Size-manipulable synthesis of single-crystalline BaMnO3 and BaTi1/2Mn1/2O3 nanorods/nanowires

We report a size-manipulable synthesis of single-crystalline nanorods/nanowires of barium manganite (BaMnO(3)) and barium titanium manganite (BaTi(1/2)Mn(1/2)O(3)) by using the composite-hydroxide-mediated approach. The synthesis cleanly yields nanorods with a hexagonal perovskite structure. Typical nanorods have widths ranging between 50 and 100 nm, and the lengths can be easily controlled by time and temperature or by adding a small amount of water during the synthesis process. Resistance measurement shows that a phase transition happened at 58 K on BaMnO(3). The photoluminescence spectrum of BaTi(1/2)Mn(1/2)O(3) presents two emission peaks at wavelengths of 465 and 593 nm, corresponding to blue and green fluorescence. The ability to synthesize nanorod manganites of a desired length should enable detailed investigations of the size-dependent evolution of magnetism, magnetoresistance, nanoscale phase separation, and realization of a nanodevice of magnetic sensors.     

鱼洗振动频率的分析和测量

运用薄板中的弯曲波波速公式和驻波图像计算了鱼洗的固有频率 ,利用李萨如图测量了不同水深时鱼洗的固有频率 ,并定性解释了水深对鱼洗的固有频率的影响 .     

Characterization and complete separation of major cyclolinopeptides in flaxseed oil by reversed‐phase chromatography

Organoleptic properties of flaxseed oil deteriorate during storage due to methionine oxidation in its major cyclolinopeptides. Cyclolinopeptide E was previously identified as being responsible for the manifestation of bitter taste with flaxseed oil ageing. We developed a chromatographic procedure to monitor the oxidation of major cyclic peptides in flaxseed oil. We also used liquid chromatography with mass spectrometry and high‐efficiency core–shell reversed‐phase sorbents to study the separation of cyclolinopeptides in detail. The Kinetex^TM family of stationary phases (C₈, C₁₈, phenyl‐hexyl) was tested, along with the standard porous Luna^TM C₁₈(2) media. We found that only the phenyl‐hexyl stationary phase allows for complete resolution of major cyclolinopeptides, thus permitting direct UV monitoring of degree of conversion for cyclolinopeptide B into C and L into E. We also report, for the first time, a significant effect of peak splitting for some methionine S‐oxide (Mso) containing cyclolinopeptides, which most likely appear due to diastereomerization. This results in poor separation efficiency for cyclolinopeptides F, G, and E, and gives baseline resolution of diastereomeric pairs for cyclolinopeptides I and P. Thus, a single oxidation of cyclolinopeptide N yields three distinct chromatographic peaks corresponding to cyclolinopeptide T (cyclo‐MsoLMPFFWV, reported for the first time) and pair of cyclolinopeptide I (cyclo‐MLMsoPFFWV) diastereomers.     

复杂网络可控性研究现状综述

控制复杂系统是人们对复杂系统模型结构及相关动力学进行研究的最终目标, 反映人们对复杂系统的认识能力. 近年来, 通过控制理论和复杂性科学相结合,复杂网络可控性的研究引起了人们的广泛关注. 在过去的几年内, 来自国内外不同领域的研究人员从不同的角度对复杂网络可控性进行了深入的分析研究, 取得了丰硕的成果. 本文重点讨论了复杂网络的结构可控性研究进展, 详细介绍了基于最大匹配方法的复杂网络结构可控性分析框架, 综述了自2011年以来复杂网络可控性的相关研究成果, 具体论述了不同类型的可控性、可控性与网络拓扑结构统计特征的关联、基于可控性的网络及节点度量、控制的鲁棒性和可控性的相关优化方法. 最后, 对网络可控性未来的研究动态进行了展望, 有助于国内同行开展网络可控性的相关研究.     

On exponential sums over primes in short intervals

Let Λ(n) be the von Mangoldt function, x real and y small compared with x. This paper gives a non-trivial estimate on the exponential sum over primes in short intervals S₂(x,y;a)=?_{x < n ￡ x+y}L(n)e(n² a)S_2(x,y;{\alpha})=\sum_{x < n \le x+y}\Lambda(n)e(n^2 {\alpha}) for all α ∈ [0,1] whenever x^\frac23+e ￡ y ￡ xx^{\frac{2}{3}+{\varepsilon}}\le y \le x . This result is as good as what was previously derived from the Generalized Riemann Hypothesis.     

Self-focusing effect in voltage-controlled PPLN waveguide arrays

Self-focusing effect via Kerr nonlinearity is observed in periodically poled lithium niobate (PPLN) waveguide arrays formed by electro-optic effect. Voltage-control method is demonstrated to control the focusing and diffraction of light. Theoretical simulation results show good agreement with experimental results.     

9MeV,小于0.1mm微焦点X射线源验证实验

密度高、成像分辨率高、成像速度快的X射线数字成像检测需要高能微焦点大剂量X射线源,高品质电子源是实现这一X射线源的关键手段。基于中国工程物理研究院太赫兹自由电子激光的主加速器,验证了低发射度、低能散度的高亮度电子束实现高能微焦点的可行性,得到电子束半高全宽尺寸小于70μm的9 MeV微焦点,并初步开展成像实验,双丝像质计焦斑清晰分辨9D号丝,丝直径0.13 mm。