Promotion of oxidative desulfurization performance of model fuel by 3DOM Ce-doped HPW/TiO2 material

Phosphotungstic acid (HPW) supported on Ce-doped three-dimensional ordered macroporous (3DOM) TiO₂ catalysts are studied in catalytic oxidation desulfurization (ODS) of model oil. The structural and textural of as-synthesized catalysts are characterized by N₂ adsorption, XRD, Raman spectroscopy, SEM-EDS, TEM, FT-IR, XPS, UV–Vis and ICP. These results upheld the existence of periodically arranged macroporous structure of catalyst, with Keggin-type of HPW dispersed homogeneously on TiO₂ matrix. Among these 3DOM Ce-doped HPW/TiO₂ materials, catalyst with 15 wt.% cerium dosage exhibits best ODS performance, which oxidized 99.8% of dibenzothiophene (DBT) into corresponding sulfone within 40 min. The excellent ODS performance of 3DOM Ce-doped HPW/TiO₂ catalyst is related to the common influence of more oxygen vacancies produced by electron transformation between Ce³⁺ and Ce⁴⁺. The chemisorbed oxygen on the surface catalyst will facilitate the selective oxidation of sulfides to sulfones. Moreover, the 3DOM structure of catalyst will further promote the mass transfer of reactants and products on the pore channel. The as-prepared catalyst shows excellent reusability in the ODS system, no obviously decrease in catalytic activity even after 6 runs.     

基于两平行线及其线上三点的摄像机标定方法

在大视场交通监控摄像机的标定中,由于不便于放置大尺寸标定靶标,常采用交通标线构成的特定几何图形替代标定靶标,但许多交通场景仅有一组平行的车道分界交通标线,难以获得传统标定方法所需的标定约束条件。针对此类交通场景,选取两平行交通标线和其中一条线上的三点作为标定参考物,依靠其中一条线上三点在单幅图像中的像素坐标、三点间的两个距离值及平行线间距作为约束条件来完成摄像机的标定。建立了图像坐标系与世界坐标系之间新的换算关系,推导出了摄像机内外参数的求解公式,探讨了旋转角对测量误差的影响。实验结果表明,在约束条件不足的情况下能够获得较好的摄像机参数近似解,沿道路方向上的测距精度优于对比文献的结果,具有标定参考物选取容易、操作简便、几何约束条件少等优点,适用于交通监控系统中大视场摄像机的快速标定场合。     

Flexible sheet with radiophotoluminescence glass beads for remotely monitoring high beta-surface-contamination

A flexible sheet was made with radiophotoluminescence (RPL) glass beads on an experimental basis for visualization of high beta-surface-contamination. A simple RPL observation system for remote contamination monitoring was constructed with a homemade UV floodlight and a commercially available digital camera with supplementary optical lenses and filters. In preliminary experiments, RPL images were well observed with the digital camera of the present system. Their precise RPL intensity was determined after the correction of nonlinear response of the camera. It was expected from experiments that RPL images of beta-surface-contamination could be quantitatively evaluated through calibration, i.e., the conversion of camera images to dose data on the sheet-type glass dosimeter.     

Digital holographic cameras and data processing for remote monitoring and measurements of mechanical parts

Fast growing technology and requirements for testing of different types of materials and devices require new methods and systems for investigation of their parameters. Among the quantities of high interest are shape, deformation, roughness, local materials constants, displacement, and strain fields of elements under load. In the paper, we present novel solutions for digital holographic cameras, which allow for remote monitoring and measurement of the above mentioned quantities at small mechanical objects or at restricted areas of interest at big structures. The systems have compact design, “black box” measurement approach, and allows for fast and accurate measurements performed directly at the element and often in outdoor environment. The principles of digital and optoelectronic reconstruction and phase manipulation are described together with the exemplary measurement results obtained by means of the cameras presented.     

高速扫描相机时间测量不确定度分析

以国内普遍使用的SJZ-30型高速扫描相机为例,用精测转速方法的结果处理数据,转速测量相对合成不确定度小于0.1%,时间间隔测量的相对扩展不确定度为0.2%.扫描速度在像面上的位置误差,采用"中值扫描速度",可予以校正.同时讨论了进一步降低转速测量不确定度和位置误差的方法.     

Kinematic Analysis of Robotic Bevel-Gear Trains: An Application of Network Model Approach

The network model approach for rigid and multi-rigid body systems developed recently [1,2] can also be used conveniently in formulating system equations or equations of motion of three-dimensional mechanical systems of interconnected rigid bodies. In this article, this method is further elaborated for establishing only the kinematics of spatial robotic bevel-gear trains. However the dynamic analysis of such systems using the same method is also possible and will be taken up in a future publication.     

Remarks on the star-triangle relation in the Baxter-Bazhanov model

We show that the restricted star-triangle relation introduced by Bazhanov and Baxter can be obtained either from the star-triangle relation of the chiral Potts model or from the star-square relation proposed by Kashaev, Mangazeev, and Stroganov, and give a response to a guess of Bazhanov and Baxter.     

一种时间分辨三通道软X射线光谱仪

报道了时间分辨的三通道软X射线光谱仪研制工作，重点介绍了研制的三通道能谱仪的工作原理以及210 eV，420 eV和900 eV三个能区的设计参数，谱仪在上海神光Ⅱ高功率激光器三倍频实验中进行了多次实时考核，取得较好实验结果，将多道平面镜、滤光片成功配接于高时间分辨X射线条纹相机上，使该谱仪在亚千电子伏能区内，可同时进行三个波段软X射线的时间和空间分辨测量，提供的实验结果也表明：X射线平面镜结合滤光片的分光技术可应用于高时间分辨的X射线条纹相机上，从而获得高达10 ps的时间分辨. 关键词： 软X射线条纹相机 平面镜 滤光片 掠入射     

摄像机标定技术在活塞视觉检测与分选中的应用研究

在机器人视觉检测及自动化分捡中,准确地校正摄像机镜头畸变对获取物体精确图像及确定物体准确位置具有重要意义。采用了带有径向畸变的小孔摄像机模型及基于线段斜率的标定方法。在标定过程中,应用线性算法求解出了镜头的径向畸变系数。实验表明,采用的标定方法简捷有效,其标定结果能够满足研究需要。