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An efficient method for mono-phosphorylation of 2(KRP203)using cbz-protection,dibenzylphosphoryl chloride and TMSI affording 2-P(KRP203-P)was developed.We applied the present method to the synthesis of KRP203 phosphate analogs which were difficult to produce through tradition procedures. 相似文献
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以聚丙烯腈(PAN)为原料,经静电纺丝、稳定化和碳化,制备了碳纳米纤维(CNFs)。系统地研究了氮的种类及含量对锂离子电池(LIBs)中Li+的储存性能和负极容量的影响。碳化过程中纤维从无定形碳向石墨化碳结构转变,含氮官能团减少,结构的变化对Li+在CNFs电极中的存储位置有很大的影响。结果表明,Li+不仅可以存储在石墨化碳层之间,还可以存储在氮功能化引起的缺陷部位,后者主要是由于碳材料的氮掺杂而使LIBs的电化学性能改善。碳化温度为600℃时,可以产生足够高的氮含量,从而提高电极的容量。在电流密度为0.1 A·g^-1时,循环200次之后比容量高达560 mAh·g^-1,即使在1 A·g^-1的高电流密度下,循环1000次比电容量仍然保持在200 mAh·g^-1。 相似文献
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We have investigated the low-lying energy spectrum and electromagnetic transition strengths in even–even 76Se using the proton–neutron interacting boson model (IBM-2). The theoretical calculation for the energy levels and E2 and M1 transition strengths is in good agreement with the experimental data. Specifically, the excitation energy and E2 transition of ${0}_{2}^{+}$ state, which is intimately associated with shape coexistence, can be accurately reproduced. The analysis on low-lying states and the key structure indicators R1, R2, R3 and R4 and M1 transitions indicates that there is a coexistence between spherical shape and γ-soft shape in 76Se. 相似文献
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Properties of the triaxial superdeformed (TSD) bands of odd-A Lu isotopes are investigated systematically within the supersymmetry scheme including many-body interactions and a perturbation possessing the S0(5) (or SU(5)) symmetry on the rotational symmetry. Quantitatively good results of the γ-ray energies, the dynamical moments of inertia and the spin of the TSD bands in odd-A Lu isotopes are obtained. The calculation shows that the competition between the pairing and anti-pairing effects exists in these TSD bands. Meanwhile, the SU(3) symmetry in TSD bands are broken more seriously than in superdeformed (SD) bands. 相似文献
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Da-Li Zhang Hong Lu Huan-Yu Wang Xin-Qiao Li Yan-Bing Xu Zheng-Hua An Hui Wang Feng Shi Ping Wang Xiao-Yun Zhao 《中国物理C(英文版)》2017,41(5):056101-056101
The silicon-strip tracker of the China Seismo-Electromagnetic Satellite(CSES) consists of two doublesided silicon strip detectors(DSSDs) which provide incident particle tracking information.A low-noise analog ASIC VA140 was used in this study for DSSD signal readout.A beam test on the DSSD module was performed at the Beijing Test Beam Facility of the Beijing Electron Positron Collider(BEPC) using a 400–800 MeV/c proton beam.The pedestal analysis results,RMSE noise,gain correction,and intensity distribution of incident particles of the DSSD module are presented. 相似文献
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