验证变力作用下的动量定理

利用CBL技术在变力作用下验证了动量定理,并介绍了实验原理及实验步骤.     

Structure and features of the fragmentation of the products of the reduction of dubinidinone

The Clemmensen reduction of dubinidinone (II) leads to the hydrogenolysis of the dihydrofuran ring with the predominant formation of α-methoxy-α-methyl-α,β-dihydropyrano-2-quinolone. An explanation of the characteristics of the fragmentation of the products of the reduction of dubinidinone has been found.     

Two new steroidal glucosides from Ophiopogon.japonicus （L.f.） Ker-Gawl

Two new steroidal glucosides, 26-O-β-D-glucopyranosyl （25S）-furost-5-ene-1β,3β,22α,26-tetraol l-O-β-D-xylopyranosyl- （1 → 3）-[α-h-rhamnopyranosyl-（1 → 2）]-[β-D-fueopyranoside and （25R） spirost-5-ene-3β,14α-diol-3-β-O-β-L-rhanmopyranosyl- （1 → 2）-[β-D-xylopyranosyl（1 → 4）]-[-β-D-glucopyranoside, were isolated from the Ophiopogon japonicus （L.f.） Ker-Gaw. Their structures were elucidated by spectroscopic methods.     

Synthesis of rupestonic acid amide derivatives and their <Emphasis Type="Italic">in vitro</Emphasis> activity against type A<Subscript>3</Subscript> and B flu virus and herpes simplex I and II

Derivatives of rupestonic acid (5a–e) were synthesized and evaluated preliminarily at the National Center for Drug Screening (PRC) for antiviral activity against type A₃ and B flu virus and HSV-I and HSV-II in order to improve the biological activity of rupestonic acid. It was found that compound 5b was more active than rupestonic acid against type A₃ flu virus. __________ Translated from Khimiya Prirodnykh Soedinenii, No. 3, pp. 247–249, May–June, 2008.     

Removal of methylene blue by seed-watermelon pulp-based low-cost adsorbent: Study of adsorption isotherms and kinetic models

Based on the abundance of seed-watermelon pulp (SWP) in Xinjiang, China, SWP was employed to prepare low-cost adsorbent toward the removal of methylene blue (MB). The effects of contact time at different initial concentration were studied. The widely used adsorption isotherm models including Langmuir, Freundlich, and Temkin isotherms were employed to depict the adsorption process. The Langmuir isotherm was best fitted to the experimental data. Batch kinetic studies showed that an equilibrium time of 300 minutes was needed for the adsorption. The adsorption properties can be well described by pseudo-second-order kinetic model and the MB uptake was not controlled by intraparticle diffusion mechanism.     

统一超混沌系统的投影同步

利用两种方法研究了统一超混沌系统的同步问题.首先以全状态混合投影自适应同步方法,基于Lyapunov稳定性理论,设计了自适应控制器,理论证明了该控制器可以实现参数已知的统一超混沌系统的全状态混合映射同步.其次使用主动控制同步方法,设计了同步控制器,实现了统一超混沌系统的完全同步,最后数值仿真实验进一步验证了所提出方案的有效性. 关键词： 统一超混沌系统 自适应控制器 全状态混合投影同步 主动控制同步     

参数未知的统一超混沌系统自适应反同步

文章研究了参数未知的统一超混沌系统的控制与同步问题.首先基于Lyapunov稳定性理论,设计了自适应控制器,证明了该控制器可使参数未知统一超混沌系统渐近稳定于不动点.其次使用自适应反同步方法,设计了自适应同步控制器,实现了参数未知统一超混沌系统的完全同步,最后数值仿真实验进一步验证了所提出方案的有效性. 关键词： 统一超混沌系统 自适应控制器 自适应反同步     

Landau Damping of Collective Mode in a Quasi-One-Dimensional Repulsive Bose-Einstein Condensate

We investigate the Landau damping of the collective mode in a quasi-one-dimensional repulsive Bose-Einstein condensate by using the self-consistent time-dependent Hartree-Fock-Bogoliubov approximation. We put forward a new method to calculate the Landau damping rate of the collective mode in the condensate and discuss the dependence of the Landau damping on temperature, on transverse trapping frequency, on atom number in the condensate, and on length of the system. Different from the usual calculation method for the three dimension system, our new calculation method is an interactive one by considering the practical relaxation of the elementary excitation. With little approximation, our theoretical calculation results agree with the experimental ones. Comparing with the usual calculation method, our theory is helpful to deduce the inter-particle interactions in damping phenomenon.     

近红外特征谱段相关系数法测定中药胶囊中添加枸橼酸西地那非

利用近红外特征谱段相关系数法对中药胶囊中是否添加枸橼酸西地那非进行快速定性分析.分别使用近红外光谱仪的积分球和光纤附件测定光谱,以枸橼酸西地那非化学对照品的近红外光谱为参照光谱,选择特定谱段,根据枸橼酸西地那非被掺入胶囊中的最小起效浓度建立待测样品光谱与参照光谱在该谱段的相似系数阈值,定性判断待测样品是否含有枸橼酸西地那非.积分球方法:选择6070～5800 cm~(-1)和4170～4070 cm~(-1)谱段,阈值为70%,用79个含枸橼酸西地那非的市售样品验证该方法,相关系数大于70%的有72个,占样品总量的91.14%;光纤方法:选定6070～5800 cm~(-1)谱段为特征谱段,设定阈值为65%,用247个含枸橼酸西地那非的市售样品进行验证,相关系数大于65%的有216个,占样品总量的87.45%.实验证明此方法具有较好的预测能力,可作为市场上该种非法添加药物的快速有效检查手段.