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排序方式: 共有321条查询结果,搜索用时 15 毫秒
21.
Most macroeconomic time series are reported on a quarterly basis. However, in many cases, official statistical agencies report annual (or ‘year-on-year’) growth rates rather than the quarterly data themselves. In this paper, we demonstrate how to recover seasonally adjusted quarterly growth rates from annual growth rates that are reported quarterly. As an illustration, we apply the technique to the highly seasonal UK Retail Sales series. Using only the annual growth rates calculated from the underlying data, we find that our procedure generates estimated seasonally adjusted quarterly growth rates that are almost indistinguishable from the ‘true’ seasonally adjusted quarterly growth rates. 相似文献
22.
Avcı Davut Altürk Sümeyye Sönmez Fatih Tamer Ömer Başoğlu Adil Atalay Yusuf Zengin Kurt Belma Dege Necmi 《Molecular diversity》2021,25(1):171-189
Molecular Diversity - The World Health Organization (WHO) report shows that diabetes mellitus (DM) will be one of the ten deadly diseases in the near future. The best way to prevent DM is to... 相似文献
23.
Selçuk Demir Hamide Merve Çepni Małgorzata Hołyńska Muammer Kavanoz Fatih Yilmaz Yunus Zorlu 《Journal of Coordination Chemistry》2017,70(19):3422-3433
Via an oxidation reaction of Cu(I) iodide with pyridine-2,6-dicarboxylic acid (H2L) in DMF three copper(II) complexes, [(CH3)2NH2]2[CuL2] (1), K2[CuL2]?H2L?H2O (2) and [Cu(L)(H2O)]n (3), were synthesized and characterized. The structures of 1–3 were determined by single crystal X-ray diffraction studies. In-situ DMF decomposition produces dimethylamine base under solvothermal conditions and a proton transfer reaction takes place for the complex formation of 1. 3-D networks are stabilized in 1 and 2 via hydrogen bonds. Complex 3 is a 1-D coordination polymer with Cu-O semi-coordination bonds. Thermal decomposition of the complexes results in the corresponding metal oxides. Also, the electrochemical behavior of 1 was determined to be a metal-centered and diffusion-controlled, one-electron reduction process. 相似文献
24.
Güneş Y Polat MF Sahin E Fleming FF Altundas R 《The Journal of organic chemistry》2010,75(21):7092-7098
Quaternary oxonitriles are stereoselectively generated from the union of five-, six-, and seven-membered 2-chloroalkenecarbonitriles with chiral alcohols via a Claisen rearrangement. The strategy rests on a new conjugate addition-elimination of allylic alkoxides to 2-chlorocycloalkenecarbonitriles to afford substituted 2-alkoxyalkenenitriles. Subsequent thermolysis unmasks a cyclic oxonitrile while selectively forming a new quaternary center with enantiomeric ratios typically greater than 9:1. The overall alkylation strategy addresses the challenge of enantioselectively generating hindered, quaternary centers while simultaneously installing ketone, nitrile, and olefin functionalities. 相似文献
25.
Dynamic diffraction gratings can be microfabricated with precision and offer extremely sensitive displacement measurements and light intensity modulation. The effect of pure translation of the moving part of the grating on diffracted order intensities is well known. This study focuses on the parameters that limit the intensity and the contrast of the interference. The effects of grating duty cycle, mirror reflectivities, sensor tilt and detector size are investigated using Fourier optics theory and Gaussian beam optics. Analytical findings reveal that fringe visibility becomes <0.3 when the optical path variation exceeds half the wavelength within the grating interferometer. The fringe visibility can be compensated by monitoring the interfering portion of the diffracted order light only through detector size reduction in the expense of optical power. Experiments were conducted with a grating interferometer that resulted in an eightfold increase in fringe visibility with reduced detector size, which is in agreement with theory. Findings show that diffraction grating readout principle is not limited to translating sensors but also can be used for sensors with tilt or other deflection modes. 相似文献
26.
This paper presents a novel discrete artificial bee colony (DABC) algorithm for solving the multi-objective flexible job shop scheduling problem with maintenance activities. Performance criteria considered are the maximum completion time so called makespan, the total workload of machines and the workload of the critical machine. Unlike the original ABC algorithm, the proposed DABC algorithm presents a unique solution representation where a food source is represented by two discrete vectors and tabu search (TS) is applied to each food source to generate neighboring food sources for the employed bees, onlooker bees, and scout bees. An efficient initialization scheme is introduced to construct the initial population with a certain level of quality and diversity. A self-adaptive strategy is adopted to enable the DABC algorithm with learning ability for producing neighboring solutions in different promising regions whereas an external Pareto archive set is designed to record the non-dominated solutions found so far. Furthermore, a novel decoding method is also presented to tackle maintenance activities in schedules generated. The proposed DABC algorithm is tested on a set of the well-known benchmark instances from the existing literature. Through a detailed analysis of experimental results, the highly effective and efficient performance of the proposed DABC algorithm is shown against the best performing algorithms from the literature. 相似文献
27.
In this study, single stage (SS), double-stage (DS), and gain flattened (GF) DS L-band erbium-doped fiber amplifier (EDFA) configurations are designed in order to obtain a flat gain amplifier. Temperature dependence of the mentioned configurations is also analyzed. Maximum spectral dependence of EDFA gain with respect to temperature is obtained for SS EDFA design while smaller spectral dependence of gains is obtained for both DS and GF DS L-EDFA configurations. It is observed that the maximum temperature dependence is in the range of 1570-1580 nm band for all configurations. It has also been found that for all configurations, reducing the temperature has greater effect than raising the temperature on EDFA gain. The overall results show that a temperature independent L-band configuration has not been possible. However, for some signal wavelengths, the erbium-doped fiber (EDF) lengths at which the gain is temperature independent are observed. 相似文献
28.
The Ni(II), Cu(II) Co(II) and Zn(II) complexes of 2,3‐hydroxyimino‐4‐phenyl‐6‐phenyazo‐1‐thia‐4,5‐diaza‐ cyclohexa‐5‐diene (H2L) were synthesized. Thermal behavior of these complexes was studied in dynamic nitrogen atmosphere by TA (thermogravimetric analysis), DTA (differential thermal analysis) and DTG (differential thermal gravimetry) techniques. The reaction order, the activation energies, the entropies, the enthalpies, the free energies, and the pre‐exponential factors of the thermal decomposition reactions were calculated from the thermogravimetric curves. The kinetic analysis of the thermogravimetric data was performed by using several methods such as MacCallum‐Tanner (MT), van Krevelen (vK), Madhusudanan‐Krishnan‐Ninan (MKN), Wanjun‐Yuwen‐Hen‐Cunxin (WYHC), Horowitz‐Metzger (HM) and Coats‐Redfern method (CR) based on the single heating rate. Most appropriate methods were determined for each decomposition step according to the least‐square linear regression. The Ni(II), Cu(II) Co(II) and Zn(II) complexes displayed one‐ or two‐stage decomposition pattern when heating in a dynamic nitrogen atmosphere and metal oxides remained as end products of the complexes. The characterization of the end products of the decomposition was performed by X‐ray diffraction. 相似文献
29.
In this paper, a new algorithm to solve a general 0–1 programming problem with linear objective function is developed. Computational experiences are carried out on problems where the constraints are inequalities on polynomials. The solution of the original problem is equivalent with the solution of a sequence of set packing problems with special constraint sets. The solution of these set packing problems is equivalent with the ordering of the binary vectors according to their objective function value. An algorithm is developed to generate this order in a dynamic way. The main tool of the algorithm is a tree which represents the desired order of the generated binary vectors. The method can be applied to the multi-knapsack type nonlinear 0–1 programming problem. Large problems of this type up to 500 variables have been solved. 相似文献
30.
Murat Kaya Mehmet Gökhan Halıcı Fatih Duman Sevil Erdoğan Talat Baran 《Natural product research》2015,29(13):1280-1284
Lichens are symbiotic associations formed mainly by ascomycete fungi and green algae or cyanobacteria. The presence of chitin in the fungal cell wall has been revealed by previous studies. Considering the presence of fungi in the lichens, this work determines the presence of chitin in a cosmopolitan lichen species Xanthoria parietina. In this study, chitin was derived from a lichen species for the first time and its physicochemical properties were determined by Fourier transform infrared spectroscopy, thermogravimetric analysis, X-ray diffraction, scanning electron microscopy and elemental analysis. The dry weight chitin content of X. parietina was 4.23%, and this chitin was in the α-form. The crystalline index value of the lichen chitin was calculated as 70.1%. The chitin from X. parietina had a smooth surface. 相似文献