醋酸甲羟孕酮与β-环糊精包络作用的光谱研究及应用

用紫外吸收、荧光光谱法对水溶液中β－环糊精（β－ＣＤ）与醋酸甲羟孕酮（ＭＡ）主客体包络物的光谱行为进行了研究．利用改进的Ｂｅｎｅｓｉ－Ｈｉｌｄｅｂｒａｎｄ法测定了包络物的形成常数，初步探讨了某些水溶性一元醇的引入对该包络物形成及荧光性质的影响，并提出了测定ＭＡ的高灵敏度荧光光度新方法，方法的最低检出限为８．９×１０－９ｍｏｌ·Ｌ－１．用该法测定样品中ＭＡ的结果令人满意，回收率为９７．９％～１０１．７％，平均回收率为９９．９％（ｎ＝５）     

Determination of lead in environmental reference materials (plant materials) by slurry-ETA-AAS

Slurry-ETA-AAS is used to determine lead in plant materials. The stability of the slurry was studied and it was shown that, when NH₄H₂PO₄ modifier is added, the shape of the time resolved absorbance signal for the sample and the standards is similar and the calibration line obtained using aqueous standards is parallel to the standard addition line. Results obtained for several reference materials (lead contents between 6.1 and 64.4 g/g) were in good agreement with the certified value, the relative standard deviation being 3–9%.     

Use of Temperature- and Humidity-Dataloggers in Food Engineering

The use of dataloggers in food engineering is discussed in two examples. The first example describes the measurement of temperature and humidity in a bulk tank car during transport and unloading. In the case of wheat flour the relative humidity in the air raises from about 80% r.h. to values near 100% r.h. at the air compressors for pneumatical unloading start working. The second example shows the use of the datalogger in education on heat transfer. The device was fixed in an ice cream sample which was placed in a store at –25°C. The measured hardeningtime agrees well to theoretical heat transfer calculation.This revised version was published online in November 2005 with corrections to the Cover Date.     

从自旋冰到自旋液态的渡越——结构与磁性质的演化

使用固相反应法得到了Ho_2-xTb_xTi₂O₇（x=0,05,1,15,2）系列多晶样品.X射线衍射（XRD）实验与2K到300K温度区间的直流磁化率测量结果显示,随着Tb即是x的增加,体系由自旋冰Ho₂Ti₂O₇向自旋液Tb₂Ti₂O_{7关键词： 自旋冰 自旋液体 自旋阻挫 晶格结构}     

磁单极子进展概述

自磁单极子概念被狄拉克提出以来,不管是理论还是实验物理学家都一直在努力寻找,但迄今仍然没能找到它们存在的确凿证据.最近,一些凝聚态物理学家声称在动量空间以及自旋冰材料中找到了磁单极子存在的有力证据,并通过磁单极子的集体激发行为解释了一些新颖的物理现象.这使得磁单极子艰难的探索之路出现了一丝新的曙光.作为电动力学教学内容的补充,本文拟把磁单极子的最新进展做一个概述,让大学生对此有一个全面的认识,从而激发他们学习和科研的兴趣.     

黄河河道冰水情定点连续自动检测及数据分析

根据黄河中上游流域冰水情监测以及预防凌汛灾害的需求,设计了一种适合黄河河道的冰水情自动测报系统.该系统由基于空气、冰与水电阻特性差异的冰层厚度传感器、DS18B20的温度梯度传感器以及智能处理仪构成.采用该系统在内蒙托克托县黄河河道进行了黄河封冻期河道冰层厚度连续监测试验,获取了大量的现场实测数据,对采样数据进行分析,提出了判别冰层厚度的平均滤波算法,实现了对冰层生消变化全过程的自动监测.     

Estimates of Europa’s ice shell thickness and strain rate from flanking cracks and bulge along Ridge R

Europa, the second Galilean satellite outward from Jupiter, has an outer layer of water of about 100 km thick and an outmost ice shell. The thickness of the ice shell is very important in understanding Europa’s habitability and thermal history, but estimates from different studies are very inconsistent, ranging from 0.2 to 30 km. Here we obtain an estimate of the ice shell thickness from locations of flanking crack and forebulge along Ridge R. Considering the water’s heating process to nearby ice shell in the crack, a flexure model is applied and it suggests the thickness of an ice shell to be 500–1500 m without a convective layer. Compared with previous studies using the same method but ignoring the water’s heating process, the rationality and accuracy have been improved dramatically in our results. We also get some constraints on the strain rate and the characteristic temperature T _c, which defines the base of the elastic layer.