一种完整测量磁光克尔效应和法拉第效应的方法

详细给出了一种测量完整克尔和法拉弟效应的原理和实验装置。该装置简单可靠,安全由计算机控制。利用傅里叶变换方法,实验系统可以在从０．０１度至几百度的克尔和法拉第旋转角范围内以及在１．５￣６．０ｅＶ的光子能量范围内,准确地测量克尔和法拉第旋转角范围内以及在１．５￣６．０ｅＶ的光子能量范围内,准确地测量克尔和法拉第效应的绝对值。作为实验测量的例子,给出了ＭｎＢｉＡｌ合金薄膜样品和ＧａＰ块状样品的克尔和法     

723A型可见分光光度计的维护保养与常见故障的排除

介绍723A型可见分光光度计的日常维护保养措施及常见故障的排除方法。     

异质双碳源对LiMn0.8Fe0.2PO4复合材料电化学性能的影响

采用水基流变相辅助的固相法,以异质碳蔗糖和石墨为碳源,合成了LiMn_0.8Fe_0.2PO₄/C复合材料,研究了不同石墨加入方式对所制复合材料电化学性能的影响,并对所制备的LiMn_0.8Fe_0.2PO₄/C复合材料进行了X射线衍射(XRD)、N₂吸附-脱附测试、扫描电子显微镜(SEM)、透射电子显微镜(TEM)等表征。结果表明,不同石墨包覆工艺对材料结构和电化学性能具有显著影响。前驱体煅烧后再加入石墨获得的样品纯度高,形貌呈均一的椭圆形,在0.1C下的放电比容量为149 mAh·g^-1,达到其理论比容量的87%;在5C下最大的放电比容量为133 mAh·g^-1;在2C倍率下经过300次循环后比容量维持在127 mAh·g^-1,衰减率仅为1.9%,表现出了优良的循环稳定性。     

APPLICATIONS AND CHALLENGES OF STRUCTURAL OPTIMIZATION IN HIGH-SPEED AEROCRAFT 1)

高速飞行器是航空航天领域发展的重要方向,具有重大战略意义和重要经济社会价值。首先,对结构优化技术及其在飞行器零部件和全机结构概念设计中的应用进行综述;然后,根据典型使用环境和设计要求,总结高速飞行器结构设计中存在的主要问题和应用需求,着重介绍近年来在高速飞行器零部件和全机结构概念设计中应用结构优化技术的典型案例;最后,提出近期亟待突破或完善的结构优化技术。结构优化技术与设计经验相结合带来设计理念的变革,将成为先进飞行器设计的必备工具和标准流程。面向重大需求的结构优化理论研究与工程实践对提升我国航空航天核心竞争力具有重要价值。     

黄花棘豆化学成分的研究（Ⅲ）

从黄花棘豆总皂苷的酸水解产物中分离出两种三萜皂苷元Ⅰ和Ⅱ,总皂苷经反复柱层析又得一微量三萜皂苷Ⅲ.本文报道它们的结构鉴定以及Ⅰ和Ⅱ的有关化学转变,用~(13)C NMR技术指定了Ⅰ和Ⅱ的~(13)C NMR信号.     

Total synthesis of snake toxin α-bungarotoxin and its analogues by hydrazide-based native chemical ligation

A new method for α-bungarotoxin was reported by combining Fmoc-SPPS and peptide hydrazide based ligat ion strategy.     

Carbothermal synthesis of ultra-fine zirconium carbide powders using inorganic precursors via sol–gel method

Ultra-fine zirconium carbide (ZrC) powders have been synthesized by carbothermal reduction reactions using inorganic precursors zirconium oxychloride (ZrOCl₂ · 8H₂O) as sources of zirconium and phenolic resin as the carbon source. The reactions were substantially completed at relatively lower temperatures (∼1400 °C/1 h) and the synthesized powders had a small average crystallite size (<200 nm) and a large specific area (54 m²/g). The oxygen content of the powder synthesized at 1400 °C/1 h was less than 1.0 wt%. The thermodynamic change process in the ZrO₂–C system and the synthesis mechanism were studied.     

镧、铈对酸雨胁迫下龙眼(Dimocarpus longana Lour.)花粉萌发和坐果的影响

研究了La3+和Ce3+对酸雨胁迫下龙眼花粉萌发和坐果的影响.结果表明,酸雨胁迫下,低浓度(0.1～1 μmol·L-1)的La(NO3)3或Ce(NO3)3可以减轻酸雨对花粉的伤害,提高花粉萌发率,高浓度(10 μmol·L-1)则加重了酸雨的伤害作用;0.1～10 mmol·L-1的La(NO3)3和Ce(NO3)3均可以提高龙眼的坐果率,减轻酸雨对龙眼果实的伤害.     

苧蔴中游离单糖的液相色谱/质谱联用分析

本文应用液相色谱/质谱联用(LC/MS)技术分析了一些已知糖混合物.随后进一步研究了芋蔴中游离单糖的结构,实验结果和经典的衍生化,气相色谱分析结果相一致。     

Effect of sheath materials on the microstructure and superconducting properties of SmO0.7F0.3FeAs wires

Fe/Ti, Nb, and Ta sheathed SmO_0.7F_0.3FeAs wires were manufactured using the powder-in-tube method. A comparative study was made of the effect of sheath material on the microstructure and superconducting properties of the SmO_0.7F_0.3FeAs wires. Among these sheath materials, the penetration depth of Ta into the superconducting core is the largest. There was nearly no difference in the critical transition temperature of the SmO_0.7F_0.3FeAs wires sheathed with different materials, and the upper critical fields were approximately the same. On the other hand, it was found that Nb-sheathed wires had a higher superconducting current density than the others. Impurities existing in the superconducting core were thought to be one of the most important factors that affected the critical current density of the SmO_0.7F_0.3FeAs wires.