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81.
The reaction of copper(II) ions with 2,2′-dipyridyl-2-pyridylhydrazone (DPPH) has been studied. Two copper complexes were found to be formed. One at pH 6.5 to 8.5 and the other at pH 11.9 to 12.6 with molecular extinction coefficients of 1.9 × 104M?1 · cm?1 at the absorption maximum of 478 nm and 3.8 × 104M?1 · cm?1 at 448 nm, respectively. A sensitive spectrophotometric procedure for the determination of copper at less than a 1-ppm level is proposed. 相似文献
82.
83.
The thermal functions S0T, -(G0T-H0O)/T and (H0T-H0O) have been calculated from structural and spectroscopic data for the gaseous organometallics C5H5BeX (X = Cl, Br and BH4), C5H5MX3 (M = Ti and Ge; X = Cl, Br and I) and CH3TiX3 (X = Cl, Br and I). The rotational barriers of the C5H5 and CH3 groups have been evaluated and discussed. 相似文献
84.
S. Iwama N. Satomi M. Yamanaka S. Goto T. Ishimura H. Ito 《International Journal of Infrared and Millimeter Waves》1981,2(6):1199-1208
A high-power CW 27.972 m water vapor laser has been constructed in order to use as a light source of an interferometer for plasma diagnostics. The laser consists of 220 cm length and 2.0 cm small bore Pyrex glass discharge tube, semi-confocal resonator and Michelson coupler. From the measurement of cavity detuning curves, it is found that two waveguide modes, EH11 and EH21 oscillate. The increase of the output power is found to become more than seven times larger by adding He(50%)–H2(50%) mixed gas. Under the optimum condition, the maximum output power of 65 mW or the output power per unit cavity volume of 83 W/cm3 is obtained. 相似文献
85.
86.
在利用迈克尔逊干涉原理测量金属热膨胀系数的基础上,运用CCD成像系统取代原有观察屏,更利于观察并记录数据。 相似文献
87.
实验验证了一种通过将氧化石墨烯分散液沉积在长周期光纤光栅的全光控制的相关研究。通过外加的垂直泵浦光的作用,氧化石墨烯吸收泵浦光产生热量,改变长周期光纤光栅的包层模式的相位差,由于热膨胀的作用改变了氧化石墨烯所覆盖部分的光栅周期,使得谐振谱发生了移动,其最大调制深度可达10.6 dB,谐振谱最大可红移12.8 nm。通过实验发现,沉积相同浓度氧化石墨烯分散液的次数影响实验结果,通过在相同光栅的相同位置分别沉积三次,发现沉积三次可以在光纤表面获得更加均匀的氧化石墨烯膜,进行了时间响应的测试,其中沉积三次后的长周期光纤光栅的响应速度可达0.61 ms,沉积多次氧化石墨烯分散液可以在光纤表面沉积得更加平整均匀,从而获得更大的导热性能。 相似文献
88.
对平行平板双光路横向剪切干涉仪的装调进行了研究,提出了一种矫正两个平行平板之间角度误差的方法.输出激光的波前采用Zernike多项式拟合,经过理论推导,发现两个方向差分波前求解出的倾斜像散之差与平行平板的角度误差存在线性关系,利用两个方向倾斜像散之差来矫正两个平行平板之间的角度误差.在平行平板横向剪切干涉仪的装调过程中使两个方向差分波前的倾斜像散之差为零即可以使两个方向的平行平板之间的角度误差值为零.进一步地从实验上证明了这个线性关系,对于所用的实验系统,当离焦像差为-3.224 7±0.001 8,两个方向差分波前的倾斜像散之差波动范围为±2.0×10^-3时,平行平板的角度误差可以控制在8.82″之内,高阶像差对平行平板的角度误差调节精度的影响约为1.63″.该方法具有装调简单、精确度高,易于流程化操作的优点. 相似文献
89.
O. Pottiez Author Vitae B. Ibarra-Escamilla Author Vitae Author Vitae R. Grajales-Coutiño Author Vitae Author Vitae 《Optics & Laser Technology》2010,42(2):403-408
In this paper we study theoretically and experimentally a wavelength-tuneable Sagnac birefringence filter. The device is a Sagnac interferometer including a symmetric fibre coupler and a length of high-birefringence fibre in the loop. A wave retarder is inserted at each end of the birefringent fibre for absolute wavelength tuning. We show theoretically that wavelength tuning through wave plate orientation ensuring constant amplitude of the filtering function is possible only if a minimum of two wave retarders are included in the setup. The position of the transmission peaks then varies linearly with the angle of one of the retarders and can be adjusted over one entire channel spacing. This happens only when a quarter-wave retarder and a half-wave retarder are used, if the former is oriented at 45° with respect to the fibre birefringence axes, while the orientation of the latter serves as the adjustment parameter. The theoretical predictions are confirmed by the experimental results. 相似文献
90.
A new type of phase-shifting interferometer was presented by rotating an azo-polymer film with photo-induced optical anisotropy in the light path of orthogonal polarization interferometry. By changing the angle of the optical axis of the azo-polymer film, four phase-shifted fringe patterns were obtained, from which phase difference between orthogonal polarized light could be calculated. The polarization states and the formation of the interferograms were analyzed theoretically using Jones matrix calculations and the experimental verification of the proposed method was also given. This method has a simple optical configuration which utilizes commercially available polarization devices and anisotropic azo-polymer film of low cost. The phase-shifting interferometer also demonstrates a new application of azo-polymer film. 相似文献