成都中科普瑞净化设备有限公司

正中国科学院高新产业|中国科学院领先技术ISO9001质量管理体系认证ISO14001环境管理体系认证国家高新技术企业(GR200851000218)国家863计划、支撑计划支持企业成都中科普瑞净化设备有限公司是中国科学院全额控股的国家高新技术企业。公司以中国科学院技术力量为依托,自1969年以来,一直专业从事气体纯化技术与设备制造、气体处理工程以及微型反应装置等方面的研究和产     

超声波辅助提取-气相色谱法同时测定湿毒清片中14种有机磷农药残留

建立了超声波辅助提取-气相色谱法同时检测湿毒清片中14种有机磷农药残留的方法。样品采用乙酸乙酯超声提取,通过石墨化炭黑净化,采用气相色谱-火焰光度法(GC-FPD)进行检测。除乐果以外,13种有机磷农药于0.1mg/kg、0.5mg/kg两个加标水平的回收率在80.4%~114.5%之间,相对标准偏差为0.6%~12.4%。方法满足农残分析的要求,可用于湿毒清片中14种有机磷农药残留量的检测。     

固相萃取/气相色谱-质谱法对土壤中有机氯农药的分析及基质效应研究

建立了一种固相萃取/气相色谱-质谱法同时测定土壤中23种有机氯农药的方法,并研究了不同基质效应补偿方式。土壤样品经正己烷∶丙酮(体积比1∶1)提取,弗罗里土小柱净化,采用气相色谱-质谱仪检测。结果发现7种有机氯存在中/强程度的基质效应;在10 mL二氯甲烷∶正己烷(体积比1∶9)+10 mL丙酮∶正己烷(体积比1∶9)为固相萃取的洗脱剂,且脉冲压力为275.8 kPa条件下,可将23种有机氯的基质效应均控制在20%以内。23种有机氯农药在0.4～10μg·mL~(-1)质量浓度范围内线性良好,相关系数(r~2)均不小于0.999 2,检出限为1.0～8.6μg·kg~(-1),定量下限为4.0～34.4μg·kg~(-1);在20、60、100μg·kg~(-1)3个加标水平下空白土壤中的平均回收率为46.3%～127%,相对标准偏差(n=6)为0.68%～15%。采用该方法在某土壤样品中检出α-六六六、γ-六六六、p,p′-DDE、异狄氏剂醛、p,p′-DDT 5种有机氯农药。     

基于超声波换能器的钢筋机械损伤与锈蚀损伤检测及其对比研究

超声导波检测技术有检测耗时少、覆盖范围大等优点.为检测钢筋混凝土结构中钢筋损伤,采用超声波换能器研究不同深度和位置的机械损伤对超声导波传播的影响,建立损伤程度与导波特征关系.通过反射系数C定量分析损伤程度,并结合损伤反射回波判断损伤位置.在钢筋点锈蚀以及均匀锈蚀损伤检测中,锈蚀程度达到最大时,L波实际波速分别为4 738.1 m·s^-1和5 069.7 m·s^-1,以此区分锈蚀损伤与机械损伤,最后基于小波变换的时频分析判断损伤状况.研究成果可为钢筋损伤检测研究提供参考.     

The simulation of ultrasonic beams with a Gaussian beam equivalent point source model

Point Sources and Gaussian beams are used frequently as fundamental building blocks for developing ultrasonic beam models. Both these models have different weaknesses that limit their effectiveness. Here, we will show that one can develop a Gaussian Beam Equivalent Point Source （GBEPS） model that removes those weaknesses and combines the accuracy and versatility of the point source models with much of the speed and well-behaved nature of Gaussian beam models. We will demonstrate the efficiency and versatility of this new GBEPS model in simulating the beams generated from ultrasonic phased arrays, using as few as one Gaussian beam per element of the array. A single element GBEPS model will be shown to be as accurate as a point source model even when substantial beam focusing or steering is present in the array or where the array beam is transmitted through an interface. At the same time the GBEPS model will be shown to be several orders of magnitude faster than the point source model.     

Non-contact evaluation of the resonant frequency of a microstructure using ultrasonic wave

This paper presents a novel non-contact method for evaluating the resonant frequency of a microstructure, Firstly, the microstructure under test is excited by ultrasonic waves. This excitation method does not impose any undefined load on the specimen like the electrostatic excitation and also this is the first actual use of ultrasonic wave for exciting a microstructure in the literature. Secondly, the amplitudes of the microstructure are determined by image edge detection using a Mexican hat wavelet transform on the vibrating images of the microstructure. The vibrating images are captured by a CCD camera when the microstructure is vibrated by ultrasonic waves at a series of discrete high frequencies （〉30 kHz）. Upon processing the vibrating images, the amplitudes at various excitation frequencies are obtained and an amplitude-frequency spectrum is obtained from which the resonant frequency is subsequently evaluated. A micro silicon structure consisting of a perforated plate （192 × 192 μm） and two cantilever beams （76 × 43 μm） which is about 4 μm thickness is tested. Since laser interferometry is not required, thermal effects on a test object can be avoided. Hence, the setup is relatively simple. Results show that the proposed method is a simple and effective approach for evaluating the dynamic characteristics of microstructures.     

血液中声参量测量值与混合定则的比较

本文测量了猪、羊、牛血液的声速和非线性声参量以及血液中水、蛋白质、脂肪的含量.把结果与Apfel和Sehgal声参量混合定则作了比较.指出两个混合定则能够反映血液声参量与其水、蛋白质、脂肪含量的关系,但在精确定量上与实验尚有距离.     

新一代超声波玉石加工机问世

交通部上海船舶运输科学研究所,采用全部国产化元、器件,经过3年多时间的努力,研制成功了新一代超声波玉石加工机,命名为CK-250-1型。前不久在北京通过定型鉴定。 该机由超声波发生器、振动系统和机床部等三大部分组成。超声波发生器:全晶体管化;输出电功率≥250W(连续可调),工作频率为21kHz±2kHz,输出阻抗:45Ω、50Ω、75Ω、100Ω、150Ω五档;有他激、自激两种工作方式,在满负荷功率下可连续工作8小时,功耗不大于450VA。振动系统:由阶梯式压电型振     

超声波原油破乳脱水的声场参数实验研究

本文阐明了超声波原油破乳脱水基本原理,实验研究了超声场参数对脱水率的影响,其中,声强,辐照时间和频率和影响原油脱水率的主要因素,而间歇比,脉冲宽度为次要回素,对本实验系统而言,声场参数有一个最佳值或范围,声强0.65W/cm^2,频率20kHz,间歇比8,脉冲宽度9.7ms,辐照时间5－10min.