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61.
In this study, silver nanoparticle (AgNP) synthesis was carried out using Onosma sericeum Willd. aqueous extract for the first time, with a simple, economical, and green method without the need for any other organic solvent or external reducing or stabilizing agent. A variety of AgNPs, all of different particle sizes, were synthesized by controlling the silver ion concentration, extract volume, temperature, and pH. It was determined that the optimum conditions for AgNP synthesis were 1 mM AgNO3, pH 8, 25 °C, 20 g/200 mL extract, silver nitrate, and extract ratio 5:1 (v/v). The AgNPs were defined using UV-Vis spectroscopy, field emission scanning electron microscopy (FESEM), energy dispersive X-ray analysis (EDAX), transmission electron microscopy (TEM), and X-ray diffraction (XRD). The particle size distribution and zeta potential measurements of the AgNPs were measured using the dynamic light scattering (DLS) technique. It was determined that the AgNPs with a particle size of less than 10 nm showed a higher catalytic effect in the reduction of 2-nitrobenzenamine. It was also found that these nanoparticles had a cytotoxic effect on the MCF-7 breast cancer cell line depending on dosage and time. The resulting IC50 values were between 76.63 µg/mL and 169.77 µg/mL. Furthermore, the biosynthesized AgNPs showed effective antibacterial activity against the Acinetobacter baumannii bacteria. The results of the study showed that synthesized AgNPs can have a promising role in biomedical and nanobiotechnology applications. 相似文献
62.
Na Li Honggang Nie Liping Jiang Guihua Ruan Fuyou Du Huwei Liu 《Journal of separation science》2020,43(15):3146-3163
The structural information and spatial distribution of molecules in biological tissues are closely related to the potential molecular mechanisms of disease origin, transfer, and classification. Ambient ionization mass spectrometry imaging is an effective tool that provides molecular images while describing in situ information of biomolecules in complex samples, in which ionization occurs at atmospheric pressure with the samples being analyzed in the native state. Ambient ionization mass spectrometry imaging can directly analyze tissue samples at a fairly high resolution to obtain molecules in situ information on the tissue surface to identify pathological features associated with a disease, resulting in the wide applications in pharmacy, food science, botanical research, and especially clinical research. Herein, novel ambient ionization techniques, such as techniques based on spray and solid‐liquid extraction, techniques based on plasma desorption, techniques based on laser desorption ablation, and techniques based on acoustic desorption were introduced, and the data processing of ambient ionization mass spectrometry imaging was briefly reviewed. Besides, we also highlight recent applications of this imaging technology in clinical researches and discuss the challenges in this imaging technology and the perspectives on the future of the clinical research. 相似文献
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H. Koch 《Isotopes in environmental and health studies》2013,49(7):233-238
Die Ausnutzung von Quanten- und Teilchenstrahlung zur Analyse von Stoiffverteilungen und Stoffzusammensetzungen hat im vergangenen Jahrzehnt einen beträctlichen und fast unübersehbaren Umfang angenommen. Es werden mögliche Schicerpunkie der zukünftigen Anforderungen an solche Analysenverfahren — die sich aus der modernen Forschung und Entvicklung ergeben — aufgezeichnet und die Anwendungsmöglichkeiten und der Entwicklungsstand spezieller Verfahren besprochen. Insbesondere werden Mönlichkeiten der Gesamtbilddurstellung, der Scanning-Verfahren und der Oberflächenuntersuchungen dünnster Schichten und Fragen der Strukluraufklärung, der chemischen Bindungen bzw. Bindungskonfigurationen diskutiert. 相似文献
64.
Suchinder K. Sharma Shreyas S. Pitale T.K. GunduRao M.S. Qureshi 《Journal of luminescence》2010,130(2):240-248
A simple solution combustion synthesis route for preparation of Cu-doped SrAl4O7 has been described. Average particle size of 33 nm and platelet-like morphology has been observed. ESR studies confirm the presence of Cu in polycrystalline SrAl4O7. Bright-green luminescence under near-UV irradiation arising due to transition between Cu+ levels with microsecond level decay time makes it suitable for application in phosphor converted light emitting diode (LED). TL measurements show broad glow peaks which when deconvoluted indicate activation energies in the range of 0.6-1.1 eV and elucidate the trapping dynamics. 相似文献
65.
From superhydrophobic‐ to superhydrophilic‐patterned poly(vinylidene fluoride‐co‐chlorotrifluoroethylene) architectures as a novel platform for biotechnological applications 下载免费PDF全文
Vanessa F. Cardoso Ana R. Machado Vânia C. Pinto Paulo J. Sousa Gabriela Botelho Graça Minas Senentxu Lanceros‐Méndez 《Journal of Polymer Science.Polymer Physics》2016,54(18):1802-1810
The manufacture of three‐dimensional patterned electroactive poly(vinylidene fluoride‐co‐chlorotrifluoroethylene) microstructures with tailored architecture, morphology, and wettability is presented. The patterned microstructures are fabricated using a simple, effective, low cost, and reproducible technique based on microfluidic technology. These novel structures can represent innovative platforms for advanced strategies in a wide range of biotechnological applications, including tissue engineering, drug delivery, microfluidic, and sensors and actuators devices. © 2016 Wiley Periodicals, Inc. J. Polym. Sci., Part B: Polym. Phys. 2016 , 54, 1802–1810 相似文献
66.
Mingfu Zhang Axel H. E. Müller 《Journal of polymer science. Part A, Polymer chemistry》2005,43(16):3461-3481
In recent years, research on cylindrical polymer brushes (or molecular bottlebrushes) has received significant attention. In this article, we discuss various strategies for their synthesis and the unique properties arising from their regular multibranched structure. Some recent advances in the application of cylindrical polymer brushes are highlighted. Amphiphilic core– shell cylindrical polymer brushes, for example, have been successfully used as single molecular templates for inorganic nanoparticle formation. © 2005 Wiley Periodicals, Inc. J Polym Sci Part A: Polym Chem 43: 3461–3481, 2005 相似文献
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