Multiple-State Storage Capability of Stacked Chalcogenide Films （Si16Sb33Te51/Si4Sb45Te51/Si11Sb39Te50） for Phase Change Memory

The multiple-state storage capability of phase change memory （PCM） is confirmed by using stacked chalcogenide films as the storage medium. The current-voltage characteristics and the resistance-current characteristics of the PCM clearly indicate that four states can be stored in this stacked film structure. Qualitative analysis indicates that the multiple-state storage capability of this stacked film structure is due to successive crystallizations in different Si-Sb-Te layers triggered by different amplitude currents.     

取代基效应(SCS)与乙烯-α-烯烃共聚物的序列结构Ⅲ.定量分析

本文在分析乙烯-α-烯烃共聚物序列结构时,把代表共单体反接单元的亚甲基(CH₂)βγ和γδ分别归属给了二元组VV和三元组EEV。与此同时,CH₂-δδ和δδ⁺归属给了二元组EE。表征乙烯长序列的CH₂-δ⁺δ⁺分属二元组EE和三元组EEE,对应峰强度在EE和EEE之间的分配是处理序列分布的关键。在本文中运用序列结构的Bovey关系和Randall统计进行演算,求得了修正值△的数学表达式,严格解和近似解。在规则链条件下得到的近似解与G.J.Ray的结果完全相同。当共单体含量较少时,谱峰强度Iδ⁺δ⁺的分配接近相等。在二元组和三元组的水平上,乙烯-α-稀烃共聚物的¹³C NMR谱中共有十三个峰,属于CH₂的有十个,属于CH的有三个。利用这些谱峰的强度数据可以建立一套计算公式,由此提供共聚物序列结构的全部信息。因此这是一个研究乙烯-α-烯烃共聚物序列结构的普适方法。     

ICP－AES法测定富锗酵母中微量元素

本文采用美国ＬｅｅｍａｎＬａｂｓ公司中阶梯光栅光谱仪测定了人工培养的富锗酵母中高含量锗及镁、铜、锌、铁、钾、钠等微量元素，研究了富锗样品的前处理方法，样品加标回收率在９０％－１０３％之间，测量相对标准偏差：锗１０％，镁、铜、锌、铁、钾、钠等元素小于７％。     

醇体系中合成CuGaS2纳米晶及其形貌演变

以CuCl2·2H2O,自制的GaCl3和(NH2)2CS为原料,在乙二醇体系中合成了花状结构的CuGaS2纳米晶．产物分别用X射线粉末衍射仪、透射电子显微镜、场发射扫描电子显微镜、高分辩透射电子显微镜和X射线光电子能谱仪进行了表征．实验结果表明,220℃反应24 h得到均匀的花状纳米结构CuGaS2,它是由厚度80-100 nm的片晶组成．同时,通过反应时间的控制,可以清楚的看到由纳米颗粒到纳米球以及花状纳米结构的演变过程．另外,研究了反应温度、反应时间、溶剂等对产物和形貌的影响．此外,对花状结构纳米晶的生长机理进行了初步的探讨．室温荧光光谱表明,随粒径的降低,发光位发生了部分蓝移．     

三角B\''{e}zier曲面和四边B\''{e}zier曲面之间的相互转化

B\'{e}zier曲面有两种不同的形式:三角B\'{e}zier曲面和四边B\'{e}zier曲面,它们有着不同的基底和不同的几何拓扑结构, 但是它们也有很多共同的性质,因此三角B\'{e}zier曲面和四边B\'{e}zier曲面之间的相互转化就成为CAGD 里一个重要研究课题.在本文中, 我们用函数复合的方法实现两者之间的相互转化.被复合的两个函数, 一个用Polar形式表示,另一个用常见的Bernstein基形式表示.     

High—Efficiency Organic Double—Quantum—Well Light—Emitting Devices Using 5,6,11,12—Tetraphenylnaphthacene Sub—monolayer as Potential Well

The double-quantum-well organic light-emitting devices of indium-tin-oxide (ITO)/NPB (50nm)/rubrene (0.05nm)/NPB (4nm)/rubrene (0.05nm)/Alq3 (50nm)/LiF (0.5nm)/Al were fabricated, in which N,N-bis-(1-naphthyl)-N,N‘-diphenyl-1,1‘-biphenyl-4,4‘‘‘‘‘‘‘‘-diamine (NPB) is used as a barrier potential or hole transport layer, tris (8-hydroxyquinoline) aluminium (Alq3) used as electron transport layer, and 5,6,11,12-tetraphenylnaphthacene (rubrene) as a potential well and emitter. The brightness can reach 18610cd/m^2 at 13V. The maximum electroluminescent efficiency of the device was 6.61cd/A at 7V, which was higher than that of common dope-type devices. In addition, the electroluminescence efficiency is relatively independent of the drive voltage in the range from 5 to 13V.     

First Total Synthesis of 12-Hydroxy-13-methylpodocarpa-9, 11, 13-trien-3-one

12-Hydroxy-13-methylpodocarpa-9, 11, 13-trien-3-one 9 was isolated from the twigs ofCroton salutaris1. Many diterpenes exhibit significant bioactivities, such as antibac-terial and antitumour and 9 has a rare structure. In order to study the relationshipb…