浅谈电子天平的选择和使用

针对电子天平的选择、使用和维护中容易忽视的问题进行分析和阐述,并提出了解决办法和正确的操作规程。     

气相色谱-正化学源-质谱联用技术测定葡萄和葡萄酒中多种唑类杀菌剂的残留量

建立了可用于葡萄和葡萄酒中20种唑类杀菌剂残留量的分散型固相萃取-气相色谱-正化学离子源质谱分析方法.葡萄和葡萄酒样品分别用乙腈(含1%冰醋酸)和乙酸乙酯提取,分散型固相萃取法净化,由气相色谱-正化学离子源质谱分时段选择离子监测技术进行测定与确证,外标法定量.20种农药在50～1000 μg/L范围内线性均良好; 所有农药的方法定量限(LOQ)均低于10 μg/kg;在3个添加水平(10, 20和40 μg/kg)下,所有农药的回收率均处于71.2%～102.2%之间, RSD≤10.6%.     

水凝胶pH传感器新技术的研究进展

pH值是许多领域的重要监测指标之一.许多化工生产中需要精确、 实时地监测pH值,生物化学和生物医学领域对微环境的pH值监测有较大的需求.水凝胶pH传感器是一种将响应型水凝胶与传感器结合的新型pH值监测技术,由于其具有微型化和智能性等特点,可应用于化学化工、生物医疗、环境检测等领域.本文综述了近年来水凝胶pH传感技术的研...     

水中镉含量的激光诱导击穿光谱高灵敏快速检测

 为了对水中的痕量镉进行高灵敏快速检测,实验采用一种未受污染的薄木片作为基底来吸收水样品,将其晾干后再用激光诱导击穿光谱（LIBS）技术对其进行分析,克服了用LIBS技术直接分析水样品时灵敏度低和稳定性差等问题。实验中选择214.44 nm的镉离子线作为分析线以提高光谱检测的灵敏度,建立了用于定量分析的校正曲线,镉的检出限达到55 μg/L,重复测量的信号相对标准偏差小于5%,单次测量的时间短于5 min。     

基于布拉格光栅的边坡监测实验研究

提出了一种基于分布式光纤光栅的边坡监测与报警系统.根据强度折减法,利用ANSYS软件分析出边坡的软弱面及滑体所在的具体位置,从而在该处安装经过特殊封装的拉线式光纤光栅位移传感器.滑体的位移通过拉线转换为作用在光栅上的应力,而光纤光栅反射波长与应变具有良好的线性关系,因此通过检测光栅反射光的中心波长的偏移量,就可以解调出...     

Proposal of metal bellows-based fiber Bragg grating accelerometer

A metal bellows-based fiber Bragg grating(FBG) accelerometer is proposed and experimentally demonstrated. The optical fiber(containing the FBG) is pre-tensioned,and the two ends of the optical fiber are fixed directly from the shell to the inertial mass. In this design,the FBG is uniformly tensioned to obtain a constant strain distribution over it. By employing this configuration,the FBG always has a sharp reflection characteristic with no broadening in its reflection spectrum during wavelength shifting. Dy...     

Signaling-based path-segment protection in mesh optical networks

Path protections have become increasingly important for current mesh optical networks because fast restorations in generalized multiprotocol label switching(GMPLS) networks are uncertain.However,setting up additional disjoint paths to protect connections leads to more path setup blocking and signaling collisions.We analyze signaling collisions,path blocking and blocking probability,as well as calculate node-to-node blocking probabilities.A signaling-based path-segment protection(PSP) is proposed,which integrates segment protections and path protections as well as enhances the performance of path protections and ring protections.The setup of PSP connections causes less blocking probability than the setup of path protection connections in the simulations.     

Method of sensitivity improving in the non-dispersive infrared gas analysis system

A method of interference correction for improving the sensitivity of non-dispersive infrared (NDIR) gas analysis system is demonstrated. Based on the proposed method, the interference due to water vapor and carbon dioxide in the NDIR NO analyzer is corrected. After interference correction, the absorbance signal at the NO filter channel is only controlled by the absorption of NO, and the sensitivity of the analyzer is improved greatly. In the field experiment for pollution source emission monitoring, the concentration trend of NO monitored by NDIR analyzer is in good agreement with the differential optical absorption spectroscopy NO analyzer. Small variations of NO concentration can also be resolved, and the measuring correlation coefficient of the two analyzers is 94.28%.     

Landsat ETM+在北方农牧交错带土壤沙化监测中的应用

北方农牧交错带是农业种植区与家畜放牧区相互交错的生态过渡地带,是多种生态系统的复合体.由于自然因素和人为因素的影响,农牧交错带土壤沙化问题日益严重,土壤沙化面积逐年扩大,关系到我国北部和中东部生态环境、经济发展和农牧区人民的生活质量等问题,亟需解决.近几年农牧交错带已经成为恢复生态学和全球气候变化研究的热点区域.针对土壤沙化的遥感监测是收集沙化土地现状及其动态变化的重要技术手段,可以为我国北方地区沙化的防治提供重要的实际数据.Landsat ETM+是研究区域尺度较为先进的多光谱遥感系统,应用十分广泛.主要阐述了Landsat ETM+系统特点以及在北方农牧交错带沙化监测中的应用,并且展望了这一系统将来的发展的景.     

基于光纤光栅测量静冰压力的应用研究

静冰压力是指冰层在升温膨胀受到约束的条件下,对约束体产生的压力.它是高寒地区水工建筑物的一种特殊载荷,也是冰科学和冰工程研究中最关键的物理指标之一.主要介绍了几种测量与确定静冰压力的方法及其存在的问题,并着重研究了适合测量静冰压力的光纤光栅传感器的工作原理和结构设计,提出了静冰压力在线检测系统的设计方法,解决了光纤光栅压力传感器的温度补偿问题.通过初步的研究表明,基于光纤光栅的静冰压力传感器具有尺寸小、分布式绝对测量、抗腐蚀能力强、抗干扰、适合于定点连续自动监测等优点.