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11.
An energy-dependent partitioning scheme is explored for extracting a small number of eigenvalues of a real symmetric matrix with the help of genetic algorithm. The proposed method is tested with matrices of different sizes (30 × 30 to 1000 × 1000). Comparison is made with Löwdin’s strategy for solving the problem. The relative advantages and disadvantages of the GA-based method are analyzed 相似文献
12.
We present a model arising from the thermal modelling of two metal casting processes. We consider an enthalpy formulation for this two‐phase Stefan problem in a time varying three‐dimensional domain and consider convective heat transfer in the liquid phase. Then, we introduce a weak formulation in a fixed domain, by means of a suitable transformation. Existence of solution is obtained by applying an abstract theorem. The proof of this theorem is done by taking an implicit discretization in time together with a regularization. By passing to the limit in the regularization parameter and in the time step, we obtain the existence of solution of the continuous problem. Copyright © 2005 John Wiley & Sons, Ltd. 相似文献
13.
The aggregation of dansyl chloride (DNS-Cl) in acetone has been studied in detail by steady-state fluorescence techniques.It has been demonstrated that DNS-Cl is stable in acetone during purification and aggregation study processes.The aggregates are not solvolyzed in acetone,and do not take part n any chemical reactions either.It has been found that DNS-Cl tends to aggregate even when its concentration is much lower than its solubility in acetone.The aggregation is reversible,and both the aggregation and the deaggregation are very slow processes.Introduction of SDS has a positive effect upon the formation and stabilization of the aggregates. 相似文献
14.
提出用发展中的硅微机械加工技术设计制作硅一体化薄膜微电极器件.这类微电化学器件具有微电极所特有的全部优点,而且由于结构上的一体化,便于器件整体的微型化和集成化.试用薄膜微电极器件电流法常温直接检测CO2气体,取得了满意的结果。设想通过器件三维构型设计的改进和完善,器件工作的长期稳定性可望进一步提高. 相似文献
15.
Fabio Schoen 《Journal of Global Optimization》1994,4(1):17-35
In this paper a new algorithm is proposed for global optimization problems. The main idea is that of modifying a standard clustering approach by sequentially sampling the objective function while adaptively deciding an appropriate sample size. Theoretical as well as computational results are presented. 相似文献
16.
T. Drglin 《Accreditation and quality assurance》2003,8(3-4):130-133
A validation procedure based on the ISO/IEC 17025 standard was used to demonstrate the long-term stability of a calibration
process and to assess the measurement uncertainty of a standard test method for optical emission vacuum spectrometric analysis
of carbon and low-alloy steel (ASTM E 415–99a). The validation was used to provide documented evidence that the selected method
fulfils the requirements and that the method is ”fit for purpose”. A test for drift was applied to determine statistically
whether the analytical results vary systematically with time. The accuracy and traceability of the optimised method were tested
by an analysis of closely matched matrix certified reference materials (CRMs). The measurement uncertainty estimations took
account of the precision study, the bias and its uncertainty, and the qualification of uncertainties not considered in the
overall performance studies.
Received: 2 November 2002 Accepted: 2 January 2003
Acknowledgement The author expresses gratitude to Dr. Aleš Fajgelj for helpful discussions during the 3rd Central European Conference on Reference Materials and Measurements.
Presented at CERMM-3, Central European Reference Materials and Measurements Conference: The function of reference materials
in the measurement process, May 30–June 1, 2002, Rogaška Slatina, Slovenia
Correspondence to T. Drglin 相似文献
17.
18.
An analytical result is not considered to be complete without a statement of the measurement uncertainty associated with
it. Evaluation of measurement uncertainty is therefore an essential part of every determination. In the present study the
measurement uncertainty of the result of determination of selenium in the reference material Seronorm Trace Elements Serum
was studied. The combination of a digestion procedure using sulfuric acid, V2O5 in H2SO4 and hydrogen peroxide and the continuous flow approach of hydride generation atomic fluorescence spectrometry (HG-AFS) detection
was used for selenium determination. The total uncertainty budget was calculated with the help of the GUM Workbench program,
in which computations follow the rules of the ’ISO guide to the expression of uncertainty in measurement’. The major sources
of uncertainty were found to be due to the recovery of the procedure, measurement of peak heights and the purity of Na2SeO3. A selenium mass fraction of 77.1±4.8 ng/g (with a coverage factor of 2.1, 95% probability) was determined, which is comparable
with the recommended value of 80 ng/g.
Received: 13 September 2002 Accepted: 23 December 2002
Acknowledgements We would like to thank Tinkara Buˇcar, B.Sc. for useful discussions and the IAEA Vienna, for financial support of the project
11553/RO.
Presented at CERMM-3, Central European Reference Materials and Measurements Conference: The function of reference materials
in the measurement process, May 30–June 1, 2002, Rogaška Slatina, Slovenia
Correspondence to V. Stibilj 相似文献
19.
We develop two implementable algorithms, the first for the solution of finite and the second for the solution of semi-infinite min-max-min problems. A smoothing technique (together with discretization for the semi-infinite case) is used to construct a sequence of approximating finite min-max problems, which are solved with increasing precision. The smoothing and discretization approximations are initially coarse, but are made progressively finer as the number of iterations is increased. This reduces the potential ill-conditioning due to high smoothing precision parameter values and computational cost due to high levels of discretization. The behavior of the algorithms is illustrated with three semi-infinite numerical examples. 相似文献
20.
Microemulsions are becoming increasingly complex systems by containing more sophisticated surfactants, polymers, biomolecules, inorganic nanoparticles, etc. The detailed understanding of such more complex systems requires increasingly more refined and comprehensive characterisation. This is typically done by the combination of complementary techniques and is aided by the fact that several experimental methods have been improved (such as electron microscopy) in recent times, new ones have become available (such as fluorescence correlation spectroscopy), and the theoretical understanding of structural data is advancing. 相似文献