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991.
Summary. We consider a discontinuous Galerkin finite element method applied in time to a model Volterra equation of the second kind. A residual-based computable Galerkin-error estimate is derived for . This estimate does not explicitly contain the time step and therefore the time step control must be based on a heuristic criterion, the estimate can then be used to demonstrate the integrity, or otherwise, of the finite element solution. After performing some numerical experiments we conclude that this approach is at least competetive with classical discretizations since it is computationally simple to implement, but has the added advantage of reliable error feedback. Received June 25, 1995  相似文献   
992.
Glucose, maltose, sucrose, lactose, ethanol and urea concentrations were monitored simultaneously during the cultivation of Escherichia coli and Saccharomyces cerevisiae by means of enzyme field effect transistors (EnFETs) applying glucose dehydrogenase (GDH), maltase (MAL)/GDH, invertase (INV)/GDH, β-galactosidase (β-GAL)/galactosedehydrogenase (GALDH), alcoholdehydrogenase (ADH)/aldehydedehydrogenase (ALDH), and urease. These enzymes were (co)immobilized on the pH sensitive gates of an eight-FET array. The FET array was integrated in a commercial FIA system.  相似文献   
993.
H?lder continuity up to the free boundary is proved for minimizing solutions if they meet the supporting surface in an angle which is bounded away from zero. The problem is localized by proving the continuity of the distance function, a result which is also true for stationary points. Received: 14 April 1998  相似文献   
994.
995.
996.
Third order nonoscillatory central scheme for hyperbolic conservation laws   总被引:5,自引:0,他引:5  
Summary. A third-order accurate Godunov-type scheme for the approximate solution of hyperbolic systems of conservation laws is presented. Its two main ingredients include: 1. A non-oscillatory piecewise-quadratic reconstruction of pointvalues from their given cell averages; and 2. A central differencing based on staggered evolution of the reconstructed cell averages. This results in a third-order central scheme, an extension along the lines of the second-order central scheme of Nessyahu and Tadmor \cite{NT}. The scalar scheme is non-oscillatory (and hence – convergent), in the sense that it does not increase the number of initial extrema (– as does the exact entropy solution operator). Extension to systems is carried out by componentwise application of the scalar framework. In particular, we have the advantage that, unlike upwind schemes, no (approximate) Riemann solvers, field-by-field characteristic decompositions, etc., are required. Numerical experiments confirm the high-resolution content of the proposed scheme. Thus, a considerable amount of simplicity and robustness is gained while retaining the expected third-order resolution. Received April 10, 1996 / Revised version received January 20, 1997  相似文献   
997.
本文证明了n维布尔矩阵维数的一个新的缺断区间为这一结果扩充了一些已知的结论.  相似文献   
998.
本文报导了聚4-氨基联苯的电化学合成,测定了它的ESR、IR及紫外可见光谱。聚合物在THF、DMF和DMSO中能全部溶解。界面移动法测得聚4-氨基联苯的DMF饱和溶液中正离子的迁移率为1.48×10~(-8)m~2·S~(-1)·V~(-1)。  相似文献   
999.
Seventeen 1-aryl-2,2-dichlorocyclopropanes were examined by using IR, 13C NMR, and mass spectrometry. The data obtained from IR and 13C NMR spectra indicate that the bond strength of carbon-chlorine on the cyclopropane ring and the electron density of that carbon depend on the substituent. The mass fragmentation patterns of compounds in this series resemble those of the dibromo analogues. The fragmentation mechanism is proposed to involve the formation of indenium ion through an electrocyclization.  相似文献   
1000.
本文测定了几种二茂铁有机锡衍生物的119Sn,13C NMR谱。对其中几种衍生物的13C NMR谱进行了归属,从而进一步验证了这类化合物的结构。着重讨论了结构如化合物中取代基X的改变对119Sn化学位移的影响。并对结构如 类化合物N→Sn异侧配位的问题进行了讨论。  相似文献   
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