters is studied under the condition of the high He and low vacancy densities. The result shows that there is a competition between He atoms detrapped and self-interstitial atoms （SIAs） emitted during the clustering of He atoms. When the He number is above a critical value of 9, the SIA emission is predominant. The SIA emission can result in deep capture of He atoms since the binding energy of He to a He-vacancy cluster is increased with the number of SIAs created. The cluster thus grows up. In addition, more SIAs are created when the temperature is elevated. The average volume of a He atom is increased. The cluster expansion takes place at high temperature.     

Syntheses and Crystal Structures of 4-Amino-3- （3-hyd roxyp ropyl）- 1H-1,2,4-triazole-5（4H）-thione and 6-（4-Biphenylyl）-3-（3-hydroxypropyl）-7H-1,2,4-triazolo[3,4-b][1,3,4]thiadiazine

1INTRODUCTION It has been reported that3,6-disubstituted-7H-1,2,4-triazolo[3,4-b][1,3,4]thiadiazines have a broad spec-trum of bioactivities,such as antimicrobial[1],antibac-terial,antifungal[2],anti-inflammatory[3],diuretic[4],an-thelmintic and analgesic[5].They can also be used as plant-growth regulating agents[6],photographic coup-lers,dyes for improved preservability and absorption characteristics,and inhibitors of malignant cellularZOU K.H.et al.:Syntheses and Crystal Structures o…     

New exact periodic solutions to （2＋1）-dimensional dispersive long wave equations

In this paper, we make use of the auxiliary equation and the expanded mapping methods to find the new exact periodic solutions for （2＋1）-dimensional dispersive long wave equations in mathematical physics, which are expressed by Jacobi elliptic functions, and obtain some new solitary wave solutions （m → 1）. This method can also be used to explore new periodic wave solutions for other nonlinear evolution equations.