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991.
Synthesis of novel 4-(4-methylsulfonylphenyl)-3-phenyl-2(3H)-thiazole thione derivatives with functionalized diarylheterocycle pharmacophore as potential COX-2 inhibitors was described. The title compounds were synthesized by cyclocondensation of corresponding dithiocarbamate and 2-bromo-1-(4-methylsulfonylphenyl)ethanone, followed by dehydration with H2SO4. All of the target compounds were characterized by ^1H NMR, IR and mass spectral data. 相似文献
992.
A simple and affordable method for high-throughput DNA extraction from animal tissues for polymerase chain reaction 总被引:1,自引:0,他引:1
We have developed a very simple and inexpensive method for high-throughput DNA extraction from animal tissues. The procedure contains three steps (digestion, heating, and centrifugation) and it is compatible with the 96-well plate format commonly used in polymerase chain reaction (PCR) amplifications. The duration for processing a plate is about 1.5 h; therefore, one researcher can isolate DNA from up to 1000 samples during a single workday. A small piece of tissue (ca. 10-20 mg) yields enough template for at least 50-70 PCR amplifications, as demonstrated by using the processed samples as templates successfully for long distance PCR, multiplex PCR, and randomly amplified polymorphic DNA (RAPD) assay. The application of our method is expected to facilitate studies that require high-throughput DNA isolation for PCR amplification, such as genotyping by microsatellites for mapping and genetic diversity studies, as well as mutant screening in zebrafish. 相似文献
993.
中国工会和企业之间的关系可以分为激烈对抗、消极追随和团结协作三种关系模式。论文构建多主体仿真模型,研究不同企业规模下的三种工会-企业关系模式对企业绩效的影响,探讨不同规模企业绩效的动态演化机制。结果表明:企业规模越小,三种关系模式下员工投入水平和企业绩效波动频率越高、幅度越大,企业越不稳健;企业规模越大,消极追随模式下企业绩效初期出现短暂高绩效的时滞越久;相同规模时,团结协作模式下的企业绩效优于消极追随模式,激烈对抗模式下的企业绩效表现最弱;企业规模越大,团结协作模式的优越性越突出。研究结论可以为工会-企业关系的发展和企业绩效提升提供建设性启示。 相似文献
994.
Effects of Reynolds number and angle of attack on the vortex shedding of a finite swept-back wing are experimentally studied. The cross-sectional profile of the wing is NACA 0012, and the sweep-back angle is 15° The time series signals detected by hot-wire in the wake region shows four distinct behaviors: laminar, subcritical, transitional, and supercritical. The derived Strouhal number curves are significantly different in these four behaviors. In addition, the statistical properties of turbulence, that is, the power spectrum density function, probability density function, correlation coefficient, Lagrangian integral time scales, and length scales are also presented in this paper. 相似文献
995.
A novel and highly selective silver-promoted monobenzylation method was developed to promote synthesis of nonsymmetrical sulfamide-based HIV-1 inhibitors. Microwave-accelerated palladium-catalyzed N-amide arylation- and aminocarbonylation reactions were employed for rapid and reliable compound generation. With this class of inhibitory agents, six active inhibitors were identified, the most potent inhibitor possessing a Ki-value of 20 nM. 相似文献
996.
The morphological stability of a growing faceted crystal is discussed. We argue that the interplay between nonuniformity in supersaturation on a growing facet and anisotropy of surface kinetics derived from the lateral motion of steps leads to a faceted instability. Qualitatively speaking, as long as the nonuniformity in supersaturation on the facet is not too large, it can be compensated for by a variation of step density along the facet, and the faceted crystal can grow in a stable manner. The problem can be modeled as a Hamilton-Jacobi equation for height of the crystal surface. The notion of a maximal stable region of a growing facet is introduced for microscopic time scale approximation of the original Hamilton-Jacobi equation. It is shown that the maximal stable region keeps its shape, determined by profile of the surface supersaturation, with constant growth rate by studying large time behavior of solution of macroscopic time scale approximation. A quantitative criterion for the facet stability is given. 相似文献
997.
M. Salmhofer 《Annalen der Physik》2007,16(3):171-206
A class of continuous renormalization group flows with a dynamical adjustment of the propagator is introduced and studied theoretically for fermionic and bosonic quantum field theories. The adjustment allows to include self–energy effects nontrivially in the denominator of the propagator and to adapt the scale decomposition to a moving singularity, and hence to define flows of Fermi surfaces in a natural way. These flows require no counterterms, but the counterterms used in earlier treatments can be constructed using them. The influence of propagator adjustment on the strong–coupling behaviour of flows is examined for a simple example, and some conclusions about the strong coupling behaviour of renormalization group flows are drawn. 相似文献
998.
In this paper, we consider the classical compound Poisson risk model with two-step premium rate. Using an alternative approach, we find the explicit expressions for the Laplace transforms of joint occupation times over disjoint intervals for this model. The Laplace transforms are expressed in terms of scale functions of L\'{e}vy processes. 相似文献
999.
In this article, the δ‐hyperbolic concept, originally developed for infinite graphs, is adapted to very large but finite graphs. Such graphs can indeed exhibit properties typical of negatively curved spaces, yet the traditional δ‐hyperbolic concept, which requires existence of an upper bound on the fatness δ of the geodesic triangles, is unable to capture those properties, as any finite graph has finite δ. Here the idea is to scale δ relative to the diameter of the geodesic triangles and use the Cartan–Alexandrov–Toponogov (CAT) theory to derive the thresholding value of δdiam below which the geometry has negative curvature properties. © 2007 Wiley Periodicals, Inc. J Graph Theory 57: 157–180, 2008 相似文献
1000.