激光致晶态Ag11In12Te26Sb51相变介质光学常量的研究

研究了结晶度对Ag11In12Te26Sb51相变薄膜光学常数的影响。用初始化仪使相变薄膜晶化，改变晶化参量得到不同的结晶度，当转速固定时，随激光功率的增加，折射率基本随之减小，消光系数先是增大，而后减小；当激光功率固定时，随转速的增大，折射率也随之增大，消光系数也是先增大后减小。非晶态与晶态间的变换、薄膜微结构的变化（包括晶型的转变和原子间键合状态的变化）以及薄膜内残余应力的影响Ag11In12Te26Sb51相变薄膜复数折射率的主要原因。测量了单层膜的透过率和CD－RW相变光盘中Ag11In12Te26Sb51薄膜非晶态和晶态的反射率。     

黄芪成分F3新制剂的工艺监测

对黄芪成分F3新制剂中多糖、蛋白质进行了工艺监测，多糖提取达99．2％，蛋白质≤0．2％，符合黄芪成分F3的质量标准要求，达到了选择最佳提取工艺的目的，结果令人满意。     

High—Efficiency Organic Double—Quantum—Well Light—Emitting Devices Using 5,6,11,12—Tetraphenylnaphthacene Sub—monolayer as Potential Well

The double-quantum-well organic light-emitting devices of indium-tin-oxide (ITO)/NPB (50nm)/rubrene (0.05nm)/NPB (4nm)/rubrene (0.05nm)/Alq3 (50nm)/LiF (0.5nm)/Al were fabricated, in which N,N-bis-(1-naphthyl)-N,N‘-diphenyl-1,1‘-biphenyl-4,4‘‘‘‘‘‘‘‘-diamine (NPB) is used as a barrier potential or hole transport layer, tris (8-hydroxyquinoline) aluminium (Alq3) used as electron transport layer, and 5,6,11,12-tetraphenylnaphthacene (rubrene) as a potential well and emitter. The brightness can reach 18610cd/m^2 at 13V. The maximum electroluminescent efficiency of the device was 6.61cd/A at 7V, which was higher than that of common dope-type devices. In addition, the electroluminescence efficiency is relatively independent of the drive voltage in the range from 5 to 13V.     

Banach空间中广义拟变分包含解的存在与逼近

研究了Banach空间中含k-次增生映射和φ-强增生映射的一类无紧性条件的广义拟变分包含解的存在惟一性与逼近问题，给出了一新的迭代算法和具混合误差的ishikawa迭代序列强收敛到变分包含解的充要条件，所得的结果改进和推广了近期许多相关结果．     

First Total Synthesis of 12-Hydroxy-13-methylpodocarpa-9, 11, 13-trien-3-one

12-Hydroxy-13-methylpodocarpa-9, 11, 13-trien-3-one 9 was isolated from the twigs ofCroton salutaris1. Many diterpenes exhibit significant bioactivities, such as antibac-terial and antitumour and 9 has a rare structure. In order to study the relationshipb…     

关于Tchebycheff—Fourier级数的（H,λ）平均的逼近

我们定义了（Ｈ，λ）求和法，它含有（Ｎ，ｐｎ），（Ｒ＾ｒｎ）和（Ｖｍｎ）求和法。讨论了函数ｆ（ｘ）∈Ｃ＾ｒ［－１，１］（ｒ∈Ｎ０）以及ｆ（ｘ）∈Ｗ＾ｒＨ＾ａ（ｒ∈Ｎ０，０＜ａ＜１）的切比晓夫－富里埃级数的逼近阶。     

算子的拟酉等价性

本文在复的，可析的、无限维Ｈｉｂｅｒｔ空间Ｈ中引进了算子拟酉等价性的概念；获得了几个重要结果。     

11-钨过渡金属杂多阴离子为配体的配合物的热稳定性研究

通式为MW_(11)O_(39)的“不饱和”11-系列杂多阴离子仍然保持了基本的Keggin结构,但失去了其中的一个W-O基团。MW_(11)O_(39)具有很高的反应活性,当其他金属离子(或3A主族元素离子)进入这一空位时,便形成了三元杂多配合物ZMW_(11)和Ln(MW_(11))_2。ZMW_(11)(Z为3A主族金属离子和过渡金属离子)中,11-杂多阴离子起着五齿配体的作用,第六个配位位置被结构水占据,ZMW_(11)基本保持原来的Keggin结构。Ln(MW_(11))_2(Ln为镧系或锕系离子)     

混合含氟对甲苄醇类菊酯的合成及其杀虫活性

报道了4种混合含氟对甲苄醇类拟除虫菊酯的新化合物,即三氟甲基氯菊酸、(±)-cis-二氯菊酸、(±)-trans-二氯菊酸、( )-trans-第一菊酸的含氟对甲苄酯的合成.生物活性测试的结果表明这些化合物对淡色库蚊四龄孑孓显示出较高的杀虫活性.