全文获取类型
收费全文 | 2769篇 |
免费 | 440篇 |
国内免费 | 259篇 |
专业分类
化学 | 1113篇 |
晶体学 | 39篇 |
力学 | 147篇 |
综合类 | 92篇 |
数学 | 315篇 |
物理学 | 1762篇 |
出版年
2024年 | 12篇 |
2023年 | 41篇 |
2022年 | 128篇 |
2021年 | 140篇 |
2020年 | 106篇 |
2019年 | 75篇 |
2018年 | 75篇 |
2017年 | 137篇 |
2016年 | 155篇 |
2015年 | 103篇 |
2014年 | 157篇 |
2013年 | 158篇 |
2012年 | 147篇 |
2011年 | 178篇 |
2010年 | 157篇 |
2009年 | 150篇 |
2008年 | 154篇 |
2007年 | 182篇 |
2006年 | 169篇 |
2005年 | 136篇 |
2004年 | 158篇 |
2003年 | 127篇 |
2002年 | 149篇 |
2001年 | 78篇 |
2000年 | 58篇 |
1999年 | 55篇 |
1998年 | 64篇 |
1997年 | 27篇 |
1996年 | 24篇 |
1995年 | 24篇 |
1994年 | 32篇 |
1993年 | 18篇 |
1992年 | 17篇 |
1991年 | 12篇 |
1990年 | 8篇 |
1989年 | 10篇 |
1988年 | 11篇 |
1987年 | 5篇 |
1986年 | 8篇 |
1985年 | 3篇 |
1984年 | 5篇 |
1983年 | 5篇 |
1982年 | 3篇 |
1981年 | 1篇 |
1979年 | 1篇 |
1975年 | 1篇 |
1974年 | 2篇 |
1973年 | 1篇 |
1971年 | 1篇 |
排序方式: 共有3468条查询结果,搜索用时 31 毫秒
101.
利用二氧化碳传感器测定钙尔奇D片中的钙含量,解决二氧化碳含量不好直接测定的问题,帮助学生提升定量认识,同时体验多种数据记录与处理方式,感受信息技术的魅力。 相似文献
102.
A. Kamitani T. Takayama A. Tanaka S. Ikuno 《Physica C: Superconductivity and its Applications》2010,470(20):1189-1192
The inductive method for measuring the critical current density jC in a high-temperature superconducting (HTS) thin film has been investigated numerically. In order to simulate the method, a non-axisymmetric numerical code has been developed for analyzing the time evolution of the shielding current density. In the code, the governing equation of the shielding current density is spatially discretized with the finite element method and the resulting first-order ordinary differential system is solved by using the 5th-order Runge–Kutta method with an adaptive step-size control algorithm. By using the code, the threshold current IT is evaluated for various positions of a coil. The results of computations show that, near a film edge, the accuracy of the estimating formula for jC is remarkably degraded. Moreover, even the proportional relationship between jC and IT will be lost there. Hence, the critical current density near a film edge cannot be estimated by using the inductive method. 相似文献
103.
104.
《高分子科学杂志,A辑:纯化学与应用化学》2013,50(11):1221-1232
Abstract trans‐1,4‐Polybutadiene (tPBD) networks crosslinked free radically with dicumyl peroxide (DCP) were reinforced by in situ silica formed in a two‐step sol–gel technique. Changing the degree of crosslinking by changing the amount of DCP, or changing the amounts of the sol–gel components [tetraethoxysilane (TEOS) and dibutyltin diacetate (DBTDA)], changed the silica generated with regard to the amount precipitated, particle size, and degree of dispersion. Stress–strain measurements in continuous extension indicated good reinforcement, even at relatively low amounts of silica. Differential scanning calorimetry (DSC) indicated decreases in heat of crystallization with increases in the amounts of silica, but thermogravimetric analysis showed initial decomposition temperatures (IDT) remained relatively constant. Suggestions are made regarding interpretation of these properties in terms of the composite morphologies. 相似文献
105.
介绍了钛材碱洗脱脂除油和酸洗除去氧化皮的原理和方法,重点阐述了钛材碱洗除油和酸洗除去氧化皮的工艺条件、工艺流程和设备. 相似文献
106.
107.
光伏太阳能电池生产过程中的污染问题 总被引:2,自引:0,他引:2
日益壮大的光伏产业正在为人类发展作出积极的贡献.采用光伏发电来代替传统的发电技术,将会减少89%的空气污染.然而,在这个倡导绿色环境的时代,光伏器件生产引起的环境、健康和安全(EHS)问题也日益引起社会各界的广泛关注.认清光伏产品在生产过程中污染的真相对维持光伏产业的可持续发展有着相当重要的意义.本文综述了常见太阳能电池的EHS问题,并提出了可以减少污染的有效途径;采用生命周期评估(LCA)方法进一步比较了各种太阳能电池生产过程中污染物的排放量数据. 相似文献
108.
Yuntao Dai Jaap van Spronsen Geert-Jan Witkamp Robert Verpoorte Young Hae Choi 《Analytica chimica acta》2013
Developing new green solvents is one of the key subjects in Green Chemistry. Ionic liquids (ILs) and deep eutectic solvents, thus, have been paid great attention to replace current harsh organic solvents and have been applied to many chemical processing such as extraction and synthesis. However, current ionic liquids and deep eutectic solvents have still limitations to be applied to a real chemical industry due to toxicity against human and environment and high cost of ILs and solid state of most deep eutectic solvents at room temperature. Recently we discovered that many plant abundant primary metabolites changed their state from solid to liquid when they were mixed in proper ratio. This finding made us hypothesize that natural deep eutectic solvents (NADES) play a role as alternative media to water in living organisms and tested a wide range of natural products, which resulted in discovery of over 100 NADES from nature. In order to prove deep eutectic feature the interaction between the molecules was investigated by nuclear magnetic resonance spectroscopy. All the tested NADES show clear hydrogen bonding between components. As next step physical properties of NADES such as water activity, density, viscosity, polarity and thermal properties were measured as well as the effect of water on the physical properties. In the last stage the novel NADES were applied to the solubilization of wide range of biomolecules such as non-water soluble bioactive natural products, gluten, starch, and DNA. In most cases the solubility of the biomolecules evaluated in this study was greatly higher than water. Based on the results the novel NADES may be expected as potential green solvents at room temperature in diverse fields of chemistry. 相似文献
109.
Antonio Calvo-López Eva Arasa-Puig Mar Puyol Joan Manel Casalta Julián Alonso-Chamarro 《Analytica chimica acta》2013
The construction and evaluation of a Low Temperature Co-fired Ceramics (LTCC)-based continuous flow potentiometric microanalyzer prototype to simultaneously monitor the presence of two ions (potassium and nitrate) in samples from the water recycling process for future manned space missions is presented. The microsystem integrates microfluidics and the detection system in a single substrate and it is smaller than a credit card. The detection system is based on two ion-selective electrodes (ISEs), which are built using all-solid state nitrate and potassium polymeric membranes, and a screen-printed Ag/AgCl reference electrode. The obtained analytical features after the optimization of the microfluidic design and hydrodynamics are a linear range from 10 to 1000 mg L−1 and from 1.9 to 155 mg L−1 and a detection limit of 9.56 mg L−1 and 0.81 mg L−1 for nitrate and potassium ions respectively. 相似文献
110.
3D打印技术制备生物医用高分子材料的研究进展 总被引:1,自引:0,他引:1
3D打印技术能够根据不同患者需要,快速精确制备适合不同患者的个性化生物医用高分子材料,并能同时对材料的微观结构进行精确控制.因此,这种新兴的医用高分子材料制备技术在未来生物医学应用(尤其是组织工程应用)中具有独特的优势.近年来,对于3D打印技术制备生物医用高分子材料的研究开发受到了越来越多的关注.不同的生物相容高分子原料被应用于3D打印技术,而这些3D成型高分子材料被用于体外细胞培养,或动物模型的软组织或硬组织修复中.本文主要介绍了近年来3D打印技术在生物医用高分子材料制备中的研究进展,并对该领域的未来应用和挑战进行了展望. 相似文献